BMRB Entry 5569
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR5569
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Title: 15N relaxation rates for backbone of GB1 PubMed: 12473458
Deposition date: 2002-10-31 Original release date: 2011-08-10
Authors: Idiyatullin, Djaudat; Nesmelova, Irina; Daragan, Vladimir; Mayo, Kevin
Citation: Idiyatullin, Djaudat; Nesmelova, Irina; Daragan, Vladimir; Mayo, Kevin. "Heat Capacities and a Snapshot of the Energy Landscape in Protein GB1 from the Pre-denaturation Temperature Dependence of Backbone NH Nanosecond Fluctuations" J. Mol. Biol. 325, 149-162 (2003).
Assembly members:
immunoglobulin-binding domain, polymer, 56 residues, Formula weight is not available
Natural source: Common Name: Streptococcus Taxonomy ID: 1301 Superkingdom: Eubacteria Kingdom: not available Genus/species: Streptococcus not available
Experimental source: Production method: recombinant technology
Entity Sequences (FASTA):
immunoglobulin-binding domain: MTYKLILNGKTLKGETTTEA
VDAATAEKVFKQYANDNGVD
GEWTYDDATKTFTVTE
- assigned_chemical_shifts
- heteronucl_NOEs
- heteronuclear_NOE_500_1
- heteronuclear_NOE_500_2
- heteronuclear_NOE_500_3
- heteronuclear_NOE_500_4
- heteronuclear_NOE_500_5
- heteronuclear_NOE_500_6
- heteronuclear_NOE_500_7
- heteronuclear_NOE_500_8
- heteronuclear_NOE_500_9
- heteronuclear_NOE_500_10
- heteronuclear_NOE_600_1
- heteronuclear_NOE_600_2
- heteronuclear_NOE_600_3
- heteronuclear_NOE_600_4
- heteronuclear_NOE_600_5
- heteronuclear_NOE_600_6
- heteronuclear_NOE_600_7
- heteronuclear_NOE_600_8
- heteronuclear_NOE_600_9
- heteronuclear_NOE_600_10
- heteronuclear_NOE_800_1
- heteronuclear_NOE_800_2
- heteronuclear_NOE_800_3
- heteronuclear_NOE_800_4
- heteronuclear_NOE_800_5
- heteronuclear_NOE_800_6
- heteronuclear_NOE_800_7
- heteronuclear_NOE_800_8
- heteronuclear_NOE_800_9
- heteronuclear_NOE_800_10
- heteronucl_T1_relaxation
- T1_relaxation_500_1
- T1_relaxation_500_2
- T1_relaxation_500_3
- T1_relaxation_500_4
- T1_relaxation_500_5
- T1_relaxation_500_6
- T1_relaxation_500_7
- T1_relaxation_500_8
- T1_relaxation_500_9
- T1_relaxation_500_10
- T1_relaxation_600_1
- T1_relaxation_600_2
- T1_relaxation_600_3
- T1_relaxation_600_4
- T1_relaxation_600_5
- T1_relaxation_600_6
- T1_relaxation_600_7
- T1_relaxation_600_8
- T1_relaxation_600_9
- T1_relaxation_600_10
- T1_relaxation_800_1
- T1_relaxation_800_2
- T1_relaxation_800_3
- T1_relaxation_800_4
- T1_relaxation_800_5
- T1_relaxation_800_6
- T1_relaxation_800_7
- T1_relaxation_800_8
- T1_relaxation_800_9
- T1_relaxation_800_10
- heteronucl_T2_relaxation
- T2_relaxation_500_1
- T2_relaxation_500_2
- T2_relaxation_500_3
- T2_relaxation_500_4
- T2_relaxation_500_5
- T2_relaxation_500_6
- T2_relaxation_500_7
- T2_relaxation_500_8
- T2_relaxation_500_9
- T2_relaxation_500_10
- T2_relaxation_600_1
- T2_relaxation_600_2
- T2_relaxation_600_3
- T2_relaxation_600_4
- T2_relaxation_600_5
- T2_relaxation_600_6
- T2_relaxation_600_7
- T2_relaxation_600_8
- T2_relaxation_600_9
- T2_relaxation_600_10
- T2_relaxation_800_1
- T2_relaxation_800_2
- T2_relaxation_800_3
- T2_relaxation_800_4
- T2_relaxation_800_5
- T2_relaxation_800_6
- T2_relaxation_800_7
- T2_relaxation_800_8
- T2_relaxation_800_9
- T2_relaxation_800_10
Data type | Count |
T1 relaxation values | 1680 |
T2 relaxation values | 1680 |
Additional metadata:
Assembly:
Entity Assembly ID | Entity Name | Entity ID |
---|---|---|
1 | GB1 monomer | 1 |
Entities:
Entity 1, GB1 monomer 56 residues - Formula weight is not available
1 | MET | THR | TYR | LYS | LEU | ILE | LEU | ASN | GLY | LYS | ||||
2 | THR | LEU | LYS | GLY | GLU | THR | THR | THR | GLU | ALA | ||||
3 | VAL | ASP | ALA | ALA | THR | ALA | GLU | LYS | VAL | PHE | ||||
4 | LYS | GLN | TYR | ALA | ASN | ASP | ASN | GLY | VAL | ASP | ||||
5 | GLY | GLU | TRP | THR | TYR | ASP | ASP | ALA | THR | LYS | ||||
6 | THR | PHE | THR | VAL | THR | GLU |
Samples:
sample_1: immunoglobulin-binding domain, [U-15N], 10 10 mg/mL
Ex-cond_1: pH: 5.25; temperature: 278 K
Ex-cond_2: pH: 5.25; temperature: 283 K
Ex-cond_3: pH: 5.25; temperature: 288 K
Ex-cond_4: pH: 5.25; temperature: 293 K
Ex-cond_5: pH: 5.25; temperature: 298 K
Ex-cond_6: pH: 5.25; temperature: 303 K
Ex-cond_7: pH: 5.25; temperature: 308 K
Ex-cond_8: pH: 5.25; temperature: 313 K
Ex-cond_9: pH: 5.25; temperature: 318 K
Ex-cond_10: pH: 5.25; temperature: 323 K
Experiments:
Name | Sample | Sample state | Sample conditions |
---|---|---|---|
1H-15N HSQC | not available | not available | not available |
Steady-state {1H}-15N NOE | not available | not available | not available |
Software:
NMRView - calculating relaxation rates, peak assignments
NMR spectrometers:
- Varian INOVA 500 MHz
- Varian INOVA 600 MHz
- Varian INOVA 800 MHz