data_30342 ####################### # Entry information # ####################### save_entry_information _Entry.Sf_category entry_information _Entry.Sf_framecode entry_information _Entry.ID 30342 _Entry.Title ; NMR structure of sea anemone toxin Kappa-actitoxin-Ate1a ; _Entry.Type macromolecule _Entry.Version_type original _Entry.Submission_date 2017-09-10 _Entry.Accession_date 2017-09-10 _Entry.Last_release_date 2017-09-13 _Entry.Original_release_date 2017-09-13 _Entry.Origination author _Entry.Format_name . _Entry.NMR_STAR_version 3.2.0.16 _Entry.Original_NMR_STAR_version 3.2.0.16 _Entry.Experimental_method NMR _Entry.Experimental_method_subtype SOLUTION _Entry.Source_data_format . _Entry.Source_data_format_version . _Entry.Generated_software_name . _Entry.Generated_software_version . _Entry.Generated_software_ID . _Entry.Generated_software_label . _Entry.Generated_date . _Entry.DOI . _Entry.UUID . _Entry.Related_coordinate_file_name . _Entry.Details . _Entry.BMRB_internal_directory_name . loop_ _Entry_author.Ordinal _Entry_author.Given_name _Entry_author.Family_name _Entry_author.First_initial _Entry_author.Middle_initials _Entry_author.Family_title _Entry_author.ORCID _Entry_author.Entry_ID 1 Y. Chin Y. K.-Y. . . 30342 2 B. Madio B. . . . 30342 3 G. King G. F. . . 30342 4 E. Undheim E. A.B. . . 30342 stop_ loop_ _Struct_keywords.Keywords _Struct_keywords.Text _Struct_keywords.Entry_ID 'Sea anemone; Actinia tenebrosa; Neurotoxin; Ion channels' . 30342 TOXIN . 30342 stop_ loop_ _Data_set.Type _Data_set.Count _Data_set.Entry_ID assigned_chemical_shifts 1 30342 spectral_peak_list 1 30342 stop_ loop_ _Datum.Type _Datum.Count _Datum.Entry_ID '13C chemical shifts' 52 30342 '15N chemical shifts' 17 30342 '1H chemical shifts' 108 30342 stop_ loop_ _Release.Release_number _Release.Format_type _Release.Format_version _Release.Date _Release.Submission_date _Release.Type _Release.Author _Release.Detail _Release.Entry_ID 1 . . 2018-09-06 . original BMRB . 30342 stop_ loop_ _Related_entries.Database_name _Related_entries.Database_accession_code _Related_entries.Relationship _Related_entries.Entry_ID PDB 6AZA 'BMRB Entry Tracking System' 30342 stop_ save_ ############### # Citations # ############### save_citation_1 _Citation.Sf_category citations _Citation.Sf_framecode citation_1 _Citation.Entry_ID 30342 _Citation.ID 1 _Citation.Class 'entry citation' _Citation.CAS_abstract_code . _Citation.MEDLINE_UI_code . _Citation.DOI . _Citation.PubMed_ID . _Citation.Full_citation . _Citation.Title ; Structure and function of AteTx1: a new type of KV sea anemone toxins ; _Citation.Status 'in preparation' _Citation.Type journal _Citation.Journal_abbrev . _Citation.Journal_name_full . _Citation.Journal_volume . _Citation.Journal_issue . _Citation.Journal_ASTM . _Citation.Journal_ISSN . _Citation.Journal_CSD 0353 _Citation.Book_title . _Citation.Book_chapter_title . _Citation.Book_volume . _Citation.Book_series . _Citation.Book_publisher . _Citation.Book_publisher_city . _Citation.Book_ISBN . _Citation.Conference_title . _Citation.Conference_site . _Citation.Conference_state_province . _Citation.Conference_country . _Citation.Conference_start_date . _Citation.Conference_end_date . _Citation.Conference_abstract_number . _Citation.Thesis_institution . _Citation.Thesis_institution_city . _Citation.Thesis_institution_country . _Citation.WWW_URL . _Citation.Page_first . _Citation.Page_last . _Citation.Year . _Citation.Details . loop_ _Citation_author.Ordinal _Citation_author.Given_name _Citation_author.Family_name _Citation_author.First_initial _Citation_author.Middle_initials _Citation_author.Family_title _Citation_author.ORCID _Citation_author.Entry_ID _Citation_author.Citation_ID 1 B. Madio B. . . . 30342 1 2 S. Peigneur S. . . . 30342 1 3 S. Henriques S. T. . . 30342 1 4 J. Smith J. J. . . 30342 1 5 B. Cristofori-Armstrong B. . . . 30342 1 6 Y. Chin Y. K.-Y. . . 30342 1 7 B. Hamilton B. R. . . 30342 1 8 Z. Dekan Z. . . . 30342 1 9 P. Alewood P. F. . . 30342 1 10 J. Tytgat J. . . . 30342 1 11 G. King G. F. . . 30342 1 12 E. Undheim E. A.B. . . 30342 1 stop_ save_ ############################################# # Molecular system (assembly) description # ############################################# save_assembly _Assembly.Sf_category assembly _Assembly.Sf_framecode assembly _Assembly.Entry_ID 30342 _Assembly.ID 1 _Assembly.Name 'sea anemone toxin Kappa-actitoxin-Ate1a' _Assembly.BMRB_code . _Assembly.Number_of_components . _Assembly.Organic_ligands . _Assembly.Metal_ions . _Assembly.Non_standard_bonds . _Assembly.Ambiguous_conformational_states . _Assembly.Ambiguous_chem_comp_sites . _Assembly.Molecules_in_chemical_exchange . _Assembly.Paramagnetic no _Assembly.Thiol_state . _Assembly.Molecular_mass . _Assembly.Enzyme_commission_number . _Assembly.Details . _Assembly.DB_query_date . _Assembly.DB_query_revised_last_date . loop_ _Entity_assembly.ID _Entity_assembly.Entity_assembly_name _Entity_assembly.Entity_ID _Entity_assembly.Entity_label _Entity_assembly.Asym_ID _Entity_assembly.PDB_chain_ID _Entity_assembly.Experimental_data_reported _Entity_assembly.Physical_state _Entity_assembly.Conformational_isomer _Entity_assembly.Chemical_exchange_state _Entity_assembly.Magnetic_equivalence_group_code _Entity_assembly.Role _Entity_assembly.Details _Entity_assembly.Entry_ID _Entity_assembly.Assembly_ID 1 entity_1 1 $entity_1 A A yes . . . . . . 30342 1 stop_ save_ #################################### # Biological polymers and ligands # #################################### save_entity_1 _Entity.Sf_category entity _Entity.Sf_framecode entity_1 _Entity.Entry_ID 30342 _Entity.ID 1 _Entity.BMRB_code . _Entity.Name 'sea anemone toxin Kappa-actitoxin-Ate1a' _Entity.Type polymer _Entity.Polymer_common_type . _Entity.Polymer_type polypeptide(L) _Entity.Polymer_type_details . _Entity.Polymer_strand_ID A _Entity.Polymer_seq_one_letter_code_can . _Entity.Polymer_seq_one_letter_code ; RCKTCSKGRCRPKPNCGX ; _Entity.Target_identifier . _Entity.Polymer_author_defined_seq . _Entity.Polymer_author_seq_details . _Entity.Ambiguous_conformational_states . _Entity.Ambiguous_chem_comp_sites . _Entity.Nstd_monomer yes _Entity.Nstd_chirality . _Entity.Nstd_linkage no _Entity.Nonpolymer_comp_ID . _Entity.Nonpolymer_comp_label . _Entity.Number_of_monomers 18 _Entity.Number_of_nonpolymer_components . _Entity.Paramagnetic no _Entity.Thiol_state . _Entity.Src_method syn _Entity.Parent_entity_ID 1 _Entity.Fragment . _Entity.Mutation . _Entity.EC_number . _Entity.Calc_isoelectric_point . _Entity.Formula_weight 1898.332 _Entity.Formula_weight_exptl . _Entity.Formula_weight_exptl_meth . _Entity.Details 'RcKTcSKGRcRPKPNcG NH2' _Entity.DB_query_date . _Entity.DB_query_revised_last_date . loop_ _Entity_comp_index.ID _Entity_comp_index.Auth_seq_ID _Entity_comp_index.Comp_ID _Entity_comp_index.Comp_label _Entity_comp_index.Entry_ID _Entity_comp_index.Entity_ID 1 . ARG . 30342 1 2 . CYS . 30342 1 3 . LYS . 30342 1 4 . THR . 30342 1 5 . CYS . 30342 1 6 . SER . 30342 1 7 . LYS . 30342 1 8 . GLY . 30342 1 9 . ARG . 30342 1 10 . CYS . 30342 1 11 . ARG . 30342 1 12 . PRO . 30342 1 13 . LYS . 30342 1 14 . PRO . 30342 1 15 . ASN . 30342 1 16 . CYS . 30342 1 17 . GLY . 30342 1 18 . NH2 . 30342 1 stop_ loop_ _Entity_poly_seq.Hetero _Entity_poly_seq.Mon_ID _Entity_poly_seq.Num _Entity_poly_seq.Comp_index_ID _Entity_poly_seq.Entry_ID _Entity_poly_seq.Entity_ID . ARG 1 1 30342 1 . CYS 2 2 30342 1 . LYS 3 3 30342 1 . THR 4 4 30342 1 . CYS 5 5 30342 1 . SER 6 6 30342 1 . LYS 7 7 30342 1 . GLY 8 8 30342 1 . ARG 9 9 30342 1 . CYS 10 10 30342 1 . ARG 11 11 30342 1 . PRO 12 12 30342 1 . LYS 13 13 30342 1 . PRO 14 14 30342 1 . ASN 15 15 30342 1 . CYS 16 16 30342 1 . GLY 17 17 30342 1 . NH2 18 18 30342 1 stop_ save_ #################### # Natural source # #################### save_natural_source _Entity_natural_src_list.Sf_category natural_source _Entity_natural_src_list.Sf_framecode natural_source _Entity_natural_src_list.Entry_ID 30342 _Entity_natural_src_list.ID 1 loop_ _Entity_natural_src.ID _Entity_natural_src.Entity_ID _Entity_natural_src.Entity_label _Entity_natural_src.Entity_chimera_segment_ID _Entity_natural_src.NCBI_taxonomy_ID _Entity_natural_src.Type _Entity_natural_src.Common _Entity_natural_src.Organism_name_scientific _Entity_natural_src.Organism_name_common _Entity_natural_src.Organism_acronym _Entity_natural_src.ICTVdb_decimal_code _Entity_natural_src.Superkingdom _Entity_natural_src.Kingdom _Entity_natural_src.Genus _Entity_natural_src.Species _Entity_natural_src.Strain _Entity_natural_src.Variant _Entity_natural_src.Organ _Entity_natural_src.Tissue _Entity_natural_src.Tissue_fraction _Entity_natural_src.Cell_line _Entity_natural_src.Cell_type _Entity_natural_src.ATCC_number _Entity_natural_src.Organelle _Entity_natural_src.Secretion _Entity_natural_src.Plasmid _Entity_natural_src.Gene_mnemonic _Entity_natural_src.Details _Entity_natural_src.Entry_ID _Entity_natural_src.Entity_natural_src_list_ID 1 1 $entity_1 . 6105 organism . 