MR Sample id: ZR18.NC.LS.II.86 buffer: 20mM MES, 100mM NaCl, 5mM CaCl2 10mM DTT, 0.02% NaN2, 5% D2O conc: 1.3 mM pH 6.5, 40C prepared by: Rong experiment: HNHA 3D - 32h instrument: INOVA500 probe 3047 acquired by: jma 05-02-03 ProteinPack configuration some water echoes HH 2D without c13 decoupling