BMRB Entry 21013
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR21013
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Title: DPC micelle bound RI23
Deposition date: 2011-06-11 Original release date: 2012-06-01
Authors: Bhattacharjya, Surajit; Saravanan, Rathi
Citation: Bhattacharjya, Surajit; Saravanan, Rathi. "." Not known ., .-..
Assembly members:
RI23, polymer, 23 residues, Formula weight is not available
Natural source: Common Name: not available Taxonomy ID: not available Superkingdom: not available Kingdom: not available Genus/species: not available not available
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
RI23: RVKRVWPLVIRTVIAGYNLY
RAI
- assigned_chemical_shifts
Data type | Count |
1H chemical shifts | 147 |
Additional metadata:
Assembly:
Entity Assembly ID | Entity Name | Entity ID |
---|---|---|
1 | RI23 | 1 |
Entities:
Entity 1, RI23 23 residues - Formula weight is not available
1 | ARG | VAL | LYS | ARG | VAL | TRP | PRO | LEU | VAL | ILE | ||||
2 | ARG | THR | VAL | ILE | ALA | GLY | TYR | ASN | LEU | TYR | ||||
3 | ARG | ALA | ILE |
Samples:
sample_1: RI23 500 uM; DPC 10 uM; H2O 90%; D2O 10%
sample_conditions_1: pH: 4.8; temperature: 310 K
Experiments:
Name | Sample | Sample state | Sample conditions |
---|---|---|---|
2D 1H-1H NOESY | sample_1 | isotropic | sample_conditions_1 |
2D 1H-1H TOCSY | sample_1 | isotropic | sample_conditions_1 |
Software:
CYANA, Guntert, Mumenthaler and Wuthrich - refinement
NMR spectrometers:
- Bruker AMX 600 MHz