'Actinia tenebrosa' 'Australian red waratah sea anemone' . . Eukaryota Metazoa Actinia tenebrosa . . . . . . . . . . . . . 30342 1 stop_ save_ ######################### # Experimental source # ######################### save_experimental_source _Entity_experimental_src_list.Sf_category experimental_source _Entity_experimental_src_list.Sf_framecode experimental_source _Entity_experimental_src_list.Entry_ID 30342 _Entity_experimental_src_list.ID 1 loop_ _Entity_experimental_src.ID _Entity_experimental_src.Entity_ID _Entity_experimental_src.Entity_label _Entity_experimental_src.Entity_chimera_segment_ID _Entity_experimental_src.Production_method _Entity_experimental_src.Host_org_scientific_name _Entity_experimental_src.Host_org_name_common _Entity_experimental_src.Host_org_details _Entity_experimental_src.Host_org_NCBI_taxonomy_ID _Entity_experimental_src.Host_org_genus _Entity_experimental_src.Host_org_species _Entity_experimental_src.Host_org_strain _Entity_experimental_src.Host_org_variant _Entity_experimental_src.Host_org_ATCC_number _Entity_experimental_src.Vector_type _Entity_experimental_src.PDBview_host_org_vector_name _Entity_experimental_src.PDBview_plasmid_name _Entity_experimental_src.Vector_name _Entity_experimental_src.Vector_details _Entity_experimental_src.Vendor_name _Entity_experimental_src.Details _Entity_experimental_src.Entry_ID _Entity_experimental_src.Entity_experimental_src_list_ID 1 1 $entity_1 . 'chemical synthesis' . . . . . . . . . . . . . . . . 30342 1 stop_ save_ ################################# # Polymer residues and ligands # ################################# save_chem_comp_NH2 _Chem_comp.Sf_category chem_comp _Chem_comp.Sf_framecode chem_comp_NH2 _Chem_comp.Entry_ID 30342 _Chem_comp.ID NH2 _Chem_comp.Provenance PDB _Chem_comp.Name 'AMINO GROUP' _Chem_comp.Type NON-POLYMER _Chem_comp.BMRB_code NH2 _Chem_comp.PDB_code NH2 _Chem_comp.Ambiguous_flag yes _Chem_comp.Initial_date 2012-11-20 _Chem_comp.Modified_date 2012-11-20 _Chem_comp.Release_status REL _Chem_comp.Replaced_by . _Chem_comp.Replaces . _Chem_comp.One_letter_code . _Chem_comp.Three_letter_code NH2 _Chem_comp.Number_atoms_all 3 _Chem_comp.Number_atoms_nh 1 _Chem_comp.Atom_nomenclature_source . _Chem_comp.PubChem_code . _Chem_comp.Subcomponent_list . _Chem_comp.InChI_code InChI=1/H3N/h1H3 _Chem_comp.Mon_nstd_flag . _Chem_comp.Mon_nstd_class . _Chem_comp.Mon_nstd_details . _Chem_comp.Mon_nstd_parent . _Chem_comp.Mon_nstd_parent_comp_ID . _Chem_comp.Std_deriv_one_letter_code . _Chem_comp.Std_deriv_three_letter_code . _Chem_comp.Std_deriv_BMRB_code . _Chem_comp.Std_deriv_PDB_code . _Chem_comp.Std_deriv_chem_comp_name . _Chem_comp.Synonyms . _Chem_comp.Formal_charge 0 _Chem_comp.Paramagnetic . _Chem_comp.Aromatic no _Chem_comp.Formula 'H2 N' _Chem_comp.Formula_weight 16.023 _Chem_comp.Formula_mono_iso_wt_nat . _Chem_comp.Formula_mono_iso_wt_13C . _Chem_comp.Formula_mono_iso_wt_15N . _Chem_comp.Formula_mono_iso_wt_13C_15N . _Chem_comp.Image_file_name . _Chem_comp.Image_file_format . _Chem_comp.Topo_file_name . _Chem_comp.Topo_file_format . _Chem_comp.Struct_file_name . _Chem_comp.Struct_file_format . _Chem_comp.Stereochem_param_file_name . _Chem_comp.Stereochem_param_file_format . _Chem_comp.Model_details . _Chem_comp.Model_erf . _Chem_comp.Model_source . _Chem_comp.Model_coordinates_details . _Chem_comp.Model_coordinates_missing_flag no _Chem_comp.Ideal_coordinates_details 'OpenEye OEToolkits' _Chem_comp.Ideal_coordinates_missing_flag no _Chem_comp.Model_coordinates_db_code 2FLY _Chem_comp.Processing_site RCSB _Chem_comp.Vendor . _Chem_comp.Vendor_product_code . _Chem_comp.Details . _Chem_comp.DB_query_date . _Chem_comp.DB_last_query_revised_last_date . save_ ##################################### # Sample contents and methodology # ##################################### ######################## # Sample description # ######################## save_sample_1 _Sample.Sf_category sample _Sample.Sf_framecode sample_1 _Sample.Entry_ID 30342 _Sample.ID 1 _Sample.Type solution _Sample.Sub_type . _Sample.Details '1 mM AteTx1, 20 mM sodium phosphate, 5 % D2O, 95 % H2O, 95% H2O/5% D2O' _Sample.Aggregate_sample_number . _Sample.Solvent_system '95% H2O/5% D2O' _Sample.Preparation_date . _Sample.Preparation_expiration_date . _Sample.Polycrystallization_protocol . _Sample.Single_crystal_protocol . _Sample.Crystal_grow_apparatus . _Sample.Crystal_grow_atmosphere . _Sample.Crystal_grow_details . _Sample.Crystal_grow_method . _Sample.Crystal_grow_method_cit_ID . _Sample.Crystal_grow_pH . _Sample.Crystal_grow_pH_range . _Sample.Crystal_grow_pressure . _Sample.Crystal_grow_pressure_esd . _Sample.Crystal_grow_seeding . _Sample.Crystal_grow_seeding_cit_ID . _Sample.Crystal_grow_temp . _Sample.Crystal_grow_temp_details . _Sample.Crystal_grow_temp_esd . _Sample.Crystal_grow_time . _Sample.Oriented_sample_prep_protocol . _Sample.Lyophilization_cryo_protectant . _Sample.Storage_protocol . loop_ _Sample_component.ID _Sample_component.Mol_common_name _Sample_component.Isotopic_labeling _Sample_component.Assembly_ID _Sample_component.Assembly_label _Sample_component.Entity_ID _Sample_component.Entity_label _Sample_component.Product_ID _Sample_component.Type _Sample_component.Concentration_val _Sample_component.Concentration_val_min _Sample_component.Concentration_val_max _Sample_component.Concentration_val_units _Sample_component.Concentration_val_err _Sample_component.Vendor _Sample_component.Vendor_product_name _Sample_component.Vendor_product_code _Sample_component.Entry_ID _Sample_component.Sample_ID 1 AteTx1 'natural abundance' . . 1 $entity_1 . . 1 . . mM . . . . 30342 1 2 D2O 'natural abundance' . . . . . . 5 . . % . . . . 30342 1 3 H2O 'natural abundance' . . . . . . 95 . . % . . . . 30342 1 4 'sodium phosphate' 'natural abundance' . . . . . . 20 . . mM . . . . 30342 1 stop_ save_ save_sample_2 _Sample.Sf_category sample _Sample.Sf_framecode sample_2 _Sample.Entry_ID 30342 _Sample.ID 2 _Sample.Type solution _Sample.Sub_type . _Sample.Details '1 mM AteTx1, 20 mM sodium phosphate, 100 % D2O, 100% D2O' _Sample.Aggregate_sample_number . _Sample.Solvent_system '100% D2O' _Sample.Preparation_date . _Sample.Preparation_expiration_date . _Sample.Polycrystallization_protocol . _Sample.Single_crystal_protocol . _Sample.Crystal_grow_apparatus . _Sample.Crystal_grow_atmosphere . _Sample.Crystal_grow_details . _Sample.Crystal_grow_method . _Sample.Crystal_grow_method_cit_ID . _Sample.Crystal_grow_pH . _Sample.Crystal_grow_pH_range . _Sample.Crystal_grow_pressure . _Sample.Crystal_grow_pressure_esd . _Sample.Crystal_grow_seeding . _Sample.Crystal_grow_seeding_cit_ID . _Sample.Crystal_grow_temp . _Sample.Crystal_grow_temp_details . _Sample.Crystal_grow_temp_esd . _Sample.Crystal_grow_time . _Sample.Oriented_sample_prep_protocol . _Sample.Lyophilization_cryo_protectant . _Sample.Storage_protocol . loop_ _Sample_component.ID _Sample_component.Mol_common_name _Sample_component.Isotopic_labeling _Sample_component.Assembly_ID _Sample_component.Assembly_label _Sample_component.Entity_ID _Sample_component.Entity_label _Sample_component.Product_ID _Sample_component.Type _Sample_component.Concentration_val _Sample_component.Concentration_val_min _Sample_component.Concentration_val_max _Sample_component.Concentration_val_units _Sample_component.Concentration_val_err _Sample_component.Vendor _Sample_component.Vendor_product_name _Sample_component.Vendor_product_code _Sample_component.Entry_ID _Sample_component.Sample_ID 1 AteTx1 'natural abundance' . . 1 $entity_1 . . 1 . . mM . . . . 30342 2 2 D2O 'natural abundance' . . . . . . 100 . . % . . . . 30342 2 3 'sodium phosphate' 'natural abundance' . . . . . . 20 . . mM . . . . 30342 2 stop_ save_ ####################### # Sample conditions # ####################### save_sample_conditions_1 _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode sample_conditions_1 _Sample_condition_list.Entry_ID 30342 _Sample_condition_list.ID 1 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID 'ionic strength' 20 . mM 30342 1 pH 6 . pH 30342 1 pressure 1 . atm 30342 1 temperature 283 . K 30342 1 stop_ save_ ############################ # Computer software used # ############################ save_software_1 _Software.Sf_category software _Software.Sf_framecode software_1 _Software.Entry_ID 30342 _Software.ID 1 _Software.Type . _Software.Name Analysis _Software.Version . _Software.DOI . _Software.Details . loop_ _Vendor.Name _Vendor.Address _Vendor.Electronic_address _Vendor.Entry_ID _Vendor.Software_ID CCPN . . 30342 1 stop_ loop_ _Task.Task _Task.Entry_ID _Task.Software_ID 'chemical shift assignment' 30342 1 'peak picking' 30342 1 stop_ save_ save_software_2 _Software.Sf_category software _Software.Sf_framecode software_2 _Software.Entry_ID 30342 _Software.ID 2 _Software.Type . _Software.Name CYANA _Software.Version . _Software.DOI . _Software.Details . loop_ _Vendor.Name _Vendor.Address _Vendor.Electronic_address _Vendor.Entry_ID _Vendor.Software_ID 'Guntert, Mumenthaler and Wuthrich' . . 