data_34038 ####################### # Entry information # ####################### save_entry_information _Entry.Sf_category entry_information _Entry.Sf_framecode entry_information _Entry.ID 34038 _Entry.Title ; SINEB2 element of the long non-coding RNA activator of translation AS Uchl1 ; _Entry.Type macromolecule _Entry.Version_type original _Entry.Submission_date 2016-09-05 _Entry.Accession_date 2016-09-05 _Entry.Last_release_date 2016-09-06 _Entry.Original_release_date 2016-09-06 _Entry.Origination author _Entry.Format_name . _Entry.NMR_STAR_version 3.2.0.16 _Entry.Original_NMR_STAR_version 3.1 _Entry.Experimental_method NMR _Entry.Experimental_method_subtype SOLUTION _Entry.Source_data_format . _Entry.Source_data_format_version . _Entry.Generated_software_name . _Entry.Generated_software_version . _Entry.Generated_software_ID . _Entry.Generated_software_label . _Entry.Generated_date . _Entry.DOI . _Entry.UUID . _Entry.Related_coordinate_file_name . _Entry.Details . _Entry.BMRB_internal_directory_name . loop_ _Entry_author.Ordinal _Entry_author.Given_name _Entry_author.Family_name _Entry_author.First_initial _Entry_author.Middle_initials _Entry_author.Family_title _Entry_author.ORCID _Entry_author.Entry_ID 1 P. Podbevsek P. . . . 34038 2 J. Plavec J. . . . 34038 stop_ loop_ _Struct_keywords.Keywords _Struct_keywords.Text _Struct_keywords.Entry_ID RNA . 34038 'RNA SINEUP hairpin' . 34038 stop_ loop_ _Data_set.Type _Data_set.Count _Data_set.Entry_ID assigned_chemical_shifts 1 34038 stop_ loop_ _Datum.Type _Datum.Count _Datum.Entry_ID '13C chemical shifts' 63 34038 '15N chemical shifts' 18 34038 '1H chemical shifts' 93 34038 stop_ loop_ _Release.Release_number _Release.Format_type _Release.Format_version _Release.Date _Release.Submission_date _Release.Type _Release.Author _Release.Detail _Release.Entry_ID 2 . . 2018-02-28 2016-09-05 update BMRB 'update entry citation' 34038 1 . . 2017-09-15 2016-09-05 original author 'original release' 34038 stop_ loop_ _Related_entries.Database_name _Related_entries.Database_accession_code _Related_entries.Relationship _Related_entries.Entry_ID PDB 5LSN 'BMRB Entry Tracking System' 34038 stop_ save_ ############### # Citations # ############### save_citation_1 _Citation.Sf_category citations _Citation.Sf_framecode citation_1 _Citation.Entry_ID 34038 _Citation.ID 1 _Citation.Class 'entry citation' _Citation.CAS_abstract_code . _Citation.MEDLINE_UI_code . _Citation.DOI . _Citation.PubMed_ID 29453387 _Citation.Full_citation . _Citation.Title ; Structural determinants of the SINE B2 element embedded in the long non-coding RNA activator of translation AS Uchl1 ; _Citation.Status published _Citation.Type journal _Citation.Journal_abbrev 'Sci. Rep.' _Citation.Journal_name_full 'Scientific reports' _Citation.Journal_volume 8 _Citation.Journal_issue 1 _Citation.Journal_ASTM . _Citation.Journal_ISSN 2045-2322 _Citation.Journal_CSD 0353 _Citation.Book_title . _Citation.Book_chapter_title . _Citation.Book_volume . _Citation.Book_series . _Citation.Book_publisher . _Citation.Book_publisher_city . _Citation.Book_ISBN . _Citation.Conference_title . _Citation.Conference_site . _Citation.Conference_state_province . _Citation.Conference_country . _Citation.Conference_start_date . _Citation.Conference_end_date . _Citation.Conference_abstract_number . _Citation.Thesis_institution . _Citation.Thesis_institution_city . _Citation.Thesis_institution_country . _Citation.WWW_URL . _Citation.Page_first 3189 _Citation.Page_last 3189 _Citation.Year 2018 _Citation.Details . loop_ _Citation_author.Ordinal _Citation_author.Given_name _Citation_author.Family_name _Citation_author.First_initial _Citation_author.Middle_initials _Citation_author.Family_title _Citation_author.ORCID _Citation_author.Entry_ID _Citation_author.Citation_ID 1 P. Podbevsek P. . . . 