data_30232 ####################### # Entry information # ####################### save_entry_information _Entry.Sf_category entry_information _Entry.Sf_framecode entry_information _Entry.ID 30232 _Entry.Title ; ovGRN12-35_3s ; _Entry.Type macromolecule _Entry.Version_type original _Entry.Submission_date 2017-01-17 _Entry.Accession_date 2017-01-17 _Entry.Last_release_date 2017-02-03 _Entry.Original_release_date 2017-02-03 _Entry.Origination author _Entry.Format_name . _Entry.NMR_STAR_version 3.2.0.16 _Entry.Original_NMR_STAR_version 3.2.0.10 _Entry.Experimental_method NMR _Entry.Experimental_method_subtype SOLUTION _Entry.Source_data_format . _Entry.Source_data_format_version . _Entry.Generated_software_name . _Entry.Generated_software_version . _Entry.Generated_software_ID . _Entry.Generated_software_label . _Entry.Generated_date . _Entry.DOI . _Entry.UUID . _Entry.Related_coordinate_file_name . _Entry.Details . _Entry.BMRB_internal_directory_name . loop_ _Entry_author.Ordinal _Entry_author.Given_name _Entry_author.Family_name _Entry_author.First_initial _Entry_author.Middle_initials _Entry_author.Family_title _Entry_author.ORCID _Entry_author.Entry_ID 1 P. Bansal P. . . . 30232 2 M. Smout M. . . . 30232 3 D. Wilson D. . . . 30232 4 C. Caceres C. C. . . 30232 5 M. Dastpeyman M. . . . 30232 6 J. Sotillo J. . . . 30232 7 J. Seifert J. . . . 30232 8 P. Brindley P. . . . 30232 9 A. Loukas A. . . . 30232 10 N. Daly N. . . . 30232 stop_ loop_ _Struct_keywords.Keywords _Struct_keywords.Text _Struct_keywords.Entry_ID CYTOKINE . 30232 'STRUCTURE FROM CYANA 3.97' . 30232 'Wound healing agent' . 30232 granulin . 30232 stop_ loop_ _Data_set.Type _Data_set.Count _Data_set.Entry_ID assigned_chemical_shifts 1 30232 spectral_peak_list 1 30232 stop_ loop_ _Datum.Type _Datum.Count _Datum.Entry_ID '13C chemical shifts' 32 30232 '1H chemical shifts' 127 30232 stop_ loop_ _Release.Release_number _Release.Format_type _Release.Format_version _Release.Date _Release.Submission_date _Release.Type _Release.Author _Release.Detail _Release.Entry_ID 1 . . 2018-01-17 . original BMRB . 30232 stop_ loop_ _Related_entries.Database_name _Related_entries.Database_accession_code _Related_entries.Relationship _Related_entries.Entry_ID BMRB 30233 ov-GRN12-34 30232 PDB 5UJG 'BMRB Entry Tracking System' 30232 stop_ save_ ############### # Citations # ############### save_citation_1 _Citation.Sf_category citations _Citation.Sf_framecode citation_1 _Citation.Entry_ID 30232 _Citation.ID 1 _Citation.Class 'entry citation' _Citation.CAS_abstract_code . _Citation.MEDLINE_UI_code . _Citation.DOI . _Citation.PubMed_ID . _Citation.Full_citation . _Citation.Title ; ovGRN12-35_3s ; _Citation.Status 'in preparation' _Citation.Type journal _Citation.Journal_abbrev . _Citation.Journal_name_full . _Citation.Journal_volume . _Citation.Journal_issue . _Citation.Journal_ASTM . _Citation.Journal_ISSN . _Citation.Journal_CSD 0353 _Citation.Book_title . _Citation.Book_chapter_title . _Citation.Book_volume . _Citation.Book_series . _Citation.Book_publisher . _Citation.Book_publisher_city . _Citation.Book_ISBN . _Citation.Conference_title . _Citation.Conference_site . _Citation.Conference_state_province . _Citation.Conference_country . _Citation.Conference_start_date . _Citation.Conference_end_date . _Citation.Conference_abstract_number . _Citation.Thesis_institution . _Citation.Thesis_institution_city . _Citation.Thesis_institution_country . _Citation.WWW_URL . _Citation.Page_first . _Citation.Page_last . _Citation.Year . _Citation.Details . loop_ _Citation_author.Ordinal _Citation_author.Given_name _Citation_author.Family_name _Citation_author.First_initial _Citation_author.Middle_initials _Citation_author.Family_title _Citation_author.ORCID _Citation_author.Entry_ID _Citation_author.Citation_ID 1 P. Bansal P. . . . 30232 1 2 M. Smout M. . . . 30232 1 3 D. Wilson D. . . . 30232 1 4 C. Caceres C. C. . . 30232 1 5 M. Dastpeyman M. . . . 30232 1 6 J. Sotillo J. . . . 30232 1 7 J. Seifert J. . . . 30232 1 8 P. Brindley P. . . . 30232 1 9 A. Loukas A. . . . 30232 1 10 N. Daly N. . . . 30232 1 stop_ save_ ############################################# # Molecular system (assembly) description # ############################################# save_assembly _Assembly.Sf_category assembly _Assembly.Sf_framecode assembly _Assembly.Entry_ID 30232 _Assembly.ID 1 _Assembly.Name Granulin _Assembly.BMRB_code . _Assembly.Number_of_components . _Assembly.Organic_ligands . _Assembly.Metal_ions . _Assembly.Non_standard_bonds . _Assembly.Ambiguous_conformational_states . _Assembly.Ambiguous_chem_comp_sites . _Assembly.Molecules_in_chemical_exchange . _Assembly.Paramagnetic no _Assembly.Thiol_state . _Assembly.Molecular_mass . _Assembly.Enzyme_commission_number . _Assembly.Details . _Assembly.DB_query_date . _Assembly.DB_query_revised_last_date . loop_ _Entity_assembly.ID _Entity_assembly.Entity_assembly_name _Entity_assembly.Entity_ID _Entity_assembly.Entity_label _Entity_assembly.Asym_ID _Entity_assembly.PDB_chain_ID _Entity_assembly.Experimental_data_reported _Entity_assembly.Physical_state _Entity_assembly.Conformational_isomer _Entity_assembly.Chemical_exchange_state _Entity_assembly.Magnetic_equivalence_group_code _Entity_assembly.Role _Entity_assembly.Details _Entity_assembly.Entry_ID _Entity_assembly.Assembly_ID 1 entity_1 1 $entity_1 A A yes . . . . . . 30232 1 stop_ loop_ _Bond.ID _Bond.Type _Bond.Value_order _Bond.Assembly_atom_ID_1 _Bond.Entity_assembly_ID_1 _Bond.Entity_assembly_name_1 _Bond.Entity_ID_1 _Bond.Comp_ID_1 _Bond.Comp_index_ID_1 _Bond.Seq_ID_1 _Bond.Atom_ID_1 _Bond.Assembly_atom_ID_2 _Bond.Entity_assembly_ID_2 _Bond.Entity_assembly_name_2 _Bond.Entity_ID_2 _Bond.Comp_ID_2 _Bond.Comp_index_ID_2 _Bond.Seq_ID_2 _Bond.Atom_ID_2 _Bond.Auth_entity_assembly_ID_1 _Bond.Auth_entity_assembly_name_1 _Bond.Auth_asym_ID_1 _Bond.Auth_seq_ID_1 _Bond.Auth_comp_ID_1 _Bond.Auth_atom_ID_1 _Bond.Auth_entity_assembly_ID_2 _Bond.Auth_entity_assembly_name_2 _Bond.Auth_asym_ID_2 _Bond.Auth_seq_ID_2 _Bond.Auth_comp_ID_2 _Bond.Auth_atom_ID_2 _Bond.Entry_ID _Bond.Assembly_ID 1 disulfide single . 1 . 1 CYS 1 1 SG . 1 . 1 CYS 14 14 SG . . . . . . . . . . . . 30232 1 2 disulfide single . 1 . 1 CYS 8 8 SG . 1 . 1 CYS 23 23 SG . . . . . . . . . . . . 30232 1 3 disulfide single . 1 . 1 CYS 15 15 SG . 1 . 1 CYS 24 24 SG . . . . . . . . . . . . 30232 1 stop_ save_ #################################### # Biological polymers and ligands # #################################### save_entity_1 _Entity.Sf_category entity _Entity.Sf_framecode entity_1 _Entity.Entry_ID 30232 _Entity.ID 1 _Entity.BMRB_code . _Entity.Name Granulin _Entity.Type polymer _Entity.Polymer_common_type . _Entity.Polymer_type polypeptide(L) _Entity.Polymer_type_details . _Entity.Polymer_strand_ID A _Entity.Polymer_seq_one_letter_code_can . _Entity.Polymer_seq_one_letter_code ; CPDPVYTCRPGQTCCRGLHG YGCC ; _Entity.Target_identifier . _Entity.Polymer_author_defined_seq . _Entity.Polymer_author_seq_details . _Entity.Ambiguous_conformational_states . _Entity.Ambiguous_chem_comp_sites . _Entity.Nstd_monomer no _Entity.Nstd_chirality . _Entity.Nstd_linkage no _Entity.Nonpolymer_comp_ID . _Entity.Nonpolymer_comp_label . _Entity.Number_of_monomers 24 _Entity.Number_of_nonpolymer_components . _Entity.Paramagnetic no _Entity.Thiol_state . _Entity.Src_method syn _Entity.Parent_entity_ID 1 _Entity.Fragment 'UNP residues 30-53' _Entity.Mutation . _Entity.EC_number . _Entity.Calc_isoelectric_point . _Entity.Formula_weight 2593.018 _Entity.Formula_weight_exptl . _Entity.Formula_weight_exptl_meth . _Entity.Details . _Entity.DB_query_date . _Entity.DB_query_revised_last_date . loop_ _Entity_comp_index.ID _Entity_comp_index.Auth_seq_ID _Entity_comp_index.Comp_ID _Entity_comp_index.Comp_label _Entity_comp_index.Entry_ID _Entity_comp_index.Entity_ID 1 1 CYS . 30232 1 2 2 PRO . 30232 1 3 3 ASP . 30232 1 4 4 PRO . 30232 1 5 5 VAL . 30232 1 6 6 TYR . 30232 1 7 7 THR . 30232 1 8 8 CYS . 30232 1 9 9 ARG . 30232 1 10 10 PRO . 30232 1 11 11 GLY . 30232 1 12 12 GLN . 30232 1 13 13 THR . 30232 1 14 14 CYS . 30232 1 15 15 CYS . 30232 1 16 16 ARG . 30232 1 17 17 GLY . 30232 1 18 18 LEU . 30232 1 19 19 HIS . 30232 1 20 20 GLY . 30232 1 21 21 TYR . 30232 1 22 22 GLY . 30232 1 23 23 CYS . 30232 1 24 24 CYS . 