30342 2 stop_ loop_ _Task.Task _Task.Entry_ID _Task.Software_ID refinement 30342 2 'structure calculation' 30342 2 stop_ save_ save_software_3 _Software.Sf_category software _Software.Sf_framecode software_3 _Software.Entry_ID 30342 _Software.ID 3 _Software.Type . _Software.Name TOPSPIN _Software.Version . _Software.DOI . _Software.Details . loop_ _Vendor.Name _Vendor.Address _Vendor.Electronic_address _Vendor.Entry_ID _Vendor.Software_ID 'Bruker Biospin' . . 30342 3 stop_ loop_ _Task.Task _Task.Entry_ID _Task.Software_ID collection 30342 3 processing 30342 3 stop_ save_ ######################### # Experimental detail # ######################### ################################## # NMR Spectrometer definitions # ################################## save_NMR_spectrometer_1 _NMR_spectrometer.Sf_category NMR_spectrometer _NMR_spectrometer.Sf_framecode NMR_spectrometer_1 _NMR_spectrometer.Entry_ID 30342 _NMR_spectrometer.ID 1 _NMR_spectrometer.Details . _NMR_spectrometer.Manufacturer Bruker _NMR_spectrometer.Model AvanceIII _NMR_spectrometer.Serial_number . _NMR_spectrometer.Field_strength 600 save_ save_NMR_spectrometer_list _NMR_spectrometer_list.Sf_category NMR_spectrometer_list _NMR_spectrometer_list.Sf_framecode NMR_spectrometer_list _NMR_spectrometer_list.Entry_ID 30342 _NMR_spectrometer_list.ID 1 loop_ _NMR_spectrometer_view.ID _NMR_spectrometer_view.Name _NMR_spectrometer_view.Manufacturer _NMR_spectrometer_view.Model _NMR_spectrometer_view.Serial_number _NMR_spectrometer_view.Field_strength _NMR_spectrometer_view.Details _NMR_spectrometer_view.Citation_ID _NMR_spectrometer_view.Citation_label _NMR_spectrometer_view.Entry_ID _NMR_spectrometer_view.NMR_spectrometer_list_ID 1 NMR_spectrometer_1 Bruker AvanceIII . 600 . . . 30342 1 stop_ save_ ############################# # NMR applied experiments # ############################# save_experiment_list _Experiment_list.Sf_category experiment_list _Experiment_list.Sf_framecode experiment_list _Experiment_list.Entry_ID 30342 _Experiment_list.ID 1 _Experiment_list.Details . loop_ _Experiment.ID _Experiment.Name _Experiment.Raw_data_flag _Experiment.NMR_spec_expt_ID _Experiment.NMR_spec_expt_label _Experiment.MS_expt_ID _Experiment.MS_expt_label _Experiment.SAXS_expt_ID _Experiment.SAXS_expt_label _Experiment.FRET_expt_ID _Experiment.FRET_expt_label _Experiment.EMR_expt_ID _Experiment.EMR_expt_label _Experiment.Sample_ID _Experiment.Sample_label _Experiment.Sample_state _Experiment.Sample_volume _Experiment.Sample_volume_units _Experiment.Sample_condition_list_ID _Experiment.Sample_condition_list_label _Experiment.Sample_spinning_rate _Experiment.Sample_angle _Experiment.NMR_tube_type _Experiment.NMR_spectrometer_ID _Experiment.NMR_spectrometer_label _Experiment.NMR_spectrometer_probe_ID _Experiment.NMR_spectrometer_probe_label _Experiment.NMR_spectral_processing_ID _Experiment.NMR_spectral_processing_label _Experiment.Mass_spectrometer_ID _Experiment.Mass_spectrometer_label _Experiment.Xray_instrument_ID _Experiment.Xray_instrument_label _Experiment.Fluorescence_instrument_ID _Experiment.Fluorescence_instrument_label _Experiment.EMR_instrument_ID _Experiment.EMR_instrument_label _Experiment.Chromatographic_system_ID _Experiment.Chromatographic_system_label _Experiment.Chromatographic_column_ID _Experiment.Chromatographic_column_label _Experiment.Entry_ID _Experiment.Experiment_list_ID 1 '2D 1H-15N HSQC' no . . . . . . . . . . 1 $sample_1 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . 30342 1 2 '2D 1H-13C HSQC' no . . . . . . . . . . 1 $sample_1 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . 30342 1 3 '2D 1H-1H TOCSY' no . . . . . . . . . . 1 $sample_1 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . 30342 1 4 '2D 1H-1H NOESY' no . . . . . . . . . . 1 $sample_1 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . 30342 1 5 '2D 1H-13C HSQC' no . . . . . . . . . . 2 $sample_2 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . 30342 1 6 '2D 1H-1H TOCSY' no . . . . . . . . . . 2 $sample_2 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . 30342 1 stop_ save_ #################### # NMR parameters # #################### ############################## # Assigned chemical shifts # ############################## ################################ # Chemical shift referencing # ################################ save_chem_shift_reference_1 _Chem_shift_reference.Sf_category chem_shift_reference _Chem_shift_reference.Sf_framecode chem_shift_reference_1 _Chem_shift_reference.Entry_ID 30342 _Chem_shift_reference.ID 1 _Chem_shift_reference.Details . loop_ _Chem_shift_ref.Atom_type _Chem_shift_ref.Atom_isotope_number _Chem_shift_ref.Mol_common_name _Chem_shift_ref.Atom_group _Chem_shift_ref.Concentration_val _Chem_shift_ref.Concentration_units _Chem_shift_ref.Solvent _Chem_shift_ref.Rank _Chem_shift_ref.Chem_shift_units _Chem_shift_ref.Chem_shift_val _Chem_shift_ref.Ref_method _Chem_shift_ref.Ref_type _Chem_shift_ref.Indirect_shift_ratio _Chem_shift_ref.External_ref_loc _Chem_shift_ref.External_ref_sample_geometry _Chem_shift_ref.External_ref_axis _Chem_shift_ref.Ref_correction_type _Chem_shift_ref.Correction_val _Chem_shift_ref.Entry_ID _Chem_shift_ref.Chem_shift_reference_ID C 13 water protons . . . . ppm 4.700 external indirect 0.23144953 . . . . . 30342 1 H 1 water protons . . . . ppm 4.700 external direct 1 . . . . . 30342 1 N 14 water protons . . . . ppm 4.700 external indirect 0.10132912 . . . . . 30342 1 stop_ save_ ################################### # Assigned chemical shift lists # ################################### ################################################################### # Chemical Shift Ambiguity Index Value Definitions # # # # The values other than 1 are used for those atoms with different # # chemical shifts that cannot be assigned to stereospecific atoms # # or to specific residues or chains. # # # # Index Value Definition # # # # 1 Unique (including isolated methyl protons, # # geminal atoms, and geminal methyl # # groups with identical chemical shifts) # # (e.g. ILE HD11, HD12, HD13 protons) # # 2 Ambiguity of geminal atoms or geminal methyl # # proton groups (e.g. ASP HB2 and HB3 # # protons, LEU CD1 and CD2 carbons, or # # LEU HD11, HD12, HD13 and HD21, HD22, # # HD23 methyl protons) # # 3 Aromatic atoms on opposite sides of # # symmetrical rings (e.g. TYR HE1 and HE2 # # protons) # # 4 Intraresidue ambiguities (e.g. LYS HG and # # HD protons or TRP HZ2 and HZ3 protons) # # 5 Interresidue ambiguities (LYS 12 vs. LYS 27) # # 6 Intermolecular ambiguities (e.g. ASP 31 CA # # in monomer 1 and ASP 31 CA in monomer 2 # # of an asymmetrical homodimer, duplex # # DNA assignments, or other assignments # # that may apply to atoms in one or more # # molecule in the molecular assembly) # # 9 Ambiguous, specific ambiguity not defined # # # ################################################################### save_assigned_chemical_shifts_1 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode assigned_chemical_shifts_1 _Assigned_chem_shift_list.Entry_ID 30342 _Assigned_chem_shift_list.ID 1 _Assigned_chem_shift_list.Sample_condition_list_ID 1 _Assigned_chem_shift_list.Sample_condition_list_label $sample_conditions_1 _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chem_shift_reference_1 _Assigned_chem_shift_list.Chem_shift_1H_err . _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err . _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID 1 '2D 1H-15N HSQC' . . . 30342 1 2 '2D 1H-13C HSQC' . . . 30342 1 3 '2D 1H-1H TOCSY' . . . 30342 1 4 '2D 1H-1H NOESY' . . . 30342 1 5 '2D 1H-13C HSQC' . . . 30342 1 6 '2D 1H-1H TOCSY' . . . 30342 1 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Ambiguity_set_ID _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 1 1 1 ARG HA H 1 3.817 0.001 . 1 . . . . A 1 ARG HA . 30342 1 2 . 1 1 1 1 ARG HB2 H 1 1.693 0.001 . 2 . . . . A 1 ARG HB2 . 30342 1 3 . 1 1 1 1 ARG HB3 H 1 1.693 0.001 . 2 . . . . A 1 ARG HB3 . 30342 1 4 . 1 1 1 1 ARG HG2 H 1 1.428 0.000 . 2 . . . . A 1 ARG HG2 . 30342 1 5 . 1 1 1 1 ARG HG3 H 1 1.428 0.000 . 2 . . . . A 1 ARG HG3 . 30342 1 6 . 1 1 1 1 ARG HD2 H 1 2.980 0.002 . 2 . . . . A 1 ARG HD2 . 30342 1 7 . 1 1 1 1 ARG HD3 H 1 2.980 0.002 . 2 . . . . A 1 ARG HD3 . 30342 1 8 . 1 1 1 1 ARG CA C 13 55.403 0.000 . 1 . . . . A 1 ARG CA . 30342 1 9 . 1 1 1 1 ARG CB C 13 31.160 0.000 . 1 . . . . A 1 ARG CB . 30342 1 10 . 1 1 1 1 ARG CG C 13 26.126 0.000 . 1 . . . . A 1 ARG CG . 30342 1 11 . 1 1 1 1 ARG CD C 13 42.915 0.000 . 1 . . . . A 1 ARG CD . 30342 1 12 . 1 1 2 2 CYS HA H 1 4.465 0.002 . 1 . . . . A 2 CYS HA . 30342 1 13 . 1 1 2 2 CYS HB2 H 1 2.808 0.003 . 2 . . . . A 2 CYS HB2 . 30342 1 14 . 1 1 2 2 CYS HB3 H 1 3.098 0.005 . 2 . . . . A 2 CYS HB3 . 30342 1 15 . 1 1 2 2 CYS CA C 13 55.505 0.000 . 1 . . . . A 2 CYS CA . 30342 1 16 . 1 1 2 2 CYS CB C 13 40.615 0.052 . 1 . . . . A 2 CYS CB . 30342 1 17 . 1 1 3 3 LYS H H 1 8.369 0.002 . 1 . . . . A 3 LYS H . 30342 1 18 . 1 1 3 3 LYS HA H 1 4.442 0.002 . 1 . . . . A 3 LYS HA . 30342 1 19 . 1 1 3 3 LYS HB2 H 1 1.492 0.001 . 2 . . . . A 3 LYS HB2 . 30342 1 20 . 1 1 3 3 LYS HB3 H 1 1.464 0.000 . 2 . . . . A 3 LYS HB3 . 30342 1 21 . 1 1 3 3 LYS HG2 H 1 1.153 0.001 . 2 . . . . A 3 LYS HG2 . 30342 1 22 . 1 1 3 3 LYS HG3 H 1 1.106 0.000 . 2 . . . . A 3 LYS HG3 . 30342 1 23 . 1 1 3 3 LYS HD2 H 1 1.356 0.001 . 2 . . . . A 3 LYS HD2 . 30342 1 24 . 1 1 3 3 LYS HD3 H 1 1.473 0.001 . 2 . . . . A 3 LYS HD3 . 30342 1 25 . 1 1 3 3 LYS HE2 H 1 2.694 0.001 . 2 . . . . A 3 LYS HE2 . 30342 1 26 . 1 1 3 3 LYS HE3 H 1 2.694 0.001 . 2 . . . . A 3 LYS HE3 . 30342 1 27 . 1 1 3 3 LYS CA C 13 55.709 0.000 . 1 . . . . A 3 LYS CA . 30342 1 28 . 1 1 3 3 LYS CB C 13 34.528 0.003 . 1 . . . . A 3 LYS CB . 30342 1 29 . 1 1 3 3 LYS CG C 13 24.398 0.004 . 1 . . . . A 3 LYS CG . 30342 1 30 . 1 1 3 3 LYS CD C 13 29.194 0.000 . 1 . . . . A 3 LYS CD . 30342 1 31 . 1 1 3 3 LYS CE C 13 41.845 0.000 . 1 . . . . A 3 LYS CE . 30342 1 32 . 1 1 3 3 LYS N N 15 122.509 0.000 . 1 . . . . A 3 LYS N . 30342 1 33 . 1 1 4 4 THR H H 1 8.469 0.002 . 1 . . . . A 4 THR H . 30342 1 34 . 1 1 4 4 THR HA H 1 4.183 0.001 . 1 . . . . A 4 THR HA . 30342 1 35 . 1 1 4 4 THR HB H 1 3.809 0.001 . 1 . . . . A 4 THR HB . 30342 1 36 . 1 1 4 4 THR HG21 H 1 0.957 0.001 . 1 . . . . A 4 THR HG21 . 30342 1 37 . 1 1 4 4 THR HG22 H 1 0.957 0.001 . 1 . . . . A 4 THR HG22 . 30342 1 38 . 1 1 4 4 THR HG23 H 1 0.957 0.001 . 1 . . . . A 4 THR HG23 . 30342 1 39 . 1 1 4 4 THR CA C 13 61.425 0.000 . 1 . . . . A 4 THR CA . 30342 1 40 . 1 1 4 4 THR CB C 13 69.799 0.000 . 1 . . . . A 4 THR CB . 30342 1 41 . 1 1 4 4 THR CG2 C 13 21.219 0.000 . 1 . . . . A 4 THR CG2 . 30342 1 42 . 1 1 4 4 THR N N 15 117.614 0.000 . 1 . . . . A 4 THR N . 30342 1 43 . 1 1 5 5 CYS H H 1 8.642 0.000 . 1 . . . . A 5 CYS H . 30342 1 44 . 1 1 5 5 CYS HA H 1 4.968 0.001 . 1 . . . . A 5 CYS HA . 30342 1 45 . 1 1 5 5 CYS HB2 H 1 2.827 0.004 . 2 . . . . A 5 CYS HB2 . 30342 1 46 . 1 1 5 5 CYS HB3 H 1 2.734 0.002 . 2 . . . . A 5 CYS HB3 . 30342 1 47 . 1 1 5 5 CYS CA C 13 55.300 0.000 . 1 . . . . A 5 CYS CA . 30342 1 48 . 1 1 5 5 CYS CB C 13 45.223 0.005 . 1 . . . . A 5 CYS CB . 30342 1 49 . 1 1 5 5 CYS N N 15 124.221 0.000 . 1 . . . . A 5 CYS N . 30342 1 50 . 1 1 6 6 SER H H 1 8.530 0.001 . 1 . . . . A 6 SER H . 30342 1 51 . 1 1 6 6 SER HA H 1 4.249 0.003 . 1 . . . . A 6 SER HA . 30342 1 52 . 1 1 6 6 SER HB2 H 1 3.611 0.003 . 2 . . . . A 6 SER HB2 . 30342 1 53 . 1 1 6 6 SER HB3 H 1 3.554 0.004 . 2 . . . . A 6 SER HB3 . 30342 1 54 . 1 1 6 6 SER CA C 13 58.243 0.000 . 1 . . . . A 6 SER CA . 30342 1 55 . 1 1 6 6 SER CB C 13 63.814 0.025 . 1 . . . . A 6 SER CB . 30342 1 56 . 1 1 6 6 SER N N 15 118.392 0.000 . 1 . . . . A 6 SER N . 30342 1 57 . 1 1 7 7 LYS H H 1 8.702 0.002 . 1 . . . . A 7 LYS H . 30342 1 58 . 1 1 7 7 LYS HA H 1 3.873 0.002 . 1 . . . . A 7 LYS HA . 30342 1 59 . 1 1 7 7 LYS HB2 H 1 1.690 0.001 . 2 . . . . A 7 LYS HB2 . 30342 1 60 . 1 1 7 7 LYS HB3 H 1 1.601 0.001 . 2 . . . . A 7 LYS HB3 . 30342 1 61 . 1 1 7 7 LYS HG2 H 1 1.188 0.018 . 2 . . . . A 7 LYS HG2 . 30342 1 62 . 1 1 7 7 LYS HG3 H 1 1.149 0.002 . 2 . . . . A 7 LYS HG3 . 30342 1 63 . 1 1 7 7 LYS HD2 H 1 1.435 0.003 . 2 . . . . A 7 LYS HD2 . 30342 1 64 . 1 1 7 7 LYS HD3 H 1 1.435 0.003 . 2 . . . . A 7 LYS HD3 . 30342 1 65 . 1 1 7 7 LYS HE2 H 1 2.736 0.001 . 2 . . . . A 7 LYS HE2 . 30342 1 66 . 1 1 7 7 LYS HE3 H 1 2.736 0.001 . 2 . . . . A 7 LYS HE3 . 30342 1 67 . 1 1 7 7 LYS CA C 13 56.749 0.000 . 1 . . . . A 7 LYS CA . 30342 1 68 . 1 1 7 7 LYS CB C 13 30.797 0.003 . 1 . . . . A 7 LYS CB . 30342 1 69 . 1 1 7 7 LYS CG C 13 24.654 0.000 . 1 . . . . A 7 LYS CG . 30342 1 70 . 1 1 7 7 LYS CD C 13 28.899 0.000 . 1 . . . . A 7 LYS CD . 30342 1 71 . 1 1 7 7 LYS CE C 13 41.941 0.000 . 1 . . . . A 7 LYS CE . 30342 1 72 . 1 1 7 7 LYS N N 15 123.016 0.000 . 1 . . . . A 7 LYS N . 30342 1 73 . 1 1 8 8 GLY H H 1 8.447 0.002 . 1 . . . . A 8 GLY H . 30342 1 74 . 1 1 8 8 GLY HA2 H 1 3.889 0.003 . 2 . . . . A 8 GLY HA2 . 30342 1 75 . 1 1 8 8 GLY HA3 H 1 3.447 0.002 . 2 . . . . A 8 GLY HA3 . 30342 1 76 . 1 1 8 8 GLY CA C 13 45.119 0.008 . 1 . . . . A 8 GLY CA . 30342 1 77 . 1 1 8 8 GLY N N 15 107.178 0.000 . 1 . . . . A 8 GLY N . 30342 1 78 . 1 1 9 9 ARG H H 1 7.833 0.002 . 1 . . . . A 9 ARG H . 30342 1 79 . 1 1 9 9 ARG HA H 1 4.290 0.002 . 1 . . . . A 9 ARG HA . 30342 1 80 . 1 1 9 9 ARG HB2 H 1 1.627 0.002 . 2 . . . . A 9 ARG HB2 . 30342 1 81 . 1 1 9 9 ARG HB3 H 1 1.573 0.001 . 2 . . . . A 9 ARG HB3 . 30342 1 82 . 1 1 9 9 ARG HG2 H 1 1.404 0.002 . 2 . . . . A 9 ARG HG2 . 30342 1 83 . 1 1 9 9 ARG HG3 H 1 1.326 0.001 . 2 . . . . A 9 ARG HG3 . 30342 1 84 . 1 1 9 9 ARG HD2 H 1 2.958 0.002 . 2 . . . . A 9 ARG HD2 . 30342 1 85 . 1 1 9 9 ARG HD3 H 1 2.958 0.002 . 2 . . . . A 9 ARG HD3 . 30342 1 86 . 1 1 9 9 ARG HE H 1 7.002 0.005 . 1 . . . . A 9 ARG HE . 30342 1 87 . 1 1 9 9 ARG CA C 13 55.237 0.000 . 1 . . . . A 9 ARG CA . 30342 1 88 . 1 1 9 9 ARG CB C 13 30.955 0.005 . 1 . . . . A 9 ARG CB . 30342 1 89 . 1 1 9 9 ARG CG C 13 26.875 0.000 . 1 . . . . A 9 ARG CG . 30342 1 90 . 1 1 9 9 ARG CD C 13 43.300 0.000 . 1 . . . . A 9 ARG CD . 30342 1 91 . 1 1 9 9 ARG N N 15 120.407 0.000 . 1 . . . . A 9 ARG N . 30342 1 92 . 1 1 9 9 ARG NE N 15 84.311 0.000 . 1 . . . . A 9 ARG NE . 30342 1 93 . 1 1 10 10 CYS H H 1 8.518 0.001 . 1 . . . . A 10 CYS H . 30342 1 94 . 1 1 10 10 CYS HA H 1 4.936 0.001 . 1 . . . . A 10 CYS HA . 30342 1 95 . 1 1 10 10 CYS HB2 H 1 2.780 0.000 . 2 . . . . A 10 CYS HB2 . 30342 1 96 . 1 1 10 10 CYS HB3 H 1 2.674 0.001 . 2 . . . . A 10 CYS HB3 . 30342 1 97 . 1 1 10 10 CYS CA C 13 55.015 0.000 . 1 . . . . A 10 CYS CA . 30342 1 98 . 1 1 10 10 CYS CB C 13 44.477 0.010 . 1 . . . . A 10 CYS CB . 30342 1 99 . 1 1 10 10 CYS N N 15 121.295 0.000 . 1 . . . . A 10 CYS N . 30342 1 100 . 1 1 11 11 ARG H H 1 8.626 0.004 . 1 . . . . A 11 ARG H . 30342 1 101 . 1 1 11 11 ARG HA H 1 4.543 0.003 . 1 . . . . A 11 ARG HA . 30342 1 102 . 1 1 11 11 ARG HB2 H 1 1.610 0.001 . 2 . . . . A 11 ARG HB2 . 30342 1 103 . 1 1 11 11 ARG HB3 H 1 1.500 0.002 . 2 . . . . A 11 ARG HB3 . 30342 1 104 . 1 1 11 11 ARG HG2 H 1 1.412 0.001 . 2 . . . . A 11 ARG HG2 . 30342 1 105 . 1 1 11 11 ARG HG3 H 1 1.412 0.001 . 2 . . . . A 11 ARG HG3 . 30342 1 106 . 1 1 11 11 ARG HD2 H 1 2.965 0.003 . 2 . . . . A 11 ARG HD2 . 30342 1 107 . 1 1 11 11 ARG HD3 H 1 2.965 0.003 . 2 . . . . A 11 ARG HD3 . 30342 1 108 . 1 1 11 11 ARG HE H 1 7.037 0.000 . 1 . . . . A 11 ARG HE . 30342 1 109 . 1 1 11 11 ARG CA C 13 53.377 0.000 . 1 . . . . A 11 ARG CA . 30342 1 110 . 1 1 11 11 ARG CB C 13 30.693 0.000 . 1 . . . . A 11 ARG CB . 30342 1 111 . 1 1 11 11 ARG CG C 13 26.146 0.000 . 1 . . . . A 11 ARG CG . 30342 1 112 . 1 1 11 11 ARG CD C 13 43.107 0.000 . 1 . . . . A 11 ARG CD . 30342 1 113 . 1 1 11 11 ARG N N 15 123.138 0.000 . 1 . . . . A 11 ARG N . 30342 1 114 . 1 1 11 11 ARG NE N 15 84.365 0.000 . 1 . . . . A 11 ARG NE . 30342 1 115 . 1 1 12 12 PRO HA H 1 4.276 0.002 . 1 . . . . A 12 PRO HA . 30342 1 116 . 1 1 12 12 PRO HB2 H 1 2.060 0.001 . 2 . . . . A 12 PRO HB2 . 30342 1 117 . 1 1 12 12 PRO HB3 H 1 1.616 0.002 . 2 . . . . A 12 PRO HB3 . 30342 1 118 . 1 1 12 12 PRO HG2 H 1 1.744 0.001 . 2 . . . . A 12 PRO HG2 . 30342 1 119 . 1 1 12 12 PRO HG3 H 1 1.832 0.001 . 2 . . . . A 12 PRO HG3 . 30342 1 120 . 1 1 12 12 PRO HD2 H 1 3.414 0.001 . 2 . . . . A 12 PRO HD2 . 30342 1 121 . 1 1 12 12 PRO HD3 H 1 3.581 0.001 . 2 . . . . A 12 PRO HD3 . 30342 1 122 . 1 1 12 12 PRO CA C 13 62.926 0.000 . 1 . . . . A 12 PRO CA . 30342 1 123 . 1 1 12 12 PRO CB C 13 32.063 0.007 . 1 . . . . A 12 PRO CB . 30342 1 124 . 1 1 12 12 PRO CG C 13 27.268 0.004 . 1 . . . . A 12 PRO CG . 30342 1 125 . 1 1 12 12 PRO CD C 13 50.526 0.001 . 1 . . . . A 12 PRO CD . 30342 1 126 . 1 1 13 13 LYS H H 1 7.975 0.002 . 1 . . . . A 13 LYS H . 30342 1 127 . 1 1 13 13 LYS HA H 1 4.409 0.005 . 1 . . . . A 13 LYS HA . 30342 1 128 . 1 1 13 13 LYS HB2 H 1 1.568 0.001 . 2 . . . . A 13 LYS HB2 . 30342 1 129 . 1 1 13 13 LYS HB3 H 1 1.368 0.001 . 2 . . . . A 13 LYS HB3 . 30342 1 130 . 1 1 13 13 LYS HG2 H 1 1.197 0.001 . 2 . . . . A 13 LYS HG2 . 30342 1 131 . 1 1 13 13 LYS HG3 H 1 1.197 0.001 . 2 . . . . A 13 LYS HG3 . 30342 1 132 . 1 1 13 13 LYS HD2 H 1 1.433 0.001 . 2 . . . . A 13 LYS HD2 . 30342 1 133 . 1 1 13 13 LYS HD3 H 1 1.433 0.001 . 2 . . . . A 13 LYS HD3 . 30342 1 134 . 1 1 13 13 LYS HE2 H 1 2.743 0.002 . 2 . . . . A 13 LYS HE2 . 30342 1 135 . 1 1 13 13 LYS HE3 H 1 2.743 0.002 . 2 . . . . A 13 LYS HE3 . 30342 1 136 . 1 1 13 13 LYS CA C 13 55.898 0.000 . 1 . . . . A 13 LYS CA . 30342 1 137 . 1 1 13 13 LYS CB C 13 33.269 0.003 . 1 . . . . A 13 LYS CB . 30342 1 138 . 1 1 13 13 LYS CG C 13 24.880 0.000 . 1 . . . . A 13 LYS CG . 30342 1 139 . 1 1 13 13 LYS CD C 13 29.354 0.000 . 1 . . . . A 13 LYS CD . 30342 1 140 . 1 1 13 13 LYS CE C 13 41.861 0.000 . 1 . . . . A 13 LYS CE . 30342 1 141 . 1 1 13 13 LYS N N 15 123.183 0.000 . 1 . . . . A 13 LYS N . 30342 1 142 . 1 1 14 14 PRO HA H 1 4.101 0.001 . 1 . . . . A 14 PRO HA . 30342 1 143 . 1 1 14 14 PRO HB2 H 1 2.056 0.001 . 2 . . . . A 14 PRO HB2 . 