30232 1 stop_ loop_ _Entity_poly_seq.Hetero _Entity_poly_seq.Mon_ID _Entity_poly_seq.Num _Entity_poly_seq.Comp_index_ID _Entity_poly_seq.Entry_ID _Entity_poly_seq.Entity_ID . CYS 1 1 30232 1 . PRO 2 2 30232 1 . ASP 3 3 30232 1 . PRO 4 4 30232 1 . VAL 5 5 30232 1 . TYR 6 6 30232 1 . THR 7 7 30232 1 . CYS 8 8 30232 1 . ARG 9 9 30232 1 . PRO 10 10 30232 1 . GLY 11 11 30232 1 . GLN 12 12 30232 1 . THR 13 13 30232 1 . CYS 14 14 30232 1 . CYS 15 15 30232 1 . ARG 16 16 30232 1 . GLY 17 17 30232 1 . LEU 18 18 30232 1 . HIS 19 19 30232 1 . GLY 20 20 30232 1 . TYR 21 21 30232 1 . GLY 22 22 30232 1 . CYS 23 23 30232 1 . CYS 24 24 30232 1 stop_ save_ #################### # Natural source # #################### save_natural_source _Entity_natural_src_list.Sf_category natural_source _Entity_natural_src_list.Sf_framecode natural_source _Entity_natural_src_list.Entry_ID 30232 _Entity_natural_src_list.ID 1 loop_ _Entity_natural_src.ID _Entity_natural_src.Entity_ID _Entity_natural_src.Entity_label _Entity_natural_src.Entity_chimera_segment_ID _Entity_natural_src.NCBI_taxonomy_ID _Entity_natural_src.Type _Entity_natural_src.Common _Entity_natural_src.Organism_name_scientific _Entity_natural_src.Organism_name_common _Entity_natural_src.Organism_acronym _Entity_natural_src.ICTVdb_decimal_code _Entity_natural_src.Superkingdom _Entity_natural_src.Kingdom _Entity_natural_src.Genus _Entity_natural_src.Species _Entity_natural_src.Strain _Entity_natural_src.Variant _Entity_natural_src.Organ _Entity_natural_src.Tissue _Entity_natural_src.Tissue_fraction _Entity_natural_src.Cell_line _Entity_natural_src.Cell_type _Entity_natural_src.ATCC_number _Entity_natural_src.Organelle _Entity_natural_src.Secretion _Entity_natural_src.Plasmid _Entity_natural_src.Gene_mnemonic _Entity_natural_src.Details _Entity_natural_src.Entry_ID _Entity_natural_src.Entity_natural_src_list_ID 1 1 $entity_1 . 6198 organism . 'Opisthorchis viverrini' flatworms . . Eukaryota Metazoa Opisthorchis viverrini . . . . . . . . . . . . . 30232 1 stop_ save_ ######################### # Experimental source # ######################### save_experimental_source _Entity_experimental_src_list.Sf_category experimental_source _Entity_experimental_src_list.Sf_framecode experimental_source _Entity_experimental_src_list.Entry_ID 30232 _Entity_experimental_src_list.ID 1 loop_ _Entity_experimental_src.ID _Entity_experimental_src.Entity_ID _Entity_experimental_src.Entity_label _Entity_experimental_src.Entity_chimera_segment_ID _Entity_experimental_src.Production_method _Entity_experimental_src.Host_org_scientific_name _Entity_experimental_src.Host_org_name_common _Entity_experimental_src.Host_org_details _Entity_experimental_src.Host_org_NCBI_taxonomy_ID _Entity_experimental_src.Host_org_genus _Entity_experimental_src.Host_org_species _Entity_experimental_src.Host_org_strain _Entity_experimental_src.Host_org_variant _Entity_experimental_src.Host_org_ATCC_number _Entity_experimental_src.Vector_type _Entity_experimental_src.PDBview_host_org_vector_name _Entity_experimental_src.PDBview_plasmid_name _Entity_experimental_src.Vector_name _Entity_experimental_src.Vector_details _Entity_experimental_src.Vendor_name _Entity_experimental_src.Details _Entity_experimental_src.Entry_ID _Entity_experimental_src.Entity_experimental_src_list_ID 1 1 $entity_1 . 'chemical synthesis' . . . . . . . . . . . . . . . . 30232 1 stop_ save_ ##################################### # Sample contents and methodology # ##################################### ######################## # Sample description # ######################## save_sample_1 _Sample.Sf_category sample _Sample.Sf_framecode sample_1 _Sample.Entry_ID 30232 _Sample.ID 1 _Sample.Type solution _Sample.Sub_type . _Sample.Details '0.5 mM NA ov-GRN12-35_3S peptide, 90% H2O/10% D2O' _Sample.Aggregate_sample_number . _Sample.Solvent_system '90% H2O/10% D2O' _Sample.Preparation_date . _Sample.Preparation_expiration_date . _Sample.Polycrystallization_protocol . _Sample.Single_crystal_protocol . _Sample.Crystal_grow_apparatus . _Sample.Crystal_grow_atmosphere . _Sample.Crystal_grow_details . _Sample.Crystal_grow_method . _Sample.Crystal_grow_method_cit_ID . _Sample.Crystal_grow_pH . _Sample.Crystal_grow_pH_range . _Sample.Crystal_grow_pressure . _Sample.Crystal_grow_pressure_esd . _Sample.Crystal_grow_seeding . _Sample.Crystal_grow_seeding_cit_ID . _Sample.Crystal_grow_temp . _Sample.Crystal_grow_temp_details . _Sample.Crystal_grow_temp_esd . _Sample.Crystal_grow_time . _Sample.Oriented_sample_prep_protocol . _Sample.Lyophilization_cryo_protectant . _Sample.Storage_protocol . loop_ _Sample_component.ID _Sample_component.Mol_common_name _Sample_component.Isotopic_labeling _Sample_component.Assembly_ID _Sample_component.Assembly_label _Sample_component.Entity_ID _Sample_component.Entity_label _Sample_component.Product_ID _Sample_component.Type _Sample_component.Concentration_val _Sample_component.Concentration_val_min _Sample_component.Concentration_val_max _Sample_component.Concentration_val_units _Sample_component.Concentration_val_err _Sample_component.Vendor _Sample_component.Vendor_product_name _Sample_component.Vendor_product_code _Sample_component.Entry_ID _Sample_component.Sample_ID 1 D2O 'natural abundance' . . . . . . 10 . . % . . . . 30232 1 2 H2O 'natural abundance' . . . . . . 90 . . % . . . . 30232 1 3 'ov-GRN12-35_3S peptide' NA . . 1 $entity_1 . . 0.5 . . mM . . . . 30232 1 stop_ save_ ####################### # Sample conditions # ####################### save_sample_conditions_1 _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode sample_conditions_1 _Sample_condition_list.Entry_ID 30232 _Sample_condition_list.ID 1 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID pH 5 . pH 30232 1 pressure 1 . atm 30232 1 temperature 290 . K 30232 1 stop_ save_ ############################ # Computer software used # ############################ save_software_1 _Software.Sf_category software _Software.Sf_framecode software_1 _Software.Entry_ID 30232 _Software.ID 1 _Software.Type . _Software.Name CYANA _Software.Version . _Software.DOI . _Software.Details . loop_ _Vendor.Name _Vendor.Address _Vendor.Electronic_address _Vendor.Entry_ID _Vendor.Software_ID 'Guntert, Mumenthaler and Wuthrich' . . 30232 1 stop_ loop_ _Task.Task _Task.Entry_ID _Task.Software_ID 'structure calculation' 30232 1 stop_ save_ save_software_2 _Software.Sf_category software _Software.Sf_framecode software_2 _Software.Entry_ID 30232 _Software.ID 2 _Software.Type . _Software.Name CcpNMR _Software.Version . _Software.DOI . _Software.Details . loop_ _Vendor.Name _Vendor.Address _Vendor.Electronic_address _Vendor.Entry_ID _Vendor.Software_ID CCPN . . 30232 2 stop_ loop_ _Task.Task _Task.Entry_ID _Task.Software_ID 'chemical shift assignment' 30232 2 'data analysis' 30232 2 stop_ save_ save_software_3 _Software.Sf_category software _Software.Sf_framecode software_3 _Software.Entry_ID 30232 _Software.ID 3 _Software.Type . _Software.Name TALOS _Software.Version . _Software.DOI . _Software.Details . loop_ _Vendor.Name _Vendor.Address _Vendor.Electronic_address _Vendor.Entry_ID _Vendor.Software_ID 'Cornilescu, Delaglio and Bax' . . 30232 3 stop_ loop_ _Task.Task _Task.Entry_ID _Task.Software_ID 'data analysis' 30232 3 stop_ save_ save_software_4 _Software.Sf_category software _Software.Sf_framecode software_4 _Software.Entry_ID 30232 _Software.ID 4 _Software.Type . _Software.Name TOPSPIN _Software.Version 3.5PL6 _Software.DOI . _Software.Details . loop_ _Vendor.Name _Vendor.Address _Vendor.Electronic_address _Vendor.Entry_ID _Vendor.Software_ID 'Bruker Biospin' . . 30232 4 stop_ loop_ _Task.Task _Task.Entry_ID _Task.Software_ID collection 30232 4 stop_ save_ ######################### # Experimental detail # ######################### ################################## # NMR Spectrometer definitions # ################################## save_NMR_spectrometer_1 _NMR_spectrometer.Sf_category NMR_spectrometer _NMR_spectrometer.Sf_framecode NMR_spectrometer_1 _NMR_spectrometer.Entry_ID 30232 _NMR_spectrometer.ID 1 _NMR_spectrometer.Details . _NMR_spectrometer.Manufacturer Bruker _NMR_spectrometer.Model Avance _NMR_spectrometer.Serial_number . _NMR_spectrometer.Field_strength 600 save_ save_NMR_spectrometer_list _NMR_spectrometer_list.Sf_category NMR_spectrometer_list _NMR_spectrometer_list.Sf_framecode NMR_spectrometer_list _NMR_spectrometer_list.Entry_ID 30232 _NMR_spectrometer_list.ID 1 loop_ _NMR_spectrometer_view.ID _NMR_spectrometer_view.Name _NMR_spectrometer_view.Manufacturer _NMR_spectrometer_view.Model _NMR_spectrometer_view.Serial_number _NMR_spectrometer_view.Field_strength _NMR_spectrometer_view.Details _NMR_spectrometer_view.Citation_ID _NMR_spectrometer_view.Citation_label _NMR_spectrometer_view.Entry_ID _NMR_spectrometer_view.NMR_spectrometer_list_ID 1 NMR_spectrometer_1 Bruker Avance . 600 . . . 