30342 1 144 . 1 1 14 14 PRO HB3 H 1 1.662 0.001 . 2 . . . . A 14 PRO HB3 . 30342 1 145 . 1 1 14 14 PRO HG2 H 1 1.816 0.002 . 2 . . . . A 14 PRO HG2 . 30342 1 146 . 1 1 14 14 PRO HG3 H 1 1.767 0.001 . 2 . . . . A 14 PRO HG3 . 30342 1 147 . 1 1 14 14 PRO HD2 H 1 3.570 0.002 . 2 . . . . A 14 PRO HD2 . 30342 1 148 . 1 1 14 14 PRO HD3 H 1 3.459 0.002 . 2 . . . . A 14 PRO HD3 . 30342 1 149 . 1 1 14 14 PRO CA C 13 63.719 0.000 . 1 . . . . A 14 PRO CA . 30342 1 150 . 1 1 14 14 PRO CB C 13 31.930 0.009 . 1 . . . . A 14 PRO CB . 30342 1 151 . 1 1 14 14 PRO CG C 13 27.216 0.010 . 1 . . . . A 14 PRO CG . 30342 1 152 . 1 1 14 14 PRO CD C 13 50.475 0.010 . 1 . . . . A 14 PRO CD . 30342 1 153 . 1 1 15 15 ASN H H 1 8.329 0.001 . 1 . . . . A 15 ASN H . 30342 1 154 . 1 1 15 15 ASN HA H 1 4.334 0.003 . 1 . . . . A 15 ASN HA . 30342 1 155 . 1 1 15 15 ASN HB2 H 1 2.634 0.003 . 2 . . . . A 15 ASN HB2 . 30342 1 156 . 1 1 15 15 ASN HB3 H 1 2.584 0.001 . 2 . . . . A 15 ASN HB3 . 30342 1 157 . 1 1 15 15 ASN HD21 H 1 6.741 0.001 . 2 . . . . A 15 ASN HD21 . 30342 1 158 . 1 1 15 15 ASN HD22 H 1 7.456 0.000 . 2 . . . . A 15 ASN HD22 . 30342 1 159 . 1 1 15 15 ASN CA C 13 53.351 0.000 . 1 . . . . A 15 ASN CA . 30342 1 160 . 1 1 15 15 ASN CB C 13 37.761 0.008 . 1 . . . . A 15 ASN CB . 30342 1 161 . 1 1 15 15 ASN N N 15 115.148 0.000 . 1 . . . . A 15 ASN N . 30342 1 162 . 1 1 15 15 ASN ND2 N 15 113.390 0.006 . 1 . . . . A 15 ASN ND2 . 30342 1 163 . 1 1 16 16 CYS H H 1 8.037 0.001 . 1 . . . . A 16 CYS H . 30342 1 164 . 1 1 16 16 CYS HA H 1 4.421 0.008 . 1 . . . . A 16 CYS HA . 30342 1 165 . 1 1 16 16 CYS HB2 H 1 2.989 0.001 . 2 . . . . A 16 CYS HB2 . 30342 1 166 . 1 1 16 16 CYS HB3 H 1 2.741 0.001 . 2 . . . . A 16 CYS HB3 . 30342 1 167 . 1 1 16 16 CYS CA C 13 53.632 0.000 . 1 . . . . A 16 CYS CA . 30342 1 168 . 1 1 16 16 CYS CB C 13 40.643 0.019 . 1 . . . . A 16 CYS CB . 30342 1 169 . 1 1 16 16 CYS N N 15 118.344 0.000 . 1 . . . . A 16 CYS N . 30342 1 170 . 1 1 17 17 GLY H H 1 8.399 0.001 . 1 . . . . A 17 GLY H . 30342 1 171 . 1 1 17 17 GLY HA2 H 1 3.687 0.001 . 2 . . . . A 17 GLY HA2 . 30342 1 172 . 1 1 17 17 GLY HA3 H 1 3.687 0.001 . 2 . . . . A 17 GLY HA3 . 30342 1 173 . 1 1 17 17 GLY CA C 13 44.918 0.000 . 1 . . . . A 17 GLY CA . 30342 1 174 . 1 1 17 17 GLY N N 15 112.340 0.000 . 1 . . . . A 17 GLY N . 30342 1 175 . 1 1 18 18 NH2 N N 15 107.477 0.000 . 1 . . . . A 18 NH2 N . 30342 1 176 . 1 1 18 18 NH2 HN1 H 1 6.950 0.000 . 1 . . . . A 18 NH2 HN1 . 30342 1 177 . 1 1 18 18 NH2 HN2 H 1 7.305 0.000 . 1 . . . . A 18 NH2 HN2 . 30342 1 stop_ save_ ######################### # Spectral peak lists # ######################### save_spectral_peak_list_1 _Spectral_peak_list.Sf_category spectral_peak_list _Spectral_peak_list.Sf_framecode spectral_peak_list_1 _Spectral_peak_list.Entry_ID 30342 _Spectral_peak_list.ID 1 _Spectral_peak_list.Sample_ID 1 _Spectral_peak_list.Sample_label $sample_1 _Spectral_peak_list.Sample_condition_list_ID 1 _Spectral_peak_list.Sample_condition_list_label $sample_conditions_1 _Spectral_peak_list.Experiment_ID 4 _Spectral_peak_list.Experiment_name '2D 1H-1H NOESY' _Spectral_peak_list.Experiment_class . _Spectral_peak_list.Experiment_type . _Spectral_peak_list.Number_of_spectral_dimensions 2 _Spectral_peak_list.Chemical_shift_list . _Spectral_peak_list.Assigned_chem_shift_list_ID . _Spectral_peak_list.Assigned_chem_shift_list_label . _Spectral_peak_list.Details . _Spectral_peak_list.Text_data_format text _Spectral_peak_list.Text_data . loop_ _Spectral_dim.ID _Spectral_dim.Axis_code _Spectral_dim.Spectrometer_frequency _Spectral_dim.Atom_type _Spectral_dim.Atom_isotope_number _Spectral_dim.Spectral_region _Spectral_dim.Magnetization_linkage_ID _Spectral_dim.Under_sampling_type _Spectral_dim.Sweep_width _Spectral_dim.Sweep_width_units _Spectral_dim.Value_first_point _Spectral_dim.Absolute_peak_positions _Spectral_dim.Acquisition _Spectral_dim.Center_frequency_offset _Spectral_dim.Encoding_code _Spectral_dim.Encoded_reduced_dimension_ID _Spectral_dim.Entry_ID _Spectral_dim.Spectral_peak_list_ID 1 . . H 1 H . . 16 ppm . . . 4.700 . . 30342 1 2 . . H 1 H . . 16 ppm . . . 4.700 . . 30342 1 stop_ loop_ _Peak.ID _Peak.Figure_of_merit _Peak.Restraint _Peak.Details _Peak.Entry_ID _Peak.Spectral_peak_list_ID 1 . . . 30342 1 2 . . . 30342 1 3 . . . 30342 1 4 . . . 30342 1 5 . . . 30342 1 6 . . . 30342 1 7 . . . 30342 1 8 . . . 30342 1 9 . . . 30342 1 10 . . . 30342 1 11 . . . 30342 1 12 . . . 30342 1 13 . . . 30342 1 14 . . . 30342 1 15 . . . 30342 1 16 . . . 30342 1 17 . . . 30342 1 18 . . . 30342 1 19 . . . 30342 1 20 . . . 30342 1 21 . . . 30342 1 22 . . . 30342 1 23 . . . 30342 1 24 . . . 30342 1 25 . . . 30342 1 26 . . . 30342 1 27 . . . 30342 1 28 . . . 30342 1 29 . . . 30342 1 30 . . . 30342 1 31 . . . 30342 1 32 . . . 30342 1 33 . . . 30342 1 34 . . . 30342 1 35 . . . 30342 1 36 . . . 30342 1 37 . . . 30342 1 38 . . . 30342 1 39 . . . 30342 1 40 . . . 30342 1 41 . . . 30342 1 42 . . . 30342 1 43 . . . 30342 1 44 . . . 30342 1 45 . . . 30342 1 46 . . . 30342 1 47 . . . 30342 1 48 . . . 30342 1 49 . . . 30342 1 50 . . . 30342 1 51 . . . 30342 1 52 . . . 30342 1 53 . . . 30342 1 54 . . . 30342 1 55 . . . 30342 1 56 . . . 30342 1 57 . . . 30342 1 58 . . . 30342 1 59 . . . 30342 1 60 . . . 30342 1 61 . . . 30342 1 62 . . . 30342 1 63 . . . 30342 1 64 . . . 30342 1 65 . . . 30342 1 66 . . . 30342 1 67 . . . 30342 1 68 . . . 30342 1 69 . . . 30342 1 70 . . . 30342 1 71 . . . 30342 1 72 . . . 30342 1 73 . . . 30342 1 74 . . . 30342 1 75 . . . 30342 1 76 . . . 30342 1 77 . . . 30342 1 78 . . . 30342 1 79 . . . 30342 1 80 . . . 30342 1 81 . . . 30342 1 82 . . . 30342 1 83 . . . 30342 1 84 . . . 30342 1 85 . . . 30342 1 86 . . . 30342 1 87 . . . 30342 1 88 . . . 30342 1 89 . . . 30342 1 90 . . . 30342 1 91 . . . 30342 1 92 . . . 30342 1 93 . . . 30342 1 94 . . . 30342 1 95 . . . 30342 1 96 . . . 30342 1 97 . . . 30342 1 98 . . . 30342 1 99 . . . 30342 1 100 . . . 30342 1 101 . . . 30342 1 102 . . . 30342 1 103 . . . 30342 1 104 . . . 30342 1 105 . . . 30342 1 106 . . . 30342 1 107 . . . 30342 1 108 . . . 30342 1 109 . . . 30342 1 110 . . . 30342 1 111 . . . 30342 1 112 . . . 30342 1 113 . . . 30342 1 114 . . . 30342 1 115 . . . 30342 1 116 . . . 30342 1 117 . . . 30342 1 118 . . . 30342 1 119 . . . 30342 1 120 . . . 30342 1 121 . . . 30342 1 122 . . . 30342 1 123 . . . 30342 1 124 . . . 30342 1 125 . . . 30342 1 126 . . . 30342 1 127 . . . 30342 1 128 . . . 30342 1 129 . . . 30342 1 130 . . . 30342 1 131 . . . 30342 1 132 . . . 30342 1 133 . . . 30342 1 134 . . . 30342 1 135 . . . 30342 1 136 . . . 30342 1 137 . . . 30342 1 138 . . . 30342 1 139 . . . 30342 1 140 . . . 30342 1 141 . . . 30342 1 142 . . . 30342 1 143 . . . 30342 1 144 . . . 30342 1 145 . . . 30342 1 146 . . . 30342 1 147 . . . 30342 1 148 . . . 30342 1 149 . . . 30342 1 150 . . . 30342 1 151 . . . 30342 1 152 . . . 30342 1 153 . . . 30342 1 154 . . . 30342 1 155 . . . 30342 1 156 . . . 30342 1 157 . . . 30342 1 158 . . . 30342 1 159 . . . 30342 1 160 . . . 30342 1 161 . . . 30342 1 162 . . . 30342 1 163 . . . 30342 1 164 . . . 30342 1 165 . . . 30342 1 166 . . . 30342 1 167 . . . 30342 1 168 . . . 30342 1 169 . . . 30342 1 170 . . . 30342 1 171 . . . 30342 1 172 . . . 30342 1 173 . . . 30342 1 174 . . . 30342 1 175 . . . 30342 1 176 . . . 30342 1 177 . . . 30342 1 178 . . . 30342 1 179 . . . 30342 1 180 . . . 30342 1 181 . . . 30342 1 182 . . . 30342 1 183 . . . 30342 1 184 . . . 30342 1 185 . . . 30342 1 186 . . . 30342 1 187 . . . 30342 1 188 . . . 30342 1 189 . . . 30342 1 190 . . . 30342 1 191 . . . 30342 1 192 . . . 30342 1 193 . . . 30342 1 194 . . . 30342 1 195 . . . 30342 1 196 . . . 30342 1 197 . . . 30342 1 198 . . . 30342 1 199 . . . 30342 1 200 . . . 30342 1 201 . . . 30342 1 202 . . . 30342 1 203 . . . 30342 1 204 . . . 30342 1 205 . . . 30342 1 206 . . . 30342 1 207 . . . 30342 1 208 . . . 30342 1 209 . . . 30342 1 210 . . . 30342 1 211 . . . 30342 1 212 . . . 30342 1 213 . . . 30342 1 214 . . . 30342 1 215 . . . 30342 1 216 . . . 30342 1 217 . . . 30342 1 218 . . . 30342 1 219 . . . 30342 1 220 . . . 30342 1 221 . . . 30342 1 222 . . . 30342 1 223 . . . 30342 1 224 . . . 30342 1 225 . . . 30342 1 226 . . . 30342 1 227 . . . 30342 1 228 . . . 30342 1 229 . . . 30342 1 230 . . . 30342 1 231 . . . 30342 1 232 . . . 30342 1 233 . . . 30342 1 234 . . . 30342 1 235 . . . 30342 1 236 . . . 30342 1 237 . . . 30342 1 238 . . . 30342 1 239 . . . 30342 1 240 . . . 30342 1 241 . . . 30342 1 242 . . . 30342 1 243 . . . 30342 1 244 . . . 30342 1 245 . . . 30342 1 246 . . . 30342 1 247 . . . 30342 1 248 . . . 