30232 1 stop_ save_ ############################# # NMR applied experiments # ############################# save_experiment_list _Experiment_list.Sf_category experiment_list _Experiment_list.Sf_framecode experiment_list _Experiment_list.Entry_ID 30232 _Experiment_list.ID 1 _Experiment_list.Details . loop_ _Experiment.ID _Experiment.Name _Experiment.Raw_data_flag _Experiment.NMR_spec_expt_ID _Experiment.NMR_spec_expt_label _Experiment.MS_expt_ID _Experiment.MS_expt_label _Experiment.SAXS_expt_ID _Experiment.SAXS_expt_label _Experiment.FRET_expt_ID _Experiment.FRET_expt_label _Experiment.EMR_expt_ID _Experiment.EMR_expt_label _Experiment.Sample_ID _Experiment.Sample_label _Experiment.Sample_state _Experiment.Sample_volume _Experiment.Sample_volume_units _Experiment.Sample_condition_list_ID _Experiment.Sample_condition_list_label _Experiment.Sample_spinning_rate _Experiment.Sample_angle _Experiment.NMR_tube_type _Experiment.NMR_spectrometer_ID _Experiment.NMR_spectrometer_label _Experiment.NMR_spectrometer_probe_ID _Experiment.NMR_spectrometer_probe_label _Experiment.NMR_spectral_processing_ID _Experiment.NMR_spectral_processing_label _Experiment.Mass_spectrometer_ID _Experiment.Mass_spectrometer_label _Experiment.Xray_instrument_ID _Experiment.Xray_instrument_label _Experiment.Fluorescence_instrument_ID _Experiment.Fluorescence_instrument_label _Experiment.EMR_instrument_ID _Experiment.EMR_instrument_label _Experiment.Chromatographic_system_ID _Experiment.Chromatographic_system_label _Experiment.Chromatographic_column_ID _Experiment.Chromatographic_column_label _Experiment.Entry_ID _Experiment.Experiment_list_ID 1 '2D 1H-13C HSQC' no . . . . . . . . . . 1 $sample_1 anisotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . 30232 1 2 '2D 1H-1H TOCSY' no . . . . . . . . . . 1 $sample_1 anisotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . 30232 1 3 '2D 1H-1H NOESY' no . . . . . . . . . . 1 $sample_1 anisotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . 30232 1 4 '2D 1H-1H COSY' no . . . . . . . . . . 1 $sample_1 anisotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . 30232 1 stop_ save_ #################### # NMR parameters # #################### ############################## # Assigned chemical shifts # ############################## ################################ # Chemical shift referencing # ################################ save_chem_shift_reference_1 _Chem_shift_reference.Sf_category chem_shift_reference _Chem_shift_reference.Sf_framecode chem_shift_reference_1 _Chem_shift_reference.Entry_ID 30232 _Chem_shift_reference.ID 1 _Chem_shift_reference.Details . loop_ _Chem_shift_ref.Atom_type _Chem_shift_ref.Atom_isotope_number _Chem_shift_ref.Mol_common_name _Chem_shift_ref.Atom_group _Chem_shift_ref.Concentration_val _Chem_shift_ref.Concentration_units _Chem_shift_ref.Solvent _Chem_shift_ref.Rank _Chem_shift_ref.Chem_shift_units _Chem_shift_ref.Chem_shift_val _Chem_shift_ref.Ref_method _Chem_shift_ref.Ref_type _Chem_shift_ref.Indirect_shift_ratio _Chem_shift_ref.External_ref_loc _Chem_shift_ref.External_ref_sample_geometry _Chem_shift_ref.External_ref_axis _Chem_shift_ref.Ref_correction_type _Chem_shift_ref.Correction_val _Chem_shift_ref.Entry_ID _Chem_shift_ref.Chem_shift_reference_ID C 13 DSS 'methyl protons' . . . . ppm 0.000 internal indirect 0.25144953 . . . . . 30232 1 H 1 DSS 'methyl protons' . . . . ppm 0.000 internal direct 1.0 . . . . . 30232 1 stop_ save_ ################################### # Assigned chemical shift lists # ################################### ################################################################### # Chemical Shift Ambiguity Index Value Definitions # # # # The values other than 1 are used for those atoms with different # # chemical shifts that cannot be assigned to stereospecific atoms # # or to specific residues or chains. # # # # Index Value Definition # # # # 1 Unique (including isolated methyl protons, # # geminal atoms, and geminal methyl # # groups with identical chemical shifts) # # (e.g. ILE HD11, HD12, HD13 protons) # # 2 Ambiguity of geminal atoms or geminal methyl # # proton groups (e.g. ASP HB2 and HB3 # # protons, LEU CD1 and CD2 carbons, or # # LEU HD11, HD12, HD13 and HD21, HD22, # # HD23 methyl protons) # # 3 Aromatic atoms on opposite sides of # # symmetrical rings (e.g. TYR HE1 and HE2 # # protons) # # 4 Intraresidue ambiguities (e.g. LYS HG and # # HD protons or TRP HZ2 and HZ3 protons) # # 5 Interresidue ambiguities (LYS 12 vs. LYS 27) # # 6 Intermolecular ambiguities (e.g. ASP 31 CA # # in monomer 1 and ASP 31 CA in monomer 2 # # of an asymmetrical homodimer, duplex # # DNA assignments, or other assignments # # that may apply to atoms in one or more # # molecule in the molecular assembly) # # 9 Ambiguous, specific ambiguity not defined # # # ################################################################### save_assigned_chemical_shifts_1 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode assigned_chemical_shifts_1 _Assigned_chem_shift_list.Entry_ID 30232 _Assigned_chem_shift_list.ID 1 _Assigned_chem_shift_list.Sample_condition_list_ID 1 _Assigned_chem_shift_list.Sample_condition_list_label $sample_conditions_1 _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chem_shift_reference_1 _Assigned_chem_shift_list.Chem_shift_1H_err . _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err . _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID 1 '2D 1H-13C HSQC' . . . 30232 1 2 '2D 1H-1H TOCSY' . . . 30232 1 3 '2D 1H-1H NOESY' . . . 30232 1 4 '2D 1H-1H COSY' . . . 30232 1 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Ambiguity_set_ID _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 1 3 3 ASP H H 1 7.129 0.001 . . . . . . A 3 ASP H . 30232 1 2 . 1 1 3 3 ASP HA H 1 5.029 0.000 . . . . . . A 3 ASP HA . 30232 1 3 . 1 1 3 3 ASP HB2 H 1 2.850 0.001 . . . . . . A 3 ASP HB2 . 30232 1 4 . 1 1 3 3 ASP HB3 H 1 2.605 0.000 . . . . . . A 3 ASP HB3 . 30232 1 5 . 1 1 3 3 ASP CB C 13 40.241 0.000 . . . . . . A 3 ASP CB . 30232 1 6 . 1 1 4 4 PRO HA H 1 4.415 0.000 . . . . . . A 4 PRO HA . 30232 1 7 . 1 1 4 4 PRO HB2 H 1 2.242 0.003 . . . . . . A 4 PRO HB2 . 30232 1 8 . 1 1 4 4 PRO HB3 H 1 1.931 0.000 . . . . . . A 4 PRO HB3 . 30232 1 9 . 1 1 4 4 PRO HG2 H 1 2.016 0.000 . . . . . . A 4 PRO HG2 . 30232 1 10 . 1 1 4 4 PRO HG3 H 1 2.016 0.000 . . . . . . A 4 PRO HG3 . 30232 1 11 . 1 1 4 4 PRO HD2 H 1 3.885 0.005 . . . . . . A 4 PRO HD2 . 30232 1 12 . 1 1 4 4 PRO HD3 H 1 3.885 0.005 . . . . . . A 4 PRO HD3 . 30232 1 13 . 1 1 4 4 PRO CD C 13 48.287 0.000 . . . . . . A 4 PRO CD . 30232 1 14 . 1 1 5 5 VAL H H 1 7.491 0.000 . . . . . . A 5 VAL H . 30232 1 15 . 1 1 5 5 VAL HA H 1 3.872 0.002 . . . . . . A 5 VAL HA . 30232 1 16 . 1 1 5 5 VAL HB H 1 1.875 0.008 . . . . . . A 5 VAL HB . 30232 1 17 . 1 1 5 5 VAL HG11 H 1 0.619 0.001 . . . . . . A 5 VAL HG11 . 30232 1 18 . 1 1 5 5 VAL HG12 H 1 0.619 0.001 . . . . . . A 5 VAL HG12 . 30232 1 19 . 1 1 5 5 VAL HG13 H 1 0.619 0.001 . . . . . . A 5 VAL HG13 . 30232 1 20 . 1 1 5 5 VAL HG21 H 1 0.764 0.000 . . . . . . A 5 VAL HG21 . 30232 1 21 . 1 1 5 5 VAL HG22 H 1 0.764 0.000 . . . . . . A 5 VAL HG22 . 30232 1 22 . 1 1 5 5 VAL HG23 H 1 0.764 0.000 . . . . . . A 5 VAL HG23 . 30232 1 23 . 1 1 5 5 VAL CA C 13 60.731 0.000 . . . . . . A 5 VAL CA . 30232 1 24 . 1 1 5 5 VAL CB C 13 29.282 0.000 . . . . . . A 5 VAL CB . 30232 1 25 . 1 1 5 5 VAL CG1 C 13 18.215 0.012 . . . . . . A 5 VAL CG1 . 30232 1 26 . 1 1 5 5 VAL CG2 C 13 18.215 0.012 . . . . . . A 5 VAL CG2 . 30232 1 27 . 1 1 6 6 TYR H H 1 7.649 0.001 . . . . . . A 6 TYR H . 30232 1 28 . 1 1 6 6 TYR HA H 1 4.629 0.011 . . . . . . A 6 TYR HA . 30232 1 29 . 1 1 6 6 TYR HB2 H 1 2.713 0.001 . . . . . . A 6 TYR HB2 . 30232 1 30 . 1 1 6 6 TYR HB3 H 1 3.071 0.000 . . . . . . A 6 TYR HB3 . 30232 1 31 . 1 1 6 6 TYR HD1 H 1 7.052 0.000 . . . . . . A 6 TYR HD1 . 30232 1 32 . 1 1 6 6 TYR HD2 H 1 7.052 0.000 . . . . . . A 6 TYR HD2 . 30232 1 33 . 1 1 6 6 TYR HE1 H 1 6.821 0.000 . . . . . . A 6 TYR HE1 . 30232 1 34 . 1 1 6 6 TYR HE2 H 1 6.821 0.000 . . . . . . A 6 TYR HE2 . 30232 1 35 . 1 1 6 6 TYR CA C 13 55.803 0.000 . . . . . . A 6 TYR CA . 30232 1 36 . 1 1 6 6 TYR CB C 13 36.928 0.000 . . . . . . A 6 TYR CB . 30232 1 37 . 1 1 7 7 THR H H 1 8.200 0.000 . . . . . . A 7 THR H . 30232 1 38 . 1 1 7 7 THR HA H 1 4.411 0.002 . . . . . . A 7 THR HA . 30232 1 39 . 1 1 7 7 THR HB H 1 4.083 0.000 . . . . . . A 7 THR HB . 30232 1 40 . 1 1 7 7 THR HG21 H 1 1.162 0.002 . . . . . . A 7 THR HG21 . 30232 1 41 . 1 1 7 7 THR HG22 H 1 1.162 0.002 . . . . . . A 7 THR HG22 . 30232 1 42 . 1 1 7 7 THR HG23 H 1 1.162 0.002 . . . . . . A 7 THR HG23 . 30232 1 43 . 1 1 7 7 THR CA C 13 61.320 0.000 . . . . . . A 7 THR CA . 30232 1 44 . 1 1 7 7 THR CB C 13 67.688 0.000 . . . . . . A 7 THR CB . 30232 1 45 . 1 1 7 7 THR CG2 C 13 18.793 0.000 . . . . . . A 7 THR CG2 . 30232 1 46 . 1 1 8 8 CYS H H 1 8.352 0.000 . . . . . . A 8 CYS H . 30232 1 47 . 1 1 8 8 CYS HA H 1 5.075 0.000 . . . . . . A 8 CYS HA . 30232 1 48 . 1 1 8 8 CYS HB2 H 1 3.258 0.000 . . . . . . A 8 CYS HB2 . 30232 1 49 . 