30342 1 stop_ loop_ _Peak_general_char.Peak_ID _Peak_general_char.Intensity_val _Peak_general_char.Intensity_val_err _Peak_general_char.Measurement_method _Peak_general_char.Entry_ID _Peak_general_char.Spectral_peak_list_ID 1 0.0 . volume 30342 1 2 0.0 . volume 30342 1 3 0.0 . volume 30342 1 4 0.0 . volume 30342 1 5 0.0 . volume 30342 1 6 0.0 . volume 30342 1 7 0.0 . volume 30342 1 8 0.0 . volume 30342 1 9 0.0 . volume 30342 1 10 0.0 . volume 30342 1 11 0.0 . volume 30342 1 12 0.0 . volume 30342 1 13 0.0 . volume 30342 1 14 0.0 . volume 30342 1 15 0.0 . volume 30342 1 16 0.0 . volume 30342 1 17 0.0 . volume 30342 1 18 0.0 . volume 30342 1 19 0.0 . volume 30342 1 20 0.0 . volume 30342 1 21 0.0 . volume 30342 1 22 0.0 . volume 30342 1 23 0.0 . volume 30342 1 24 0.0 . volume 30342 1 25 0.0 . volume 30342 1 26 0.0 . volume 30342 1 27 0.0 . volume 30342 1 28 0.0 . volume 30342 1 29 0.0 . volume 30342 1 30 0.0 . volume 30342 1 31 0.0 . volume 30342 1 32 0.0 . volume 30342 1 33 0.0 . volume 30342 1 34 0.0 . volume 30342 1 35 0.0 . volume 30342 1 36 0.0 . volume 30342 1 37 0.0 . volume 30342 1 38 0.0 . volume 30342 1 39 0.0 . volume 30342 1 40 0.0 . volume 30342 1 41 0.0 . volume 30342 1 42 0.0 . volume 30342 1 43 0.0 . volume 30342 1 44 0.0 . volume 30342 1 45 0.0 . volume 30342 1 46 0.0 . volume 30342 1 47 0.0 . volume 30342 1 48 0.0 . volume 30342 1 49 0.0 . volume 30342 1 50 0.0 . volume 30342 1 51 0.0 . volume 30342 1 52 0.0 . volume 30342 1 53 0.0 . volume 30342 1 54 0.0 . volume 30342 1 55 0.0 . volume 30342 1 56 0.0 . volume 30342 1 57 0.0 . volume 30342 1 58 0.0 . volume 30342 1 59 0.0 . volume 30342 1 60 0.0 . volume 30342 1 61 0.0 . volume 30342 1 62 0.0 . volume 30342 1 63 0.0 . volume 30342 1 64 0.0 . volume 30342 1 65 0.0 . volume 30342 1 66 0.0 . volume 30342 1 67 0.0 . volume 30342 1 68 0.0 . volume 30342 1 69 0.0 . volume 30342 1 70 0.0 . volume 30342 1 71 0.0 . volume 30342 1 72 0.0 . volume 30342 1 73 0.0 . volume 30342 1 74 0.0 . volume 30342 1 75 0.0 . volume 30342 1 76 0.0 . volume 30342 1 77 0.0 . volume 30342 1 78 0.0 . volume 30342 1 79 0.0 . volume 30342 1 80 0.0 . volume 30342 1 81 0.0 . volume 30342 1 82 0.0 . volume 30342 1 83 0.0 . volume 30342 1 84 0.0 . volume 30342 1 85 0.0 . volume 30342 1 86 0.0 . volume 30342 1 87 0.0 . volume 30342 1 88 0.0 . volume 30342 1 89 0.0 . volume 30342 1 90 0.0 . volume 30342 1 91 0.0 . volume 30342 1 92 0.0 . volume 30342 1 93 0.0 . volume 30342 1 94 0.0 . volume 30342 1 95 0.0 . volume 30342 1 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0.0 . volume 30342 1 177 0.0 . volume 30342 1 178 0.0 . volume 30342 1 179 0.0 . volume 30342 1 180 0.0 . volume 30342 1 181 0.0 . volume 30342 1 182 0.0 . volume 30342 1 183 0.0 . volume 30342 1 184 0.0 . volume 30342 1 185 0.0 . volume 30342 1 186 0.0 . volume 30342 1 187 0.0 . volume 30342 1 188 0.0 . volume 30342 1 189 0.0 . volume 30342 1 190 0.0 . volume 30342 1 191 0.0 . volume 30342 1 192 0.0 . volume 30342 1 193 0.0 . volume 30342 1 194 0.0 . volume 30342 1 195 0.0 . volume 30342 1 196 0.0 . volume 30342 1 197 0.0 . volume 30342 1 198 0.0 . volume 30342 1 199 0.0 . volume 30342 1 200 0.0 . volume 30342 1 201 0.0 . volume 30342 1 202 0.0 . volume 30342 1 203 0.0 . volume 30342 1 204 0.0 . volume 30342 1 205 0.0 . volume 30342 1 206 0.0 . volume 30342 1 207 0.0 . volume 30342 1 208 0.0 . volume 30342 1 209 0.0 . volume 30342 1 210 0.0 . volume 30342 1 211 0.0 . volume 30342 1 212 0.0 . volume 30342 1 213 0.0 . volume 30342 1 214 0.0 . volume 30342 1 215 0.0 . volume 30342 1 216 0.0 . volume 30342 1 217 0.0 . volume 30342 1 218 0.0 . volume 30342 1 219 0.0 . volume 30342 1 220 0.0 . volume 30342 1 221 0.0 . volume 30342 1 222 0.0 . volume 30342 1 223 0.0 . volume 30342 1 224 0.0 . volume 30342 1 225 0.0 . volume 30342 1 226 0.0 . volume 30342 1 227 0.0 . volume 30342 1 228 0.0 . volume 30342 1 229 0.0 . volume 30342 1 230 0.0 . volume 30342 1 231 0.0 . volume 30342 1 232 0.0 . volume 30342 1 233 0.0 . volume 30342 1 234 0.0 . volume 30342 1 235 0.0 . volume 30342 1 236 0.0 . volume 30342 1 237 106800.0 . volume 30342 1 238 71160.0 . volume 30342 1 239 44500.0 . volume 30342 1 240 38090.0 . volume 30342 1 241 31210.0 . volume 30342 1 242 321300.0 . volume 30342 1 243 1196000.0 . volume 30342 1 244 344700.0 . volume 30342 1 245 898100.0 . volume 30342 1 246 294400.0 . volume 30342 1 247 1186000.0 . volume 30342 1 248 398900.0 . volume 30342 1 stop_ loop_ _Peak_char.Peak_ID _Peak_char.Spectral_dim_ID _Peak_char.Chem_shift_val _Peak_char.Chem_shift_val_err _Peak_char.Line_width_val _Peak_char.Line_width_val_err _Peak_char.Phase_val _Peak_char.Phase_val_err _Peak_char.Decay_rate_val _Peak_char.Decay_rate_val_err _Peak_char.Coupling_pattern _Peak_char.Bounding_box_upper_val _Peak_char.Bounding_box_lower_val _Peak_char.Bounding_box_range_val _Peak_char.Details _Peak_char.Derivation_method_ID _Peak_char.Entry_ID _Peak_char.Spectral_peak_list_ID 1 1 4.256 . . . . . . . . . . . . . 30342 1 1 2 8.703 . . . . . . . . . . . . . 30342 1 2 1 3.876 . . . . . . . . . . . . . 30342 1 2 2 8.703 . . . . . . . . . . . . . 30342 1 3 1 3.812 . . . . . . . . . . . . . 30342 1 3 2 8.639 . . . . . . . . . . . . . 30342 1 4 1 4.186 . . . . . . . . . . . . . 30342 1 4 2 8.642 . . . . . . . . . . . . . 30342 1 5 1 4.553 . . . . . . . . . . . . . 30342 1 5 2 8.625 . . . . . . . . . . . . . 30342 1 6 1 4.935 . . . . . . . . . . . . . 30342 1 6 2 8.626 . . . . . . . . . . . . . 30342 1 7 1 2.766 . . . . . . . . . . . . . 30342 1 7 2 8.628 . . . . . . . . . . . . . 30342 1 8 1 2.683 . . . . . . . . . . . . . 30342 1 8 2 8.626 . . . . . . . . . . . . . 30342 1 9 1 0.958 . . . . . . . . . . . . . 30342 1 9 2 8.636 . . . . . . . . . . . . . 30342 1 10 1 1.612 . . . . . . . . . . . . . 30342 1 10 2 8.625 . . . . . . . . . . . . . 30342 1 11 1 1.495 . . . . . . . . . . . . . 30342 1 11 2 8.625 . . . . . . . . . . . . . 30342 1 12 1 1.419 . . . . . . . . . . . . . 30342 1 12 2 8.625 . . . . . . . . . . . . . 30342 1 13 1 8.476 . . . . . . . . . . . . . 30342 1 13 2 8.631 . . . . . . . . . . . . . 30342 1 14 1 8.702 . . . . . . . . . . . . . 30342 1 14 2 4.252 . . . . . . . . . . . . . 30342 1 15 1 8.642 . . . . . . . . . . . . . 30342 1 15 2 4.183 . . . . . . . . . . . . . 30342 1 16 1 8.704 . . . . . . . . . . . . . 30342 1 16 2 3.872 . . . . . . . . . . . . . 30342 1 17 1 8.636 . . . . . . . . . . . . . 30342 1 17 2 3.809 . . . . . . . . . . . . . 30342 1 18 1 8.642 . . . . . . . . . . . . . 30342 1 18 2 2.965 . . . . . . . . . . . . . 30342 1 19 1 8.642 . . . . . . . . . . . . . 30342 1 19 2 2.821 . . . . . . . . . . . . . 30342 1 20 1 8.636 . . . . . . . . . . . . . 30342 1 20 2 2.746 . . . . . . . . . . . . . 30342 1 21 1 8.626 . . . . . . . . . . . . . 30342 1 21 2 2.683 . . . . . . . . . . . . . 30342 1 22 1 8.632 . . . . . . . . . . . . . 30342 1 22 2 0.958 . . . . . . . . . . . . . 30342 1 23 1 8.625 . . . . . . . . . . . . . 30342 1 23 2 1.606 . . . . . . . . . . . . . 30342 1 24 1 8.625 . . . . . . . . . . . . . 30342 1 24 2 1.5 . . . . . . . . . . . . . 30342 1 25 1 8.62 . . . . . . . . . . . . . 30342 1 25 2 1.416 . . . . . . . . . . . . . 30342 1 26 1 4.948 . . . . . . . . . . . . . 30342 1 26 2 8.525 . . . . . . . . . . . . . 30342 1 27 1 4.292 . . . . . . . . . . . . . 30342 1 27 2 8.518 . . . . . . . . . . . . . 30342 1 28 1 3.557 . . . . . . . . . . . . . 30342 1 28 2 8.528 . . . . . . . . . . . . . 30342 1 29 1 3.612 . . . . . . . . . . . . . 30342 1 29 2 8.528 . . . . . . . . . . . . . 30342 1 30 1 2.776 . . . . . . . . . . . . . 30342 1 30 2 8.519 . . . . . . . . . . . . . 30342 1 31 1 2.686 . . . . . . . . . . . . . 30342 1 31 2 8.519 . . . . . . . . . . . . . 30342 1 32 1 3.449 . . . . . . . . . . . . . 30342 1 32 2 8.447 . . . . . . . . . . . . . 30342 1 33 1 3.882 . . . . . . . . . . . . . 30342 1 33 2 8.448 . . . . . . . . . . . . . 30342 1 34 1 3.817 . . . . . . . . . . . . . 30342 1 34 2 8.469 . . . . . . . . . . . . . 30342 1 35 1 4.183 . . . . . . . . . . . . . 30342 1 35 2 8.465 . . . . . . . . . . . . . 30342 1 36 1 4.455 . . . . . . . . . . . . . 30342 1 36 2 8.47 . . . . . . . . . . . . . 30342 1 37 1 7.832 . . . . . . . . . . . . . 30342 1 37 2 8.519 . . . . . . . . . . . . . 30342 1 38 1 7.831 . . . . . . . . . . . . . 30342 1 38 2 8.447 . . . . . . . . . . . . . 30342 1 39 1 8.627 . . . . . . . . . . . . . 30342 1 39 2 8.468 . . . . . . . . . . . . . 30342 1 40 1 8.71 . . . . . . . . . . . . . 30342 1 40 2 8.449 . . . . . . . . . . . . . 30342 1 41 1 8.452 . . . . . . . . . . . . . 30342 1 41 2 7.83 . . . . . . . . . . . . . 30342 1 42 1 8.522 . . . . . . . . . . . . . 30342 1 42 2 7.827 . . . . . . . . . . . . . 30342 1 43 1 8.465 . . . . . . . . . . . . . 30342 1 43 2 4.182 . . . . . . . . . . . . . 30342 1 44 1 8.517 . . . . . . . . . . . . . 30342 1 44 2 4.289 . . . . . . . . . . . . . 30342 1 45 1 8.449 . . . . . . . . . . . . . 30342 1 45 2 3.886 . . . . . . . . . . . . . 30342 1 46 1 8.471 . . . . . . . . . . . . . 30342 1 46 2 3.808 . . . . . . . . . . . . . 30342 1 47 1 8.447 . . . . . . . . . . . . . 30342 1 47 2 3.462 . . . . . . . . . . . . . 30342 1 48 1 8.449 . . . . . . . . . . . . . 30342 1 48 2 3.433 . . . . . . . . . . . . . 30342 1 49 1 8.529 . . . . . . . . . . . . . 30342 1 49 2 3.555 . . . . . . . . . . . . . 30342 1 50 1 8.526 . . . . . . . . . . . . . 30342 1 50 2 3.611 . . . . . . . . . . . . . 30342 1 51 1 8.474 . . . . . . . . . . . . . 