1 1 8 8 CYS HB3 H 1 2.618 0.000 . . . . . . A 8 CYS HB3 . 30232 1 50 . 1 1 9 9 ARG H H 1 8.492 0.001 . . . . . . A 9 ARG H . 30232 1 51 . 1 1 9 9 ARG HA H 1 4.531 0.003 . . . . . . A 9 ARG HA . 30232 1 52 . 1 1 9 9 ARG HB2 H 1 1.712 0.004 . . . . . . A 9 ARG HB2 . 30232 1 53 . 1 1 9 9 ARG HB3 H 1 1.895 0.000 . . . . . . A 9 ARG HB3 . 30232 1 54 . 1 1 9 9 ARG HG2 H 1 1.587 0.000 . . . . . . A 9 ARG HG2 . 30232 1 55 . 1 1 9 9 ARG HG3 H 1 1.587 0.000 . . . . . . A 9 ARG HG3 . 30232 1 56 . 1 1 9 9 ARG HD2 H 1 3.205 0.001 . . . . . . A 9 ARG HD2 . 30232 1 57 . 1 1 9 9 ARG HD3 H 1 3.205 0.001 . . . . . . A 9 ARG HD3 . 30232 1 58 . 1 1 9 9 ARG HE H 1 7.242 0.000 . . . . . . A 9 ARG HE . 30232 1 59 . 1 1 9 9 ARG CA C 13 52.324 0.000 . . . . . . A 9 ARG CA . 30232 1 60 . 1 1 9 9 ARG CG C 13 24.617 0.000 . . . . . . A 9 ARG CG . 30232 1 61 . 1 1 10 10 PRO HA H 1 4.359 0.001 . . . . . . A 10 PRO HA . 30232 1 62 . 1 1 10 10 PRO HB2 H 1 2.340 0.001 . . . . . . A 10 PRO HB2 . 30232 1 63 . 1 1 10 10 PRO HB3 H 1 1.875 0.002 . . . . . . A 10 PRO HB3 . 30232 1 64 . 1 1 10 10 PRO HG2 H 1 2.157 0.001 . . . . . . A 10 PRO HG2 . 30232 1 65 . 1 1 10 10 PRO HG3 H 1 2.035 0.003 . . . . . . A 10 PRO HG3 . 30232 1 66 . 1 1 10 10 PRO HD2 H 1 3.587 0.000 . . . . . . A 10 PRO HD2 . 30232 1 67 . 1 1 10 10 PRO HD3 H 1 3.884 0.003 . . . . . . A 10 PRO HD3 . 30232 1 68 . 1 1 10 10 PRO CA C 13 61.823 0.000 . . . . . . A 10 PRO CA . 30232 1 69 . 1 1 10 10 PRO CD C 13 47.880 0.005 . . . . . . A 10 PRO CD . 30232 1 70 . 1 1 11 11 GLY H H 1 8.897 0.000 . . . . . . A 11 GLY H . 30232 1 71 . 1 1 11 11 GLY HA2 H 1 4.320 0.001 . . . . . . A 11 GLY HA2 . 30232 1 72 . 1 1 11 11 GLY HA3 H 1 3.683 0.001 . . . . . . A 11 GLY HA3 . 30232 1 73 . 1 1 11 11 GLY CA C 13 42.316 0.000 . . . . . . A 11 GLY CA . 30232 1 74 . 1 1 12 12 GLN H H 1 8.093 0.001 . . . . . . A 12 GLN H . 30232 1 75 . 1 1 12 12 GLN HA H 1 4.813 0.000 . . . . . . A 12 GLN HA . 30232 1 76 . 1 1 12 12 GLN HB2 H 1 2.338 0.006 . . . . . . A 12 GLN HB2 . 30232 1 77 . 1 1 12 12 GLN HB3 H 1 2.262 0.003 . . . . . . A 12 GLN HB3 . 30232 1 78 . 1 1 12 12 GLN HG2 H 1 2.852 0.000 . . . . . . A 12 GLN HG2 . 30232 1 79 . 1 1 12 12 GLN HG3 H 1 3.039 0.000 . . . . . . A 12 GLN HG3 . 30232 1 80 . 1 1 12 12 GLN HE21 H 1 7.682 0.000 . . . . . . A 12 GLN HE21 . 30232 1 81 . 1 1 12 12 GLN HE22 H 1 6.747 0.000 . . . . . . A 12 GLN HE22 . 30232 1 82 . 1 1 12 12 GLN CB C 13 29.091 0.000 . . . . . . A 12 GLN CB . 30232 1 83 . 1 1 12 12 GLN CG C 13 31.765 0.000 . . . . . . A 12 GLN CG . 30232 1 84 . 1 1 13 13 THR H H 1 8.977 0.001 . . . . . . A 13 THR H . 30232 1 85 . 1 1 13 13 THR HA H 1 4.589 0.002 . . . . . . A 13 THR HA . 30232 1 86 . 1 1 13 13 THR HB H 1 4.054 0.001 . . . . . . A 13 THR HB . 30232 1 87 . 1 1 13 13 THR HG21 H 1 1.225 0.002 . . . . . . A 13 THR HG21 . 30232 1 88 . 1 1 13 13 THR HG22 H 1 1.225 0.002 . . . . . . A 13 THR HG22 . 30232 1 89 . 1 1 13 13 THR HG23 H 1 1.225 0.002 . . . . . . A 13 THR HG23 . 30232 1 90 . 1 1 13 13 THR CA C 13 57.738 0.000 . . . . . . A 13 THR CA . 30232 1 91 . 1 1 13 13 THR CB C 13 68.201 0.000 . . . . . . A 13 THR CB . 30232 1 92 . 1 1 13 13 THR CG2 C 13 18.733 0.000 . . . . . . A 13 THR CG2 . 30232 1 93 . 1 1 14 14 CYS H H 1 8.879 0.000 . . . . . . A 14 CYS H . 30232 1 94 . 1 1 14 14 CYS HA H 1 5.234 0.002 . . . . . . A 14 CYS HA . 30232 1 95 . 1 1 14 14 CYS HB2 H 1 3.337 0.000 . . . . . . A 14 CYS HB2 . 30232 1 96 . 1 1 14 14 CYS HB3 H 1 3.172 0.000 . . . . . . A 14 CYS HB3 . 30232 1 97 . 1 1 14 14 CYS CA C 13 53.952 0.000 . . . . . . A 14 CYS CA . 30232 1 98 . 1 1 15 15 CYS H H 1 8.897 0.000 . . . . . . A 15 CYS H . 30232 1 99 . 1 1 15 15 CYS HA H 1 5.014 0.000 . . . . . . A 15 CYS HA . 30232 1 100 . 1 1 15 15 CYS HB2 H 1 3.086 0.000 . . . . . . A 15 CYS HB2 . 30232 1 101 . 1 1 15 15 CYS HB3 H 1 3.210 0.000 . . . . . . A 15 CYS HB3 . 30232 1 102 . 1 1 16 16 ARG H H 1 8.905 0.001 . . . . . . A 16 ARG H . 30232 1 103 . 1 1 16 16 ARG HA H 1 3.961 0.000 . . . . . . A 16 ARG HA . 30232 1 104 . 1 1 16 16 ARG HB2 H 1 1.488 0.002 . . . . . . A 16 ARG HB2 . 30232 1 105 . 1 1 16 16 ARG HB3 H 1 1.719 0.000 . . . . . . A 16 ARG HB3 . 30232 1 106 . 1 1 16 16 ARG HG2 H 1 1.211 0.004 . . . . . . A 16 ARG HG2 . 30232 1 107 . 1 1 16 16 ARG HG3 H 1 1.404 0.001 . . . . . . A 16 ARG HG3 . 30232 1 108 . 1 1 16 16 ARG HD2 H 1 2.977 0.002 . . . . . . A 16 ARG HD2 . 30232 1 109 . 1 1 16 16 ARG HD3 H 1 2.977 0.002 . . . . . . A 16 ARG HD3 . 30232 1 110 . 1 1 16 16 ARG CG C 13 24.586 0.037 . . . . . . A 16 ARG CG . 30232 1 111 . 1 1 16 16 ARG CD C 13 40.634 0.000 . . . . . . A 16 ARG CD . 30232 1 112 . 1 1 17 17 GLY H H 1 8.008 0.001 . . . . . . A 17 GLY H . 30232 1 113 . 1 1 17 17 GLY HA2 H 1 4.363 0.003 . . . . . . A 17 GLY HA2 . 30232 1 114 . 1 1 17 17 GLY HA3 H 1 3.763 0.001 . . . . . . A 17 GLY HA3 . 30232 1 115 . 1 1 17 17 GLY CA C 13 41.815 0.004 . . . . . . A 17 GLY CA . 30232 1 116 . 1 1 18 18 LEU H H 1 8.083 0.001 . . . . . . A 18 LEU H . 30232 1 117 . 1 1 18 18 LEU HA H 1 3.981 0.004 . . . . . . A 18 LEU HA . 30232 1 118 . 1 1 18 18 LEU HG H 1 1.930 0.000 . . . . . . A 18 LEU HG . 30232 1 119 . 1 1 18 18 LEU HD11 H 1 0.849 0.000 . . . . . . A 18 LEU HD11 . 30232 1 120 . 1 1 18 18 LEU HD12 H 1 0.849 0.000 . . . . . . A 18 LEU HD12 . 30232 1 121 . 1 1 18 18 LEU HD13 H 1 0.849 0.000 . . . . . . A 18 LEU HD13 . 30232 1 122 . 1 1 18 18 LEU HD21 H 1 0.849 0.000 . . . . . . A 18 LEU HD21 . 30232 1 123 . 1 1 18 18 LEU HD22 H 1 0.849 0.000 . . . . . . A 18 LEU HD22 . 30232 1 124 . 1 1 18 18 LEU HD23 H 1 0.849 0.000 . . . . . . A 18 LEU HD23 . 30232 1 125 . 1 1 18 18 LEU CA C 13 54.614 0.000 . . . . . . A 18 LEU CA . 30232 1 126 . 1 1 18 18 LEU CD1 C 13 21.776 0.000 . . . . . . A 18 LEU CD1 . 30232 1 127 . 1 1 18 18 LEU CD2 C 13 21.776 0.000 . . . . . . A 18 LEU CD2 . 30232 1 128 . 1 1 19 19 HIS H H 1 8.649 0.001 . . . . . . A 19 HIS H . 30232 1 129 . 1 1 19 19 HIS HA H 1 4.873 0.000 . . . . . . A 19 HIS HA . 30232 1 130 . 1 1 19 19 HIS HB2 H 1 3.042 0.000 . . . . . . A 19 HIS HB2 . 30232 1 131 . 1 1 19 19 HIS HB3 H 1 3.421 0.000 . . . . . . A 19 HIS HB3 . 30232 1 132 . 1 1 19 19 HIS HD2 H 1 7.301 0.000 . . . . . . A 19 HIS HD2 . 30232 1 133 . 1 1 19 19 HIS HE1 H 1 8.631 0.000 . . . . . . A 19 HIS HE1 . 30232 1 134 . 1 1 19 19 HIS CB C 13 25.822 0.005 . . . . . . A 19 HIS CB . 30232 1 135 . 1 1 20 20 GLY H H 1 7.607 0.000 . . . . . . A 20 GLY H . 30232 1 136 . 1 1 20 20 GLY HA2 H 1 3.647 0.000 . . . . . . A 20 GLY HA2 . 30232 1 137 . 1 1 20 20 GLY HA3 H 1 4.271 0.001 . . . . . . A 20 GLY HA3 . 30232 1 138 . 1 1 20 20 GLY CA C 13 42.268 0.000 . . . . . . A 20 GLY CA . 30232 1 139 . 1 1 21 21 TYR H H 1 8.141 0.001 . . . . . . A 21 TYR H . 30232 1 140 . 1 1 21 21 TYR HA H 1 4.627 0.000 . . . . . . A 21 TYR HA . 30232 1 141 . 1 1 21 21 TYR HB2 H 1 2.766 0.000 . . . . . . A 21 TYR HB2 . 30232 1 142 . 1 1 21 21 TYR HB3 H 1 2.567 0.000 . . . . . . A 21 TYR HB3 . 30232 1 143 . 1 1 21 21 TYR HD1 H 1 6.950 0.000 . . . . . . A 21 TYR HD1 . 30232 1 144 . 1 1 21 21 TYR HD2 H 1 6.950 0.000 . . . . . . A 21 TYR HD2 . 30232 1 145 . 1 1 21 21 TYR HE1 H 1 6.799 0.000 . . . . . . A 21 TYR HE1 . 30232 1 146 . 1 1 21 21 TYR HE2 H 1 6.799 0.000 . . . . . . A 21 TYR HE2 . 30232 1 147 . 1 1 22 22 GLY H H 1 8.295 0.001 . . . . . . A 22 GLY H . 30232 1 148 . 1 1 22 22 GLY HA2 H 1 4.134 0.001 . . . . . . A 22 GLY HA2 . 30232 1 149 . 1 1 22 22 GLY HA3 H 1 3.798 0.000 . . . . . . A 22 GLY HA3 . 30232 1 150 . 1 1 22 22 GLY CA C 13 42.294 0.013 . . . . . . A 22 GLY CA . 30232 1 151 . 1 1 23 23 CYS H H 1 8.541 0.001 . . . . . . A 23 CYS H . 30232 1 152 . 1 1 23 23 CYS HA H 1 5.353 0.004 . . . . . . A 23 CYS HA . 30232 1 153 . 1 1 23 23 CYS HB2 H 1 2.847 0.000 . . . . . . A 23 CYS HB2 . 30232 1 154 . 1 1 23 23 CYS HB3 H 1 2.779 0.000 . . . . . . A 23 CYS HB3 . 30232 1 155 . 1 1 23 23 CYS CA C 13 52.179 0.000 . . . . . . A 23 CYS CA . 30232 1 156 . 1 1 24 24 CYS H H 1 9.446 0.000 . . . . . . A 24 CYS H . 30232 1 157 . 1 1 24 24 CYS HA H 1 4.757 0.000 . . . . . . A 24 CYS HA . 30232 1 158 . 1 1 24 24 CYS HB2 H 1 3.048 0.000 . . . . . . A 24 CYS HB2 . 30232 1 159 . 1 1 24 24 CYS HB3 H 1 3.048 0.000 . . . . . . A 24 CYS HB3 . 30232 1 stop_ save_ ######################### # Spectral peak lists # ######################### save_spectral_peak_list_1 _Spectral_peak_list.Sf_category spectral_peak_list _Spectral_peak_list.Sf_framecode spectral_peak_list_1 _Spectral_peak_list.Entry_ID 30232 _Spectral_peak_list.ID 1 _Spectral_peak_list.Sample_ID 1 _Spectral_peak_list.Sample_label $sample_1 _Spectral_peak_list.Sample_condition_list_ID 1 _Spectral_peak_list.Sample_condition_list_label $sample_conditions_1 _Spectral_peak_list.Experiment_ID 1 _Spectral_peak_list.Experiment_name '2D 1H-13C HSQC' _Spectral_peak_list.Experiment_class . _Spectral_peak_list.Experiment_type . _Spectral_peak_list.Number_of_spectral_dimensions 2 _Spectral_peak_list.Chemical_shift_list . _Spectral_peak_list.Assigned_chem_shift_list_ID . _Spectral_peak_list.Assigned_chem_shift_list_label . _Spectral_peak_list.Details . _Spectral_peak_list.Text_data_format text _Spectral_peak_list.Text_data . loop_ _Spectral_dim.ID _Spectral_dim.Axis_code _Spectral_dim.Spectrometer_frequency _Spectral_dim.Atom_type _Spectral_dim.Atom_isotope_number _Spectral_dim.Spectral_region _Spectral_dim.Magnetization_linkage_ID _Spectral_dim.Under_sampling_type _Spectral_dim.Sweep_width _Spectral_dim.Sweep_width_units _Spectral_dim.Value_first_point _Spectral_dim.Absolute_peak_positions _Spectral_dim.Acquisition _Spectral_dim.Center_frequency_offset _Spectral_dim.Encoding_code _Spectral_dim.Encoded_reduced_dimension_ID _Spectral_dim.Entry_ID _Spectral_dim.Spectral_peak_list_ID 1 . . H 1 H . aliased 11.98 ppm . . . 4.88 . . 30232 1 2 . . C 13 C . aliased 150.6 ppm . . . 75.19 . . 30232 1 stop_ loop_ _Peak.ID _Peak.Figure_of_merit _Peak.Restraint _Peak.Details _Peak.Entry_ID _Peak.Spectral_peak_list_ID 1 . . . 30232 1 2 . . . 30232 1 3 . . . 30232 1 4 . . . 30232 1 5 . . . 30232 1 6 . . . 30232 1 7 . . . 30232 1 8 . . . 30232 1 9 . . . 30232 1 10 . . . 30232 1 11 . . . 30232 1 12 . . . 30232 1 13 . . . 30232 1 14 . . . 30232 1 15 . . . 30232 1 16 . . . 30232 1 17 . . . 30232 1 18 . . . 30232 1 19 . . . 30232 1 20 . . . 30232 1 21 . . . 30232 1 22 . . . 30232 1 23 . . . 30232 1 24 . . . 30232 1 25 . . . 30232 1 26 . . . 30232 1 27 . . . 30232 1 28 . . . 30232 1 29 . . . 30232 1 30 . . . 30232 1 31 . . . 30232 1 32 . . . 30232 1 33 . . . 30232 1 34 . . . 30232 1 35 . . . 30232 1 36 . . . 30232 1 37 . . . 30232 1 38 . . . 30232 1 39 . . . 30232 1 40 . . . 30232 1 41 . . . 30232 1 42 . . . 30232 1 43 . . . 30232 1 44 . . . 30232 1 45 . . . 30232 1 46 . . . 30232 1 47 . . . 30232 1 48 . . . 30232 1 49 . . . 30232 1 50 . . . 30232 1 51 . . . 30232 1 52 . . . 30232 1 53 . . . 30232 1 54 . . . 30232 1 55 . . . 30232 1 56 . . . 30232 1 57 . . . 30232 1 58 . . . 30232 1 59 . . . 30232 1 60 . . . 30232 1 61 . . . 30232 1 62 . . . 30232 1 63 . . . 30232 1 64 . . . 30232 1 65 . . . 30232 1 66 . . . 30232 1 67 . . . 30232 1 68 . . . 30232 1 69 . . . 30232 1 70 . . . 30232 1 71 . . . 30232 1 72 . . . 30232 1 73 . . . 30232 1 74 . . . 30232 1 75 . . . 30232 1 76 . . . 30232 1 77 . . . 30232 1 78 . . . 30232 1 79 . . . 30232 1 80 . . . 30232 1 81 . . . 30232 1 82 . . . 30232 1 83 . . . 30232 1 84 . . . 30232 1 85 . . . 30232 1 86 . . . 30232 1 87 . . . 30232 1 88 . . . 30232 1 89 . . . 30232 1 90 . . . 30232 1 91 . . . 30232 1 92 . . . 30232 1 93 . . . 30232 1 94 . . . 30232 1 95 . . . 30232 1 96 . . . 30232 1 97 . . . 30232 1 98 . . . 30232 1 99 . . . 30232 1 100 . . . 30232 1 101 . . . 30232 1 102 . . . 30232 1 103 . . . 30232 1 104 . . . 30232 1 105 . . . 30232 1 106 . . . 30232 1 107 . . . 30232 1 108 . . . 30232 1 109 . . . 30232 1 110 . . . 30232 1 111 . . . 30232 1 112 . . . 30232 1 113 . . . 30232 1 114 . . . 30232 1 115 . . . 30232 1 116 . . . 30232 1 117 . . . 30232 1 118 . . . 30232 1 119 . . . 30232 1 120 . . . 30232 1 121 . . . 30232 1 122 . . . 30232 1 123 . . . 30232 1 124 . . . 30232 1 125 . . . 30232 1 126 . . . 30232 1 127 . . . 30232 1 128 . . . 30232 1 129 . . . 30232 1 130 . . . 30232 1 131 . . . 30232 1 132 . . . 30232 1 133 . . . 30232 1 134 . . . 30232 1 135 . . . 30232 1 136 . . . 30232 1 137 . . . 30232 1 138 . . . 30232 1 139 . . . 30232 1 140 . . . 30232 1 141 . . . 30232 1 142 . . . 30232 1 143 . . . 30232 1 144 . . . 30232 1 145 . . . 30232 1 146 . . . 30232 1 147 . . . 30232 1 148 . . . 30232 1 149 . . . 30232 1 150 . . . 30232 1 151 . . . 30232 1 152 . . . 30232 1 153 . . . 30232 1 154 . . . 30232 1 155 . . . 30232 1 156 . . . 30232 1 157 . . . 30232 1 158 . . . 30232 1 159 . . . 30232 1 160 . . . 30232 1 161 . . . 30232 1 162 . . . 30232 1 163 . . . 30232 1 164 . . . 30232 1 165 . . . 30232 1 166 . . . 30232 1 167 . . . 30232 1 168 . . . 30232 1 169 . . . 30232 1 170 . . . 30232 1 171 . . . 30232 1 172 . . . 30232 1 173 . . . 30232 1 174 . . . 30232 1 175 . . . 30232 1 176 . . . 30232 1 177 . . . 30232 1 178 . . . 30232 1 179 . . . 30232 1 180 . . . 30232 1 181 . . . 30232 1 182 . . . 30232 1 183 . . . 30232 1 184 . . . 30232 1 185 . . . 30232 1 186 . . . 30232 1 187 . . . 30232 1 188 . . . 30232 1 189 . . . 30232 1 190 . . . 30232 1 191 . . . 30232 1 192 . . . 30232 1 193 . . . 30232 1 194 . . . 30232 1 195 . . . 30232 1 196 . . . 30232 1 197 . . . 30232 1 198 . . . 30232 1 199 . . . 30232 1 200 . . . 30232 1 201 . . . 30232 1 202 . . . 30232 1 203 . . . 30232 1 204 . . . 30232 1 205 . . . 30232 1 206 . . . 30232 1 207 . . . 30232 1 208 . . . 30232 1 209 . . . 30232 1 210 . . . 30232 1 211 . . . 30232 1 212 . . . 30232 1 213 . . . 30232 1 214 . . . 30232 1 215 . . . 30232 1 216 . . . 30232 1 217 . . . 30232 1 218 . . . 30232 1 219 . . . 30232 1 220 . . . 30232 1 221 . . . 30232 1 222 . . . 30232 1 223 . . . 30232 1 224 . . . 30232 1 225 . . . 30232 1 226 . . . 30232 1 227 . . . 30232 1 228 . . . 30232 1 229 . . . 30232 1 230 . . . 30232 1 231 . . . 30232 1 232 . . . 30232 1 233 . . . 30232 1 234 . . . 30232 1 235 . . . 30232 1 236 . . . 30232 1 237 . . . 30232 1 238 . . . 30232 1 239 . . . 30232 1 240 . . . 30232 1 241 . . . 30232 1 stop_ loop_ _Peak_general_char.Peak_ID _Peak_general_char.Intensity_val _Peak_general_char.Intensity_val_err _Peak_general_char.Measurement_method _Peak_general_char.Entry_ID _Peak_general_char.Spectral_peak_list_ID 1 214200.0 . volume 30232 1 2 48530.0 . volume 30232 1 3 316500.0 . volume 30232 1 4 74160.0 . volume 30232 1 5 64830.0 . volume 30232 1 6 277200.0 . volume 30232 1 7 33020.0 . volume 30232 1 8 64170.0 . volume 30232 1 9 60690.0 . volume 30232 1 10 55920.0 . volume 30232 1 11 124200.0 . volume 30232 1 12 221300.0 . volume 30232 1 13 270500.0 . volume 30232 1 14 140300.0 . volume 30232 1 15 145700.0 . volume 30232 1 16 66050.0 . volume 30232 1 17 84370.0 . volume 30232 1 18 133600.0 . volume 30232 1 19 142500.0 . volume 30232 1 20 34530.0 . volume 30232 1 21 82190.0 . volume 30232 1 22 25340.0 . volume 30232 1 23 58680.0 . volume 30232 1 24 90430.0 . volume 30232 1 25 81110.0 . volume 30232 1 26 187400.0 . volume 30232 1 27 288200.0 . volume 30232 1 28 59320.0 . volume 30232 1 29 78460.0 . volume 30232 1 30 164300.0 . volume 30232 1 31 119300.0 . volume 30232 1 32 39850.0 . volume 30232 1 33 61110.0 . volume 30232 1 34 264200.0 . volume 30232 1 35 219800.0 . volume 30232 1 36 379800.0 . volume 30232 1 37 193400.0 . volume 30232 1 38 445600.0 . volume 30232 1 39 210700.0 . volume 30232 1 40 150000.0 . volume 30232 1 41 214800.0 . volume 30232 1 42 87910.0 . volume 30232 1 43 70360.0 . volume 30232 1 44 321300.0 . volume 30232 1 45 273700.0 . volume 30232 1 46 33020.0 . volume 30232 1 47 109600.0 . volume 30232 1 48 79020.0 . volume 30232 1 49 312500.0 . volume 30232 1 50 224200.0 . volume 30232 1 51 70730.0 . volume 30232 1 52 162400.0 . volume 30232 1 53 211900.0 . volume 30232 1 54 72760.0 . volume 30232 1 55 12330.0 . volume 30232 1 56 126400.0 . volume 30232 1 57 122700.0 . volume 30232 1 58 31530.0 . volume 30232 1 59 1989000.0 . volume 30232 1 60 390900.0 . volume 30232 1 61 478800.0 . volume 30232 1 62 107700.0 . volume 30232 1 63 356000.0 . volume 30232 1 64 534300.0 . volume 30232 1 65 222700.0 . volume 30232 1 66 59150.0 . volume 30232 1 67 64180.0 . volume 30232 1 68 42010.0 . volume 30232 1 69 74160.0 . volume 30232 1 70 39120.0 . volume 30232 1 71 144600.0 . volume 30232 1 72 50430.0 . volume 30232 1 73 43620.0 . volume 30232 1 74 57320.0 . volume 30232 1 75 463900.0 . volume 30232 1 76 565500.0 . volume 30232 1 77 137800.0 . volume 30232 1 78 235700.0 . volume 30232 1 79 108200.0 . volume 30232 1 80 167100.0 . volume 30232 1 81 91600.0 . volume 30232 1 82 72970.0 . volume 30232 1 83 37550.0 . volume 30232 1 84 151400.0 . volume 30232 1 85 20390.0 . volume 30232 1 86 185100.0 . volume 30232 1 87 256300.0 . volume 30232 1 88 614500.0 . volume 30232 1 89 112200.0 . volume 30232 1 90 89440.0 . volume 30232 1 91 135700.0 . volume 30232 1 92 240100.0 . volume 30232 1 93 87340.0 . volume 30232 1 94 90400.0 . volume 30232 1 95 177000.0 . volume 30232 1 96 135400.0 . volume 30232 1 97 50940.0 . volume 30232 1 98 151900.0 . volume 30232 1 99 186700.0 . volume 30232 1 100 2061000.0 . volume 30232 1 101 2537000.0 . volume 30232 1 102 46390.0 . volume 30232 1 103 16820.0 . volume 30232 1 104 38130.0 . volume 30232 1 105 36460.0 . volume 30232 1 106 88110.0 . volume 30232 1 107 17870.0 . volume 30232 1 108 73010.0 . volume 30232 1 109 860500.0 . volume 30232 1 110 1260000.0 . volume 30232 1 111 226200.0 . volume 30232 1 112 831800.0 . volume 30232 1 113 209600.0 . volume 30232 1 114 62180.0 . volume 30232 1 115 81610.0 . volume 30232 1 116 31230.0 . volume 30232 1 117 281600.0 . volume 30232 1 118 68160.0 . volume 30232 1 119 141100.0 . volume 30232 1 120 91140.0 . volume 30232 1 121 73950.0 . volume 30232 1 122 42320.0 . volume 30232 1 123 1201000.0 . volume 30232 1 124 493100.0 . volume 30232 1 125 95740.0 . volume 30232 1 126 40910.0 . volume 30232 1 127 65530.0 . volume 30232 1 128 76640.0 . volume 30232 1 129 69760.0 . volume 30232 1 130 94170.0 . volume 30232 1 131 105400.0 . volume 30232 1 132 403300.0 . volume 30232 1 133 83010.0 . volume 30232 1 134 71040.0 . volume 30232 1 135 141500.0 . volume 30232 1 136 356900.0 . volume 30232 1 137 148100.0 . volume 30232 1 138 92340.0 . volume 30232 1 139 33330.0 . volume 30232 1 140 67860.0 . volume 30232 1 141 109600.0 . volume 30232 1 142 31780.0 . volume 30232 1 143 25740.0 . volume 30232 1 144 114300.0 . volume 30232 1 145 289700.0 . volume 30232 1 146 197500.0 . volume 30232 1 147 422700.0 . volume 30232 1 148 251100.0 . volume 30232 1 149 413100.0 . volume 30232 1 150 128700.0 . volume 30232 1 151 26910.0 . volume 30232 1 152 47550.0 . volume 30232 1 153 39650.0 . volume 30232 1 154 29850.0 . volume 30232 1 155 301200.0 . volume 30232 1 156 63770.0 . volume 30232 1 157 35940.0 . volume 30232 1 158 84690.0 . volume 30232 1 159 55600.0 . volume 30232 1 160 77910.0 . volume 30232 1 161 79600.0 . volume 30232 1 162 404100.0 . volume 30232 1 163 611900.0 . volume 30232 1 164 928900.0 . volume 30232 1 165 273100.0 . volume 30232 1 166 142500.0 . volume 30232 1 167 120200.0 . volume 30232 1 168 61990.0 . volume 30232 1 169 119800.0 . volume 30232 1 170 112200.0 . volume 30232 1 171 71560.0 . volume 30232 1 172 49560.0 . volume 30232 1 173 27650.0 . volume 30232 1 174 19340.0 . volume 30232 1 175 133200.0 . volume 30232 1 176 634100.0 . volume 30232 1 177 160100.0 . volume 30232 1 178 106100.0 . volume 30232 1 179 129300.0 . volume 30232 1 180 407500.0 . volume 30232 1 181 128000.0 . volume 30232 1 182 43180.0 . volume 30232 1 183 145300.0 . volume 30232 1 184 85130.0 . volume 30232 1 185 23150.0 . volume 30232 1 186 242600.0 . volume 30232 1 187 707900.0 . volume 30232 1 188 171900.0 . volume 30232 1 189 307500.0 . volume 30232 1 190 331200.0 . volume 30232 1 191 87180.0 . volume 30232 1 192 38060.0 . volume 30232 1 193 1367000.0 . volume 30232 1 194 107700.0 . volume 30232 1 195 44370.0 . volume 30232 1 196 2012000.0 . volume 30232 1 197 935800.0 . volume 30232 1 198 317200.0 . volume 30232 1 199 94110.0 . volume 30232 1 200 55720.0 . volume 30232 1 201 180000.0 . volume 30232 1 202 42960.0 . volume 30232 1 203 138400.0 . volume 30232 1 204 172000.0 . volume 30232 1 205 379000.0 . volume 30232 1 206 155200.0 . volume 30232 1 207 567400.0 . volume 30232 1 208 134400.0 . volume 30232 1 209 305000.0 . volume 30232 1 210 205900.0 . volume 30232 1 211 152000.0 . volume 30232 1 212 48220.0 . volume 30232 1 213 63370.0 . volume 30232 1 214 71390.0 . volume 30232 1 215 74570.0 . volume 30232 1 216 76380.0 . volume 30232 1 217 110200.0 . volume 30232 1 218 42900.0 . volume 30232 1 219 31390.0 . volume 30232 1 220 25020.0 . volume 30232 1 221 73260.0 . volume 30232 1 222 54460.0 . volume 30232 1 223 77770.0 . volume 30232 1 224 -15740.0 . volume 30232 1 225 69980.0 . volume 30232 1 226 123600.0 . volume 30232 1 227 133400.0 . volume 30232 1 228 50370.0 . volume 30232 1 229 175100.0 . volume 30232 1 230 535000.0 . volume 30232 1 231 433800.0 . volume 30232 1 232 54750.0 . volume 30232 1 233 287400.0 . volume 30232 1 234 20980.0 . volume 30232 1 235 55010.0 . volume 30232 1 236 288100.0 . volume 30232 1 237 20530.0 . volume 30232 1 238 36880.0 . volume 30232 1 239 159700.0 . volume 30232 1 240 312500.0 . volume 30232 1 241 46090.0 . volume 30232 1 stop_ loop_ _Peak_char.Peak_ID _Peak_char.Spectral_dim_ID _Peak_char.Chem_shift_val _Peak_char.Chem_shift_val_err _Peak_char.Line_width_val _Peak_char.Line_width_val_err _Peak_char.Phase_val _Peak_char.Phase_val_err _Peak_char.Decay_rate_val _Peak_char.Decay_rate_val_err _Peak_char.Coupling_pattern _Peak_char.Bounding_box_upper_val _Peak_char.Bounding_box_lower_val _Peak_char.Bounding_box_range_val _Peak_char.Details _Peak_char.Derivation_method_ID _Peak_char.Entry_ID _Peak_char.Spectral_peak_list_ID 1 1 2.264 . . . . . . . . . . . . . 30232 1 1 2 8.093 . . . . . . . . . . . . . 30232 1 2 1 2.852 . . . . . . . . . . . . . 30232 1 2 2 8.092 . . . . . . . . . . . . . 30232 1 3 1 6.747 . . . . . . . . . . . . . 30232 1 3 2 7.682 . . . . . . . . . . . . . 30232 1 4 1 4.591 . . . . . . . . . . . . . 30232 1 4 2 8.977 . . . . . . . . . . . . . 30232 1 5 1 1.227 . . . . . . . . . . . . . 30232 1 5 2 8.978 . . . . . . . . . . . . . 30232 1 6 1 3.337 . . . . . . . . . . . . . 30232 1 6 2 8.88 . . . . . . . . . . . . . 30232 1 7 1 4.36 . . . . . . . . . . . . . 30232 1 7 2 8.008 . . . . . . . . . . . . . 30232 1 8 1 4.413 . . . . . . . . . . . . . 30232 1 8 2 8.2 . . . . . . . . . . . . . 30232 1 9 1 1.164 . . . . . . . . . . . . . 30232 1 9 2 8.2 . . . . . . . . . . . . . 30232 1 10 1 3.258 . . . . . . . . . . . . . 30232 1 10 2 8.352 . . . . . . . . . . . . . 30232 1 11 1 2.618 . . . . . . . . . . . . . 30232 1 11 2 8.352 . . . . . . . . . . . . . 30232 1 12 1 4.534 . . . . . . . . . . . . . 30232 1 12 2 8.494 . . . . . . . . . . . . . 30232 1 13 1 1.587 . . . . . . . . . . . . . 30232 1 13 2 8.492 . . . . . . . . . . . . . 30232 1 14 1 1.895 . . . . . . . . . . . . . 30232 1 14 2 8.492 . . . . . . . . . . . . . 30232 1 15 1 2.712 . . . . . . . . . . . . . 30232 1 15 2 7.65 . . . . . . . . . . . . . 30232 1 16 1 3.071 . . . . . . . . . . . . . 30232 1 16 2 7.648 . . . . . . . . . . . . . 30232 1 17 1 4.64 . . . . . . . . . . . . . 30232 1 17 2 7.649 . . . . . . . . . . . . . 30232 1 18 1 3.874 . . . . . . . . . . . . . 30232 1 18 2 7.49 . . . . . . . . . . . . . 30232 1 19 1 1.883 . . . . . . . . . . . . . 30232 1 19 2 7.491 . . . . . . . . . . . . . 30232 1 20 1 0.849 . . . . . . . . . . . . . 30232 1 20 2 8.082 . . . . . . . . . . . . . 30232 1 21 1 1.93 . . . . . . . . . . . . . 30232 1 21 2 8.084 . . . . . . . . . . . . . 30232 1 22 1 1.405 . . . . . . . . . . . . . 30232 1 22 2 8.905 . . . . . . . . . . . . . 30232 1 23 1 3.064 . . . . . . . . . . . . . 30232 1 23 2 9.392 . . . . . . . . . . . . . 30232 1 24 1 2.702 . . . . . . . . . . . . . 30232 1 24 2 8.579 . . . . . . . . . . . . . 30232 1 25 1 2.742 . . . . . . . . . . . . . 30232 1 25 2 8.505 . . . . . . . . . . . . . 30232 1 26 1 2.626 . . . . . . . . . . . . . 30232 1 26 2 8.498 . . . . . . . . . . . . . 30232 1 27 1 2.847 . . . . . . . . . . . . . 30232 1 27 2 8.542 . . . . . . . . . . . . . 30232 1 28 1 1.571 . . . . . . . . . . . . . 30232 1 28 2 8.867 . . . . . . . . . . . . . 30232 1 29 1 1.215 . . . . . . . . . . . . . 30232 1 29 2 8.906 . . . . . . . . . . . . . 30232 1 30 1 1.574 . . . . . . . . . . . . . 30232 1 30 2 8.423 . . . . . . . . . . . . . 30232 1 31 1 1.712 . . . . . . . . . . . . . 30232 1 31 2 8.422 . . . . . . . . . . . . . 30232 1 32 1 3.039 . . . . . . . . . . . . . 30232 1 32 2 8.093 . . . . . . . . . . . . . 30232 1 33 1 4.135 . . . . . . . . . . . . . 30232 1 33 2 8.867 . . . . . . . . . . . . . 30232 1 34 1 4.823 . . . . . . . . . . . . . 30232 1 34 2 8.978 . . . . . . . . . . . . . 30232 1 35 1 4.979 . . . . . . . . . . . . . 30232 1 35 2 8.566 . . . . . . . . . . . . . 30232 1 36 1 5.362 . . . . . . . . . . . . . 30232 1 36 2 9.446 . . . . . . . . . . . . . 30232 1 37 1 5.149 . . . . . . . . . . . . . 30232 1 37 2 8.417 . . . . . . . . . . . . . 30232 1 38 1 3.785 . . . . . . . . . . . . . 30232 1 38 2 8.542 . . . . . . . . . . . . . 30232 1 39 1 4.075 . . . . . . . . . . . . . 30232 1 39 2 8.024 . . . . . . . . . . . . . 30232 1 40 1 4.135 . . . . . . . . . . . . . 30232 1 40 2 8.12 . . . . . . . . . . . . . 30232 1 41 1 2.344 . . . . . . . . . . . . . 30232 1 41 2 8.093 . . . . . . . . . . . . . 30232 1 42 1 4.813 . . . . . . . . . . . . . 30232 1 42 2 8.094 . . . . . . . . . . . . . 30232 1 43 1 4.054 . . . . . . . . . . . . . 30232 1 43 2 8.977 . . . . . . . . . . . . . 30232 1 44 1 5.236 . . . . . . . . . . . . . 30232 1 44 2 8.879 . . . . . . . . . . . . . 30232 1 45 1 3.172 . . . . . . . . . . . . . 30232 1 45 2 8.879 . . . . . . . . . . . . . 30232 1 46 1 3.764 . . . . . . . . . . . . . 30232 1 46 2 8.009 . . . . . . . . . . . . . 30232 1 47 1 4.084 . . . . . . . . . . . . . 30232 1 47 2 8.2 . . . . . . . . . . . . . 30232 1 48 1 5.075 . . . . . . . . . . . . . 30232 1 48 2 8.353 . . . . . . . . . . . . . 30232 1 49 1 3.206 . . . . . . . . . . . . . 30232 1 49 2 8.493 . . . . . . . . . . . . . 