30342 1 51 2 0.957 . . . . . . . . . . . . . 30342 1 52 1 1.142 . . . . . . . . . . . . . 30342 1 52 2 8.466 . . . . . . . . . . . . . 30342 1 53 1 0.957 . . . . . . . . . . . . . 30342 1 53 2 8.469 . . . . . . . . . . . . . 30342 1 54 1 1.597 . . . . . . . . . . . . . 30342 1 54 2 8.453 . . . . . . . . . . . . . 30342 1 55 1 1.48 . . . . . . . . . . . . . 30342 1 55 2 8.47 . . . . . . . . . . . . . 30342 1 56 1 1.622 . . . . . . . . . . . . . 30342 1 56 2 8.517 . . . . . . . . . . . . . 30342 1 57 1 1.694 . . . . . . . . . . . . . 30342 1 57 2 8.451 . . . . . . . . . . . . . 30342 1 58 1 1.107 . . . . . . . . . . . . . 30342 1 58 2 8.371 . . . . . . . . . . . . . 30342 1 59 1 1.491 . . . . . . . . . . . . . 30342 1 59 2 8.37 . . . . . . . . . . . . . 30342 1 60 1 1.656 . . . . . . . . . . . . . 30342 1 60 2 8.329 . . . . . . . . . . . . . 30342 1 61 1 1.567 . . . . . . . . . . . . . 30342 1 61 2 8.328 . . . . . . . . . . . . . 30342 1 62 1 1.812 . . . . . . . . . . . . . 30342 1 62 2 8.328 . . . . . . . . . . . . . 30342 1 63 1 2.052 . . . . . . . . . . . . . 30342 1 63 2 8.329 . . . . . . . . . . . . . 30342 1 64 1 1.204 . . . . . . . . . . . . . 30342 1 64 2 8.328 . . . . . . . . . . . . . 30342 1 65 1 1.146 . . . . . . . . . . . . . 30342 1 65 2 8.37 . . . . . . . . . . . . . 30342 1 66 1 1.471 . . . . . . . . . . . . . 30342 1 66 2 8.369 . . . . . . . . . . . . . 30342 1 67 1 2.656 . . . . . . . . . . . . . 30342 1 67 2 8.329 . . . . . . . . . . . . . 30342 1 68 1 2.591 . . . . . . . . . . . . . 30342 1 68 2 8.328 . . . . . . . . . . . . . 30342 1 69 1 2.695 . . . . . . . . . . . . . 30342 1 69 2 8.37 . . . . . . . . . . . . . 30342 1 70 1 3.102 . . . . . . . . . . . . . 30342 1 70 2 8.371 . . . . . . . . . . . . . 30342 1 71 1 3.463 . . . . . . . . . . . . . 30342 1 71 2 8.329 . . . . . . . . . . . . . 30342 1 72 1 4.342 . . . . . . . . . . . . . 30342 1 72 2 8.327 . . . . . . . . . . . . . 30342 1 73 1 4.103 . . . . . . . . . . . . . 30342 1 73 2 8.328 . . . . . . . . . . . . . 30342 1 74 1 4.466 . . . . . . . . . . . . . 30342 1 74 2 8.372 . . . . . . . . . . . . . 30342 1 75 1 1.364 . . . . . . . . . . . . . 30342 1 75 2 7.974 . . . . . . . . . . . . . 30342 1 76 1 1.197 . . . . . . . . . . . . . 30342 1 76 2 7.974 . . . . . . . . . . . . . 30342 1 77 1 1.416 . . . . . . . . . . . . . 30342 1 77 2 7.975 . . . . . . . . . . . . . 30342 1 78 1 1.583 . . . . . . . . . . . . . 30342 1 78 2 7.974 . . . . . . . . . . . . . 30342 1 79 1 2.058 . . . . . . . . . . . . . 30342 1 79 2 7.973 . . . . . . . . . . . . . 30342 1 80 1 2.748 . . . . . . . . . . . . . 30342 1 80 2 7.974 . . . . . . . . . . . . . 30342 1 81 1 2.743 . . . . . . . . . . . . . 30342 1 81 2 8.036 . . . . . . . . . . . . . 30342 1 82 1 2.99 . . . . . . . . . . . . . 30342 1 82 2 8.036 . . . . . . . . . . . . . 30342 1 83 1 3.573 . . . . . . . . . . . . . 30342 1 83 2 7.975 . . . . . . . . . . . . . 30342 1 84 1 3.452 . . . . . . . . . . . . . 30342 1 84 2 7.974 . . . . . . . . . . . . . 30342 1 85 1 1.329 . . . . . . . . . . . . . 30342 1 85 2 7.833 . . . . . . . . . . . . . 30342 1 86 1 1.405 . . . . . . . . . . . . . 30342 1 86 2 7.833 . . . . . . . . . . . . . 30342 1 87 1 1.572 . . . . . . . . . . . . . 30342 1 87 2 7.833 . . . . . . . . . . . . . 30342 1 88 1 1.624 . . . . . . . . . . . . . 30342 1 88 2 7.833 . . . . . . . . . . . . . 30342 1 89 1 3.448 . . . . . . . . . . . . . 30342 1 89 2 7.83 . . . . . . . . . . . . . 30342 1 90 1 3.889 . . . . . . . . . . . . . 30342 1 90 2 7.83 . . . . . . . . . . . . . 30342 1 91 1 4.294 . . . . . . . . . . . . . 30342 1 91 2 7.831 . . . . . . . . . . . . . 30342 1 92 1 4.43 . . . . . . . . . . . . . 30342 1 92 2 7.974 . . . . . . . . . . . . . 30342 1 93 1 4.278 . . . . . . . . . . . . . 30342 1 93 2 7.974 . . . . . . . . . . . . . 30342 1 94 1 4.136 . . . . . . . . . . . . . 30342 1 94 2 8.033 . . . . . . . . . . . . . 30342 1 95 1 4.436 . . . . . . . . . . . . . 30342 1 95 2 8.037 . . . . . . . . . . . . . 30342 1 96 1 4.341 . . . . . . . . . . . . . 30342 1 96 2 8.036 . . . . . . . . . . . . . 30342 1 97 1 3.571 . . . . . . . . . . . . . 30342 1 97 2 8.327 . . . . . . . . . . . . . 30342 1 98 1 2.988 . . . . . . . . . . . . . 30342 1 98 2 8.399 . . . . . . . . . . . . . 30342 1 99 1 2.748 . . . . . . . . . . . . . 30342 1 99 2 8.4 . . . . . . . . . . . . . 30342 1 100 1 4.435 . . . . . . . . . . . . . 30342 1 100 2 8.399 . . . . . . . . . . . . . 30342 1 101 1 3.689 . . . . . . . . . . . . . 30342 1 101 2 8.396 . . . . . . . . . . . . . 30342 1 102 1 8.368 . . . . . . . . . . . . . 30342 1 102 2 7.973 . . . . . . . . . . . . . 30342 1 103 1 7.305 . . . . . . . . . . . . . 30342 1 103 2 6.949 . . . . . . . . . . . . . 30342 1 104 1 7.464 . . . . . . . . . . . . . 30342 1 104 2 6.889 . . . . . . . . . . . . . 30342 1 105 1 6.95 . . . . . . . . . . . . . 30342 1 105 2 7.303 . . . . . . . . . . . . . 30342 1 106 1 6.743 . . . . . . . . . . . . . 30342 1 106 2 7.455 . . . . . . . . . . . . . 30342 1 107 1 6.889 . . . . . . . . . . . . . 30342 1 107 2 7.462 . . . . . . . . . . . . . 30342 1 108 1 7.456 . . . . . . . . . . . . . 30342 1 108 2 6.74 . . . . . . . . . . . . . 30342 1 109 1 2.583 . . . . . . . . . . . . . 30342 1 109 2 7.456 . . . . . . . . . . . . . 30342 1 110 1 2.594 . . . . . . . . . . . . . 30342 1 110 2 6.741 . . . . . . . . . . . . . 30342 1 111 1 2.96 . . . . . . . . . . . . . 30342 1 111 2 7.017 . . . . . . . . . . . . . 30342 1 112 1 4.698 . . . . . . . . . . . . . 30342 1 112 2 7.024 . . . . . . . . . . . . . 30342 1 113 1 3.683 . . . . . . . . . . . . . 30342 1 113 2 7.3 . . . . . . . . . . . . . 30342 1 114 1 3.684 . . . . . . . . . . . . . 30342 1 114 2 6.95 . . . . . . . . . . . . . 30342 1 115 1 2.657 . . . . . . . . . . . . . 30342 1 115 2 7.453 . . . . . . . . . . . . . 30342 1 116 1 7.302 . . . . . . . . . . . . . 30342 1 116 2 3.683 . . . . . . . . . . . . . 30342 1 117 1 6.951 . . . . . . . . . . . . . 30342 1 117 2 3.684 . . . . . . . . . . . . . 30342 1 118 1 8.328 . . . . . . . . . . . . . 30342 1 118 2 4.338 . . . . . . . . . . . . . 30342 1 119 1 7.976 . . . . . . . . . . . . . 30342 1 119 2 4.276 . . . . . . . . . . . . . 30342 1 120 1 8.33 . . . . . . . . . . . . . 30342 1 120 2 4.1 . . . . . . . . . . . . . 30342 1 121 1 7.978 . . . . . . . . . . . . . 30342 1 121 2 1.561 . . . . . . . . . . . . . 30342 1 122 1 7.977 . . . . . . . . . . . . . 30342 1 122 2 1.364 . . . . . . . . . . . . . 30342 1 123 1 7.976 . . . . . . . . . . . . . 30342 1 123 2 1.198 . . . . . . . . . . . . . 30342 1 124 1 8.329 . . . . . . . . . . . . . 30342 1 124 2 1.193 . . . . . . . . . . . . . 30342 1 125 1 8.328 . . . . . . . . . . . . . 30342 1 125 2 1.661 . . . . . . . . . . . . . 30342 1 126 1 8.331 . . . . . . . . . . . . . 30342 1 126 2 1.564 . . . . . . . . . . . . . 30342 1 127 1 8.329 . . . . . . . . . . . . . 30342 1 127 2 2.048 . . . . . . . . . . . . . 30342 1 128 1 7.974 . . . . . . . . . . . . . 30342 1 128 2 2.055 . . . . . . . . . . . . . 30342 1 129 1 7.971 . . . . . . . . . . . . . 30342 1 129 2 1.822 . . . . . . . . . . . . . 30342 1 130 1 7.971 . . . . . . . . . . . . . 30342 1 130 2 1.742 . . . . . . . . . . . . . 30342 1 131 1 7.978 . . . . . . . . . . . . . 30342 1 131 2 1.614 . . . . . . . . . . . . . 30342 1 132 1 7.835 . . . . . . . . . . . . . 30342 1 132 2 1.627 . . . . . . . . . . . . . 30342 1 133 1 7.835 . . . . . . . . . . . . . 30342 1 133 2 1.574 . . . . . . . . . . . . . 30342 1 134 1 7.845 . . . . . . . . . . . . . 30342 1 134 2 1.409 . . . . . . . . . . . . . 30342 1 135 1 7.837 . . . . . . . . . . . . . 30342 1 135 2 1.328 . . . . . . . . . . . . . 30342 1 136 1 8.332 . . . . . . . . . . . . . 30342 1 136 2 2.631 . . . . . . . . . . . . . 30342 1 137 1 8.333 . . . . . . . . . . . . . 30342 1 137 2 2.586 . . . . . . . . . . . . . 30342 1 138 1 7.982 . . . . . . . . . . . . . 30342 1 138 2 3.567 . . . . . . . . . . . . . 30342 1 139 1 7.974 . . . . . . . . . . . . . 30342 1 139 2 3.459 . . . . . . . . . . . . . 30342 1 140 1 8.031 . . . . . . . . . . . . . 30342 1 140 2 4.135 . . . . . . . . . . . . . 30342 1 141 1 7.833 . . . . . . . . . . . . . 30342 1 141 2 3.902 . . . . . . . . . . . . . 30342 1 142 1 7.833 . . . . . . . . . . . . . 30342 1 142 2 3.87 . . . . . . . . . . . . . 30342 1 143 1 7.834 . . . . . . . . . . . . . 30342 1 143 2 3.46 . . . . . . . . . . . . . 30342 1 144 1 7.834 . . . . . . . . . . . . . 30342 1 144 2 3.43 . . . . . . . . . . . . . 30342 1 145 1 8.399 . . . . . . . . . . . . . 30342 1 145 2 3.685 . . . . . . . . . . . . . 30342 1 146 1 8.515 . . . . . . . . . . . . . 30342 1 146 2 2.761 . . . . . . . . . . . . . 30342 1 147 1 8.518 . . . . . . . . . . . . . 30342 1 147 2 2.68 . . . . . . . . . . . . . 30342 1 148 1 8.519 . . . . . . . . . . . . . 30342 1 148 2 2.805 . . . . . . . . . . . . . 30342 1 149 1 2.059 . . . . . . . . . . . . . 30342 1 149 2 4.279 . . . . . . . . . . . . . 30342 1 150 1 2.054 . . . . . . . . . . . . . 30342 1 150 2 4.102 . . . . . . . . . . . . . 