30232 1 50 1 1.716 . . . . . . . . . . . . . 30232 1 50 2 8.491 . . . . . . . . . . . . . 30232 1 51 1 0.619 . . . . . . . . . . . . . 30232 1 51 2 7.491 . . . . . . . . . . . . . 30232 1 52 1 0.764 . . . . . . . . . . . . . 30232 1 52 2 7.491 . . . . . . . . . . . . . 30232 1 53 1 3.977 . . . . . . . . . . . . . 30232 1 53 2 8.082 . . . . . . . . . . . . . 30232 1 54 1 3.961 . . . . . . . . . . . . . 30232 1 54 2 8.905 . . . . . . . . . . . . . 30232 1 55 1 2.979 . . . . . . . . . . . . . 30232 1 55 2 8.906 . . . . . . . . . . . . . 30232 1 56 1 1.719 . . . . . . . . . . . . . 30232 1 56 2 8.905 . . . . . . . . . . . . . 30232 1 57 1 1.486 . . . . . . . . . . . . . 30232 1 57 2 8.904 . . . . . . . . . . . . . 30232 1 58 1 7.301 . . . . . . . . . . . . . 30232 1 58 2 8.631 . . . . . . . . . . . . . 30232 1 59 1 4.415 . . . . . . . . . . . . . 30232 1 59 2 3.888 . . . . . . . . . . . . . 30232 1 60 1 3.886 . . . . . . . . . . . . . 30232 1 60 2 2.158 . . . . . . . . . . . . . 30232 1 61 1 3.887 . . . . . . . . . . . . . 30232 1 61 2 2.032 . . . . . . . . . . . . . 30232 1 62 1 3.887 . . . . . . . . . . . . . 30232 1 62 2 1.93 . . . . . . . . . . . . . 30232 1 63 1 3.886 . . . . . . . . . . . . . 30232 1 63 2 1.878 . . . . . . . . . . . . . 30232 1 64 1 4.36 . . . . . . . . . . . . . 30232 1 64 2 2.341 . . . . . . . . . . . . . 30232 1 65 1 4.36 . . . . . . . . . . . . . 30232 1 65 2 1.873 . . . . . . . . . . . . . 30232 1 66 1 3.883 . . . . . . . . . . . . . 30232 1 66 2 2.339 . . . . . . . . . . . . . 30232 1 67 1 3.594 . . . . . . . . . . . . . 30232 1 67 2 2.342 . . . . . . . . . . . . . 30232 1 68 1 3.674 . . . . . . . . . . . . . 30232 1 68 2 2.332 . . . . . . . . . . . . . 30232 1 69 1 3.68 . . . . . . . . . . . . . 30232 1 69 2 2.037 . . . . . . . . . . . . . 30232 1 70 1 4.785 . . . . . . . . . . . . . 30232 1 70 2 8.637 . . . . . . . . . . . . . 30232 1 71 1 3.797 . . . . . . . . . . . . . 30232 1 71 2 8.294 . . . . . . . . . . . . . 30232 1 72 1 5.357 . . . . . . . . . . . . . 30232 1 72 2 8.54 . . . . . . . . . . . . . 30232 1 73 1 4.757 . . . . . . . . . . . . . 30232 1 73 2 9.446 . . . . . . . . . . . . . 30232 1 74 1 2.779 . . . . . . . . . . . . . 30232 1 74 2 8.542 . . . . . . . . . . . . . 30232 1 75 1 4.319 . . . . . . . . . . . . . 30232 1 75 2 8.897 . . . . . . . . . . . . . 30232 1 76 1 3.683 . . . . . . . . . . . . . 30232 1 76 2 8.896 . . . . . . . . . . . . . 30232 1 77 1 4.135 . . . . . . . . . . . . . 30232 1 77 2 8.296 . . . . . . . . . . . . . 30232 1 78 1 3.647 . . . . . . . . . . . . . 30232 1 78 2 7.606 . . . . . . . . . . . . . 30232 1 79 1 4.27 . . . . . . . . . . . . . 30232 1 79 2 7.607 . . . . . . . . . . . . . 30232 1 80 1 2.567 . . . . . . . . . . . . . 30232 1 80 2 8.142 . . . . . . . . . . . . . 30232 1 81 1 4.627 . . . . . . . . . . . . . 30232 1 81 2 8.141 . . . . . . . . . . . . . 30232 1 82 1 2.766 . . . . . . . . . . . . . 30232 1 82 2 8.141 . . . . . . . . . . . . . 30232 1 83 1 4.873 . . . . . . . . . . . . . 30232 1 83 2 8.647 . . . . . . . . . . . . . 30232 1 84 1 3.042 . . . . . . . . . . . . . 30232 1 84 2 8.65 . . . . . . . . . . . . . 30232 1 85 1 3.42 . . . . . . . . . . . . . 30232 1 85 2 8.649 . . . . . . . . . . . . . 30232 1 86 1 3.21 . . . . . . . . . . . . . 30232 1 86 2 8.897 . . . . . . . . . . . . . 30232 1 87 1 3.086 . . . . . . . . . . . . . 30232 1 87 2 8.897 . . . . . . . . . . . . . 30232 1 88 1 5.014 . . . . . . . . . . . . . 30232 1 88 2 8.897 . . . . . . . . . . . . . 30232 1 89 1 4.36 . . . . . . . . . . . . . 30232 1 89 2 3.882 . . . . . . . . . . . . . 30232 1 90 1 4.359 . . . . . . . . . . . . . 30232 1 90 2 3.587 . . . . . . . . . . . . . 30232 1 91 1 4.359 . . . . . . . . . . . . . 30232 1 91 2 2.037 . . . . . . . . . . . . . 30232 1 92 1 4.358 . . . . . . . . . . . . . 30232 1 92 2 2.157 . . . . . . . . . . . . . 30232 1 93 1 5.029 . . . . . . . . . . . . . 30232 1 93 2 7.13 . . . . . . . . . . . . . 30232 1 94 1 2.605 . . . . . . . . . . . . . 30232 1 94 2 7.13 . . . . . . . . . . . . . 30232 1 95 1 2.851 . . . . . . . . . . . . . 30232 1 95 2 7.128 . . . . . . . . . . . . . 30232 1 96 1 4.415 . . . . . . . . . . . . . 30232 1 96 2 2.245 . . . . . . . . . . . . . 30232 1 97 1 4.415 . . . . . . . . . . . . . 30232 1 97 2 1.931 . . . . . . . . . . . . . 30232 1 98 1 2.713 . . . . . . . . . . . . . 30232 1 98 2 7.052 . . . . . . . . . . . . . 30232 1 99 1 3.071 . . . . . . . . . . . . . 30232 1 99 2 7.054 . . . . . . . . . . . . . 30232 1 100 1 6.821 . . . . . . . . . . . . . 30232 1 100 2 7.052 . . . . . . . . . . . . . 30232 1 101 1 6.799 . . . . . . . . . . . . . 30232 1 101 2 6.95 . . . . . . . . . . . . . 30232 1 102 1 2.85 . . . . . . . . . . . . . 30232 1 102 2 9.444 . . . . . . . . . . . . . 30232 1 103 1 2.79 . . . . . . . . . . . . . 30232 1 103 2 9.444 . . . . . . . . . . . . . 30232 1 104 1 1.985 . . . . . . . . . . . . . 30232 1 104 2 9.445 . . . . . . . . . . . . . 30232 1 105 1 5.239 . . . . . . . . . . . . . 30232 1 105 2 9.444 . . . . . . . . . . . . . 30232 1 106 1 8.972 . . . . . . . . . . . . . 30232 1 106 2 9.444 . . . . . . . . . . . . . 30232 1 107 1 8.894 . . . . . . . . . . . . . 30232 1 107 2 9.444 . . . . . . . . . . . . . 30232 1 108 1 5.229 . . . . . . . . . . . . . 30232 1 108 2 5.354 . . . . . . . . . . . . . 30232 1 109 1 1.884 . . . . . . . . . . . . . 30232 1 109 2 1.579 . . . . . . . . . . . . . 30232 1 110 1 1.883 . . . . . . . . . . . . . 30232 1 110 2 1.73 . . . . . . . . . . . . . 30232 1 111 1 1.795 . . . . . . . . . . . . . 30232 1 111 2 1.633 . . . . . . . . . . . . . 30232 1 112 1 1.723 . . . . . . . . . . . . . 30232 1 112 2 1.492 . . . . . . . . . . . . . 30232 1 113 1 1.725 . . . . . . . . . . . . . 30232 1 113 2 1.41 . . . . . . . . . . . . . 30232 1 114 1 5.359 . . . . . . . . . . . . . 30232 1 114 2 8.895 . . . . . . . . . . . . . 30232 1 115 1 3.888 . . . . . . . . . . . . . 30232 1 115 2 2.24 . . . . . . . . . . . . . 30232 1 116 1 6.959 . . . . . . . . . . . . . 30232 1 116 2 8.894 . . . . . . . . . . . . . 30232 1 117 1 8.092 . . . . . . . . . . . . . 30232 1 117 2 8.898 . . . . . . . . . . . . . 30232 1 118 1 8.298 . . . . . . . . . . . . . 30232 1 118 2 8.894 . . . . . . . . . . . . . 30232 1 119 1 2.339 . . . . . . . . . . . . . 30232 1 119 2 8.896 . . . . . . . . . . . . . 30232 1 120 1 1.988 . . . . . . . . . . . . . 30232 1 120 2 8.895 . . . . . . . . . . . . . 30232 1 121 1 1.869 . . . . . . . . . . . . . 30232 1 121 2 8.896 . . . . . . . . . . . . . 30232 1 122 1 6.953 . . . . . . . . . . . . . 30232 1 122 2 8.293 . . . . . . . . . . . . . 30232 1 123 1 4.362 . . . . . . . . . . . . . 30232 1 123 2 8.898 . . . . . . . . . . . . . 30232 1 124 1 4.628 . . . . . . . . . . . . . 30232 1 124 2 8.297 . . . . . . . . . . . . . 30232 1 125 1 2.768 . . . . . . . . . . . . . 30232 1 125 2 8.296 . . . . . . . . . . . . . 30232 1 126 1 2.566 . . . . . . . . . . . . . 30232 1 126 2 8.296 . . . . . . . . . . . . . 30232 1 127 1 4.707 . . . . . . . . . . . . . 30232 1 127 2 7.133 . . . . . . . . . . . . . 30232 1 128 1 4.315 . . . . . . . . . . . . . 30232 1 128 2 7.13 . . . . . . . . . . . . . 30232 1 129 1 3.281 . . . . . . . . . . . . . 30232 1 129 2 7.131 . . . . . . . . . . . . . 30232 1 130 1 4.414 . . . . . . . . . . . . . 30232 1 130 2 7.49 . . . . . . . . . . . . . 30232 1 131 1 3.878 . . . . . . . . . . . . . 30232 1 131 2 7.65 . . . . . . . . . . . . . 30232 1 132 1 3.961 . . . . . . . . . . . . . 30232 1 132 2 8.008 . . . . . . . . . . . . . 30232 1 133 1 4.63 . . . . . . . . . . . . . 30232 1 133 2 8.009 . . . . . . . . . . . . . 30232 1 134 1 3.685 . . . . . . . . . . . . . 30232 1 134 2 8.093 . . . . . . . . . . . . . 30232 1 135 1 3.649 . . . . . . . . . . . . . 30232 1 135 2 8.143 . . . . . . . . . . . . . 30232 1 136 1 4.417 . . . . . . . . . . . . . 30232 1 136 2 8.352 . . . . . . . . . . . . . 30232 1 137 1 4.299 . . . . . . . . . . . . . 30232 1 137 2 8.353 . . . . . . . . . . . . . 30232 1 138 1 4.085 . . . . . . . . . . . . . 30232 1 138 2 8.353 . . . . . . . . . . . . . 30232 1 139 1 3.894 . . . . . . . . . . . . . 30232 1 139 2 7.131 . . . . . . . . . . . . . 30232 1 140 1 4.63 . . . . . . . . . . . . . 30232 1 140 2 6.95 . . . . . . . . . . . . . 30232 1 141 1 4.643 . . . . . . . . . . . . . 30232 1 141 2 7.052 . . . . . . . . . . . . . 30232 1 142 1 3.96 . . . . . . . . . . . . . 30232 1 142 2 6.949 . . . . . . . . . . . . . 30232 1 143 1 3.172 . . . . . . . . . . . . . 30232 1 143 2 6.949 . . . . . . . . . . . . . 30232 1 144 1 2.767 . . . . . . . . . . . . . 30232 1 144 2 6.95 . . . . . . . . . . . . . 30232 1 145 1 2.567 . . . . . . . . . . . . . 30232 1 145 2 6.95 . . . . . . . . . . . . . 30232 1 146 1 2.852 . . . . . . . . . . . . . 30232 1 146 2 7.052 . . . . . . . . . . . . . 30232 1 147 1 3.586 . . . . . . . . . . . . . 30232 1 147 2 2.157 . . . . . . . . . . . . . 30232 1 148 1 3.586 . . . . . . . . . . . . . 30232 1 148 2 2.031 . . . . . . . . . . . . . 30232 1 149 1 3.592 . . . . . . . . . . . . . 30232 1 149 2 1.887 . . . . . . . . . . . . . 30232 1 150 1 3.21 . . . . . . . . . . . . . 30232 1 150 2 1.889 . . . . . . . . . . . . . 30232 1 151 1 4.416 . . . . . . . . . . . . . 30232 1 151 2 7.645 . . . . . . . . . . . . . 30232 1 152 1 1.879 . . . . . . . . . . . . . 30232 1 152 2 7.648 . . . . . . . . . . . . . 30232 1 153 1 0.764 . . . . . . . . . . . . . 30232 1 153 2 7.648 . . . . . . . . . . . . . 30232 1 154 1 0.625 . . . . . . . . . . . . . 30232 1 154 2 7.648 . . . . . . . . . . . . . 30232 1 155 1 4.644 . . . . . . . . . . . . . 30232 1 155 2 8.201 . . . . . . . . . . . . . 30232 1 156 1 3.071 . . . . . . . . . . . . . 30232 1 156 2 8.2 . . . . . . . . . . . . . 30232 1 157 1 2.708 . . . . . . . . . . . . . 30232 1 157 2 8.199 . . . . . . . . . . . . . 30232 1 158 1 1.16 . . . . . . . . . . . . . 30232 1 158 2 8.354 . . . . . . . . . . . . . 30232 1 159 1 1.175 . . . . . . . . . . . . . 30232 1 159 2 8.49 . . . . . . . . . . . . . 30232 1 160 1 2.267 . . . . . . . . . . . . . 30232 1 160 2 8.492 . . . . . . . . . . . . . 30232 1 161 1 2.342 . . . . . . . . . . . . . 30232 1 161 2 8.493 . . . . . . . . . . . . . 30232 1 162 1 5.075 . . . . . . . . . . . . . 30232 1 162 2 8.493 . . . . . . . . . . . . . 30232 1 163 1 5.024 . . . . . . . . . . . . . 30232 1 163 2 3.889 . . . . . . . . . . . . . 30232 1 164 1 4.521 . . . . . . . . . . . . . 30232 1 164 2 3.882 . . . . . . . . . . . . . 30232 1 165 1 4.521 . . . . . . . . . . . . . 30232 1 165 2 3.59 . . . . . . . . . . . . . 30232 1 166 1 4.626 . . . . . . . . . . . . . 30232 1 166 2 3.959 . . . . . . . . . . . . . 30232 1 167 1 5.233 . . . . . . . . . . . . . 30232 1 167 2 3.332 . . . . . . . . . . . . . 30232 1 168 1 5.23 . . . . . . . . . . . . . 30232 1 168 2 3.171 . . . . . . . . . . . . . 30232 1 169 1 3.593 . . . . . . . . . . . . . 30232 1 169 2 1.718 . . . . . . . . . . . . . 30232 1 170 1 3.591 . . . . . . . . . . . . . 30232 1 170 2 1.58 . . . . . . . . . . . . . 30232 1 171 1 3.878 . . . . . . . . . . . . . 30232 1 171 2 1.718 . . . . . . . . . . . . . 30232 1 172 1 3.884 . . . . . . . . . . . . . 30232 1 172 2 1.579 . . . . . . . . . . . . . 30232 1 173 1 5.028 . . . . . . . . . . . . . 30232 1 173 2 2.85 . . . . . . . . . . . . . 30232 1 174 1 5.029 . . . . . . . . . . . . . 30232 1 174 2 2.605 . . . . . . . . . . . . . 30232 1 175 1 4.414 . . . . . . . . . . . . . 30232 1 175 2 2.016 . . . . . . . . . . . . . 30232 1 176 1 1.885 . . . . . . . . . . . . . 30232 1 176 2 0.625 . . . . . . . . . . . . . 30232 1 177 1 1.888 . . . . . . . . . . . . . 30232 1 177 2 0.761 . . . . . . . . . . . . . 30232 1 178 1 3.871 . . . . . . . . . . . . . 30232 1 178 2 0.618 . . . . . . . . . . . . . 30232 1 179 1 3.875 . . . . . . . . . . . . . 30232 1 179 2 0.765 . . . . . . . . . . . . . 30232 1 180 1 3.042 . . . . . . . . . . . . . 30232 1 180 2 7.298 . . . . . . . . . . . . . 30232 1 181 1 3.421 . . . . . . . . . . . . . 30232 1 181 2 7.299 . . . . . . . . . . . . . 30232 1 182 1 3.94 . . . . . . . . . . . . . 30232 1 182 2 7.051 . . . . . . . . . . . . . 30232 1 183 1 7.494 . . . . . . . . . . . . . 30232 1 183 2 7.647 . . . . . . . . . . . . . 30232 1 184 1 7.055 . . . . . . . . . . . . . 30232 1 184 2 7.647 . . . . . . . . . . . . . 30232 1 185 1 7.651 . . . . . . . . . . . . . 30232 1 185 2 8.2 . . . . . . . . . . . . . 30232 1 186 1 4.414 . . . . . . . . . . . . . 30232 1 186 2 4.085 . . . . . . . . . . . . . 30232 1 187 1 4.083 . . . . . . . . . . . . . 30232 1 187 2 1.165 . . . . . . . . . . . . . 30232 1 188 1 4.412 . . . . . . . . . . . . . 30232 1 188 2 1.173 . . . . . . . . . . . . . 30232 1 189 1 2.852 . . . . . . . . . . . . . 30232 1 189 2 2.605 . . . . . . . . . . . . . 30232 1 190 1 3.874 . . . . . . . . . . . . . 30232 1 190 2 1.883 . . . . . . . . . . . . . 30232 1 191 1 4.64 . . . . . . . . . . . . . 30232 1 191 2 2.712 . . . . . . . . . . . . . 30232 1 192 1 4.639 . . . . . . . . . . . . . 30232 1 192 2 3.071 . . . . . . . . . . . . . 30232 1 193 1 3.26 . . . . . . . . . . . . . 30232 1 193 2 2.617 . . . . . . . . . . . . . 30232 1 194 1 5.075 . . . . . . . . . . . . . 30232 1 194 2 2.618 . . . . . . . . . . . . . 30232 1 195 1 1.982 . . . . . . . . . . . . . 30232 1 195 2 8.492 . . . . . . . . . . . . . 30232 1 196 1 3.882 . . . . . . . . . . . . . 30232 1 196 2 3.587 . . . . . . . . . . . . . 30232 1 197 1 4.32 . . . . . . . . . . . . . 30232 1 197 2 3.682 . . . . . . . . . . . . . 30232 1 198 1 2.267 . . . . . . . . . . . . . 30232 1 198 2 7.682 . . . . . . . . . . . . . 30232 1 199 1 6.938 . . . . . . . . . . . . . 30232 1 199 2 7.682 . . . . . . . . . . . . . 30232 1 200 1 4.812 . . . . . . . . . . . . . 30232 1 200 2 2.343 . . . . . . . . . . . . . 30232 1 201 1 4.814 . . . . . . . . . . . . . 30232 1 201 2 2.267 . . . . . . . . . . . . . 30232 1 202 1 2.309 . . . . . . . . . . . . . 30232 1 202 2 8.977 . . . . . . . . . . . . . 30232 1 203 1 1.986 . . . . . . . . . . . . . 30232 1 203 2 8.978 . . . . . . . . . . . . . 30232 1 204 1 4.592 . . . . . . . . . . . . . 30232 1 204 2 1.225 . . . . . . . . . . . . . 30232 1 205 1 4.052 . . . . . . . . . . . . . 30232 1 205 2 1.224 . . . . . . . . . . . . . 30232 1 206 1 4.59 . . . . . . . . . . . . . 30232 1 206 2 4.055 . . . . . . . . . . . . . 30232 1 207 1 4.59 . . . . . . . . . . . . . 30232 1 207 2 8.88 . . . . . . . . . . . . . 30232 1 208 1 1.225 . . . . . . . . . . . . . 30232 1 208 2 8.88 . . . . . . . . . . . . . 30232 1 209 1 5.013 . . . . . . . . . . . . . 30232 1 209 2 3.086 . . . . . . . . . . . . . 30232 1 210 1 5.013 . . . . . . . . . . . . . 30232 1 210 2 3.211 . . . . . . . . . . . . . 30232 1 211 1 4.836 . . . . . . . . . . . . . 30232 1 211 2 8.905 . . . . . . . . . . . . . 30232 1 212 1 3.967 . . . . . . . . . . . . . 30232 1 212 2 2.982 . . . . . . . . . . . . . 30232 1 213 1 3.959 . . . . . . . . . . . . . 30232 1 213 2 1.718 . . . . . . . . . . . . . 30232 1 214 1 3.961 . . . . . . . . . . . . . 30232 1 214 2 1.487 . . . . . . . . . . . . . 30232 1 215 1 2.979 . . . . . . . . . . . . . 30232 1 215 2 1.72 . . . . . . . . . . . . . 30232 1 216 1 2.977 . . . . . . . . . . . . . 30232 1 216 2 1.486 . . . . . . . . . . . . . 30232 1 217 1 2.981 . . . . . . . . . . . . . 30232 1 217 2 1.407 . . . . . . . . . . . . . 30232 1 218 1 3.966 . . . . . . . . . . . . . 30232 1 218 2 1.931 . . . . . . . . . . . . . 30232 1 219 1 7.604 . . . . . . . . . . . . . 30232 1 219 2 8.649 . . . . . . . . . . . . . 30232 1 220 1 3.76 . . . . . . . . . . . . . 30232 1 220 2 8.649 . . . . . . . . . . . . . 30232 1 221 1 1.212 . . . . . . . . . . . . . 30232 1 221 2 8.647 . . . . . . . . . . . . . 30232 1 222 1 1.415 . . . . . . . . . . . . . 30232 1 222 2 8.648 . . . . . . . . . . . . . 30232 1 223 1 4.628 . . . . . . . . . . . . . 30232 1 223 2 2.568 . . . . . . . . . . . . . 30232 1 224 1 4.628 . . . . . . . . . . . . . 30232 1 224 2 2.766 . . . . . . . . . . . . . 30232 1 225 1 6.949 . . . . . . . . . . . . . 30232 1 225 2 8.142 . . . . . . . . . . . . . 30232 1 226 1 4.134 . . . . . . . . . . . . . 30232 1 226 2 8.539 . . . . . . . . . . . . . 30232 1 227 1 5.357 . . . . . . . . . . . . . 30232 1 227 2 2.847 . . . . . . . . . . . . . 30232 1 228 1 5.355 . . . . . . . . . . . . . 30232 1 228 2 2.781 . . . . . . . . . . . . . 30232 1 229 1 3.048 . . . . . . . . . . . . . 30232 1 229 2 9.446 . . . . . . . . . . . . . 30232 1 230 1 4.756 . . . . . . . . . . . . . 30232 1 230 2 3.046 . . . . . . . . . . . . . 30232 1 231 1 5.236 . . . . . . . . . . . . . 30232 1 231 2 8.896 . . . . . . . . . . . . . 30232 1 232 1 2.28 . . . . . . . . . . . . . 30232 1 232 2 8.898 . . . . . . . . . . . . . 30232 1 233 1 4.265 . . . . . . . . . . . . . 30232 1 233 2 8.137 . . . . . . . . . . . . . 30232 1 234 1 1.738 . . . . . . . . . . . . . 30232 1 234 2 8.081 . . . . . . . . . . . . . 30232 1 235 1 4.1 . . . . . . . . . . . . . 30232 1 235 2 8.494 . . . . . . . . . . . . . 30232 1 236 1 4.325 . . . . . . . . . . . . . 30232 1 236 2 8.492 . . . . . . . . . . . . . 30232 1 237 1 3.649 . . . . . . . . . . . . . 30232 1 237 2 6.95 . . . . . . . . . . . . . 30232 1 238 1 4.965 . . . . . . . . . . . . . 30232 1 238 2 8.539 . . . . . . . . . . . . . 30232 1 239 1 3.205 . . . . . . . . . . . . . 30232 1 239 2 7.242 . . . . . . . . . . . . . 30232 1 240 1 3.25 . . . . . . . . . . . . . 30232 1 240 2 8.494 . . . . . . . . . . . . . 30232 1 241 1 8.142 . . . . . . . . . . . . . 30232 1 241 2 8.295 . . . . . . . . . . . . . 30232 1 stop_ save_