30342 1 151 1 0.957 . . . . . . . . . . . . . 30342 1 151 2 4.183 . . . . . . . . . . . . . 30342 1 152 1 0.957 . . . . . . . . . . . . . 30342 1 152 2 3.806 . . . . . . . . . . . . . 30342 1 153 1 1.145 . . . . . . . . . . . . . 30342 1 153 2 3.872 . . . . . . . . . . . . . 30342 1 154 1 1.429 . . . . . . . . . . . . . 30342 1 154 2 3.816 . . . . . . . . . . . . . 30342 1 155 1 1.693 . . . . . . . . . . . . . 30342 1 155 2 3.822 . . . . . . . . . . . . . 30342 1 156 1 1.689 . . . . . . . . . . . . . 30342 1 156 2 3.872 . . . . . . . . . . . . . 30342 1 157 1 1.603 . . . . . . . . . . . . . 30342 1 157 2 3.87 . . . . . . . . . . . . . 30342 1 158 1 2.589 . . . . . . . . . . . . . 30342 1 158 2 4.337 . . . . . . . . . . . . . 30342 1 159 1 2.989 . . . . . . . . . . . . . 30342 1 159 2 4.423 . . . . . . . . . . . . . 30342 1 160 1 2.743 . . . . . . . . . . . . . 30342 1 160 2 4.428 . . . . . . . . . . . . . 30342 1 161 1 3.571 . . . . . . . . . . . . . 30342 1 161 2 4.408 . . . . . . . . . . . . . 30342 1 162 1 3.456 . . . . . . . . . . . . . 30342 1 162 2 4.407 . . . . . . . . . . . . . 30342 1 163 1 3.603 . . . . . . . . . . . . . 30342 1 163 2 4.257 . . . . . . . . . . . . . 30342 1 164 1 3.809 . . . . . . . . . . . . . 30342 1 164 2 4.184 . . . . . . . . . . . . . 30342 1 165 1 3.636 . . . . . . . . . . . . . 30342 1 165 2 4.188 . . . . . . . . . . . . . 30342 1 166 1 3.451 . . . . . . . . . . . . . 30342 1 166 2 3.904 . . . . . . . . . . . . . 30342 1 167 1 3.451 . . . . . . . . . . . . . 30342 1 167 2 3.872 . . . . . . . . . . . . . 30342 1 168 1 1.196 . . . . . . . . . . . . . 30342 1 168 2 3.562 . . . . . . . . . . . . . 30342 1 169 1 2.054 . . . . . . . . . . . . . 30342 1 169 2 3.573 . . . . . . . . . . . . . 30342 1 170 1 1.781 . . . . . . . . . . . . . 30342 1 170 2 3.57 . . . . . . . . . . . . . 30342 1 171 1 1.615 . . . . . . . . . . . . . 30342 1 171 2 3.573 . . . . . . . . . . . . . 30342 1 172 1 1.502 . . . . . . . . . . . . . 30342 1 172 2 3.574 . . . . . . . . . . . . . 30342 1 173 1 1.417 . . . . . . . . . . . . . 30342 1 173 2 3.572 . . . . . . . . . . . . . 30342 1 174 1 1.198 . . . . . . . . . . . . . 30342 1 174 2 3.46 . . . . . . . . . . . . . 30342 1 175 1 1.5 . . . . . . . . . . . . . 30342 1 175 2 3.418 . . . . . . . . . . . . . 30342 1 176 1 1.422 . . . . . . . . . . . . . 30342 1 176 2 3.419 . . . . . . . . . . . . . 30342 1 177 1 1.616 . . . . . . . . . . . . . 30342 1 177 2 3.419 . . . . . . . . . . . . . 30342 1 178 1 1.766 . . . . . . . . . . . . . 30342 1 178 2 3.418 . . . . . . . . . . . . . 30342 1 179 1 1.83 . . . . . . . . . . . . . 30342 1 179 2 3.416 . . . . . . . . . . . . . 30342 1 180 1 2.054 . . . . . . . . . . . . . 30342 1 180 2 3.444 . . . . . . . . . . . . . 30342 1 181 1 2.053 . . . . . . . . . . . . . 30342 1 181 2 3.424 . . . . . . . . . . . . . 30342 1 182 1 1.787 . . . . . . . . . . . . . 30342 1 182 2 3.453 . . . . . . . . . . . . . 30342 1 183 1 1.655 . . . . . . . . . . . . . 30342 1 183 2 3.455 . . . . . . . . . . . . . 30342 1 184 1 1.596 . . . . . . . . . . . . . 30342 1 184 2 3.458 . . . . . . . . . . . . . 30342 1 185 1 1.437 . . . . . . . . . . . . . 30342 1 185 2 3.458 . . . . . . . . . . . . . 30342 1 186 1 1.363 . . . . . . . . . . . . . 30342 1 186 2 3.46 . . . . . . . . . . . . . 30342 1 187 1 4.255 . . . . . . . . . . . . . 30342 1 187 2 3.554 . . . . . . . . . . . . . 30342 1 188 1 4.253 . . . . . . . . . . . . . 30342 1 188 2 3.607 . . . . . . . . . . . . . 30342 1 189 1 4.412 . . . . . . . . . . . . . 30342 1 189 2 3.566 . . . . . . . . . . . . . 30342 1 190 1 4.412 . . . . . . . . . . . . . 30342 1 190 2 3.46 . . . . . . . . . . . . . 30342 1 191 1 4.551 . . . . . . . . . . . . . 30342 1 191 2 3.418 . . . . . . . . . . . . . 30342 1 192 1 4.55 . . . . . . . . . . . . . 30342 1 192 2 3.577 . . . . . . . . . . . . . 30342 1 193 1 3.889 . . . . . . . . . . . . . 30342 1 193 2 3.461 . . . . . . . . . . . . . 30342 1 194 1 3.889 . . . . . . . . . . . . . 30342 1 194 2 3.433 . . . . . . . . . . . . . 30342 1 195 1 4.469 . . . . . . . . . . . . . 30342 1 195 2 3.091 . . . . . . . . . . . . . 30342 1 196 1 4.959 . . . . . . . . . . . . . 30342 1 196 2 2.823 . . . . . . . . . . . . . 30342 1 197 1 4.94 . . . . . . . . . . . . . 30342 1 197 2 2.753 . . . . . . . . . . . . . 30342 1 198 1 4.933 . . . . . . . . . . . . . 30342 1 198 2 2.681 . . . . . . . . . . . . . 30342 1 199 1 4.342 . . . . . . . . . . . . . 30342 1 199 2 2.629 . . . . . . . . . . . . . 30342 1 200 1 4.34 . . . . . . . . . . . . . 30342 1 200 2 2.584 . . . . . . . . . . . . . 30342 1 201 1 4.465 . . . . . . . . . . . . . 30342 1 201 2 2.819 . . . . . . . . . . . . . 30342 1 202 1 4.438 . . . . . . . . . . . . . 30342 1 202 2 2.748 . . . . . . . . . . . . . 30342 1 203 1 4.451 . . . . . . . . . . . . . 30342 1 203 2 4.275 . . . . . . . . . . . . . 30342 1 204 1 1.781 . . . . . . . . . . . . . 30342 1 204 2 4.1 . . . . . . . . . . . . . 30342 1 205 1 1.66 . . . . . . . . . . . . . 30342 1 205 2 4.101 . . . . . . . . . . . . . 30342 1 206 1 1.423 . . . . . . . . . . . . . 30342 1 206 2 3.866 . . . . . . . . . . . . . 30342 1 207 1 3.576 . . . . . . . . . . . . . 30342 1 207 2 2.049 . . . . . . . . . . . . . 30342 1 208 1 3.435 . . . . . . . . . . . . . 30342 1 208 2 2.048 . . . . . . . . . . . . . 30342 1 209 1 4.279 . . . . . . . . . . . . . 30342 1 209 2 2.055 . . . . . . . . . . . . . 30342 1 210 1 4.105 . . . . . . . . . . . . . 30342 1 210 2 2.05 . . . . . . . . . . . . . 30342 1 211 1 1.644 . . . . . . . . . . . . . 30342 1 211 2 2.055 . . . . . . . . . . . . . 30342 1 212 1 4.553 . . . . . . . . . . . . . 30342 1 212 2 1.824 . . . . . . . . . . . . . 30342 1 213 1 4.552 . . . . . . . . . . . . . 30342 1 213 2 1.744 . . . . . . . . . . . . . 30342 1 214 1 4.55 . . . . . . . . . . . . . 30342 1 214 2 1.607 . . . . . . . . . . . . . 30342 1 215 1 4.551 . . . . . . . . . . . . . 30342 1 215 2 1.502 . . . . . . . . . . . . . 30342 1 216 1 4.549 . . . . . . . . . . . . . 30342 1 216 2 1.416 . . . . . . . . . . . . . 30342 1 217 1 4.283 . . . . . . . . . . . . . 30342 1 217 2 1.619 . . . . . . . . . . . . . 30342 1 218 1 3.878 . . . . . . . . . . . . . 30342 1 218 2 1.605 . . . . . . . . . . . . . 30342 1 219 1 4.42 . . . . . . . . . . . . . 30342 1 219 2 1.196 . . . . . . . . . . . . . 30342 1 220 1 4.459 . . . . . . . . . . . . . 30342 1 220 2 1.134 . . . . . . . . . . . . . 30342 1 221 1 2.746 . . . . . . . . . . . . . 30342 1 221 2 1.196 . . . . . . . . . . . . . 30342 1 222 1 2.698 . . . . . . . . . . . . . 30342 1 222 2 1.135 . . . . . . . . . . . . . 30342 1 223 1 3.571 . . . . . . . . . . . . . 30342 1 223 2 1.196 . . . . . . . . . . . . . 30342 1 224 1 3.462 . . . . . . . . . . . . . 30342 1 224 2 1.196 . . . . . . . . . . . . . 30342 1 225 1 3.875 . . . . . . . . . . . . . 30342 1 225 2 1.197 . . . . . . . . . . . . . 30342 1 226 1 3.877 . . . . . . . . . . . . . 30342 1 226 2 1.136 . . . . . . . . . . . . . 30342 1 227 1 4.276 . . . . . . . . . . . . . 30342 1 227 2 1.828 . . . . . . . . . . . . . 30342 1 228 1 4.279 . . . . . . . . . . . . . 30342 1 228 2 1.743 . . . . . . . . . . . . . 30342 1 229 1 1.191 . . . . . . . . . . . . . 30342 1 229 2 2.745 . . . . . . . . . . . . . 30342 1 230 1 1.125 . . . . . . . . . . . . . 30342 1 230 2 2.7 . . . . . . . . . . . . . 30342 1 231 1 1.622 . . . . . . . . . . . . . 30342 1 231 2 2.959 . . . . . . . . . . . . . 30342 1 232 1 1.571 . . . . . . . . . . . . . 30342 1 232 2 2.959 . . . . . . . . . . . . . 30342 1 233 1 7.456 . . . . . . . . . . . . . 30342 1 233 2 2.63 . . . . . . . . . . . . . 30342 1 234 1 7.458 . . . . . . . . . . . . . 30342 1 234 2 2.585 . . . . . . . . . . . . . 30342 1 235 1 3.812 . . . . . . . . . . . . . 30342 1 235 2 0.958 . . . . . . . . . . . . . 30342 1 236 1 4.185 . . . . . . . . . . . . . 30342 1 236 2 0.955 . . . . . . . . . . . . . 30342 1 237 1 1.629 . . . . . . . . . . . . . 30342 1 237 2 4.288 . . . . . . . . . . . . . 30342 1 238 1 1.571 . . . . . . . . . . . . . 30342 1 238 2 4.289 . . . . . . . . . . . . . 30342 1 239 1 1.399 . . . . . . . . . . . . . 30342 1 239 2 4.288 . . . . . . . . . . . . . 30342 1 240 1 1.326 . . . . . . . . . . . . . 30342 1 240 2 4.287 . . . . . . . . . . . . . 30342 1 241 1 2.965 . . . . . . . . . . . . . 30342 1 241 2 4.292 . . . . . . . . . . . . . 30342 1 242 1 1.327 . . . . . . . . . . . . . 30342 1 242 2 2.959 . . . . . . . . . . . . . 30342 1 243 1 1.402 . . . . . . . . . . . . . 30342 1 243 2 2.959 . . . . . . . . . . . . . 30342 1 244 1 1.693 . . . . . . . . . . . . . 30342 1 244 2 2.979 . . . . . . . . . . . . . 30342 1 245 1 1.429 . . . . . . . . . . . . . 30342 1 245 2 2.979 . . . . . . . . . . . . . 30342 1 246 1 1.496 . . . . . . . . . . . . . 30342 1 246 2 2.965 . . . . . . . . . . . . . 30342 1 247 1 1.416 . . . . . . . . . . . . . 30342 1 247 2 2.965 . . . . . . . . . . . . . 30342 1 248 1 1.609 . . . . . . . . . . . . . 30342 1 248 2 2.965 . . . . . . . . . . . . . 30342 1 stop_ save_