34038 1 2 F. Fasolo F. . . . 34038 1 3 C. Bon C. . . . 34038 1 4 L. Cimatti L. . . . 34038 1 5 S. Reisser S. . . . 34038 1 6 P. Carninci P. . . . 34038 1 7 G. Bussi G. . . . 34038 1 8 S. Zucchelli S. . . . 34038 1 9 J. Plavec J. . . . 34038 1 10 S. Gustincich S. . . . 34038 1 stop_ save_ ############################################# # Molecular system (assembly) description # ############################################# save_assembly _Assembly.Sf_category assembly _Assembly.Sf_framecode assembly _Assembly.Entry_ID 34038 _Assembly.ID 1 _Assembly.Name 'RNA (29-MER)' _Assembly.BMRB_code . _Assembly.Number_of_components . _Assembly.Organic_ligands . _Assembly.Metal_ions . _Assembly.Non_standard_bonds . _Assembly.Ambiguous_conformational_states . _Assembly.Ambiguous_chem_comp_sites . _Assembly.Molecules_in_chemical_exchange . _Assembly.Paramagnetic no _Assembly.Thiol_state . _Assembly.Molecular_mass . _Assembly.Enzyme_commission_number . _Assembly.Details . _Assembly.DB_query_date . _Assembly.DB_query_revised_last_date . loop_ _Entity_assembly.ID _Entity_assembly.Entity_assembly_name _Entity_assembly.Entity_ID _Entity_assembly.Entity_label _Entity_assembly.Asym_ID _Entity_assembly.PDB_chain_ID _Entity_assembly.Experimental_data_reported _Entity_assembly.Physical_state _Entity_assembly.Conformational_isomer _Entity_assembly.Chemical_exchange_state _Entity_assembly.Magnetic_equivalence_group_code _Entity_assembly.Role _Entity_assembly.Details _Entity_assembly.Entry_ID _Entity_assembly.Assembly_ID 1 entity_1 1 $entity_1 A A yes . . . . . . 34038 1 stop_ save_ #################################### # Biological polymers and ligands # #################################### save_entity_1 _Entity.Sf_category entity _Entity.Sf_framecode entity_1 _Entity.Entry_ID 34038 _Entity.ID 1 _Entity.BMRB_code . _Entity.Name entity_1 _Entity.Type polymer _Entity.Polymer_common_type . _Entity.Polymer_type polyribonucleotide _Entity.Polymer_type_details . _Entity.Polymer_strand_ID A _Entity.Polymer_seq_one_letter_code_can . _Entity.Polymer_seq_one_letter_code ; CCUCGUGGUGGUUGUGAACC ACCAUGUGG ; _Entity.Target_identifier . _Entity.Polymer_author_defined_seq . _Entity.Polymer_author_seq_details . _Entity.Ambiguous_conformational_states . _Entity.Ambiguous_chem_comp_sites . _Entity.Nstd_monomer no _Entity.Nstd_chirality . _Entity.Nstd_linkage no _Entity.Nonpolymer_comp_ID . _Entity.Nonpolymer_comp_label . _Entity.Number_of_monomers 29 _Entity.Number_of_nonpolymer_components . _Entity.Paramagnetic no _Entity.Thiol_state 'not present' _Entity.Src_method syn _Entity.Parent_entity_ID 1 _Entity.Fragment . _Entity.Mutation . _Entity.EC_number . _Entity.Calc_isoelectric_point . _Entity.Formula_weight 9309.521 _Entity.Formula_weight_exptl . _Entity.Formula_weight_exptl_meth . _Entity.Details . _Entity.DB_query_date . _Entity.DB_query_revised_last_date . loop_ _Entity_comp_index.ID _Entity_comp_index.Auth_seq_ID _Entity_comp_index.Comp_ID _Entity_comp_index.Comp_label _Entity_comp_index.Entry_ID _Entity_comp_index.Entity_ID 1 64 C . 34038 1 2 65 C . 34038 1 3 66 U . 34038 1 4 67 C . 34038 1 5 68 G . 34038 1 6 69 U . 34038 1 7 70 G . 34038 1 8 71 G . 34038 1 9 72 U . 34038 1 10 73 G . 34038 1 11 74 G . 34038 1 12 75 U . 34038 1 13 76 U . 34038 1 14 77 G . 34038 1 15 78 U . 34038 1 16 79 G . 34038 1 17 80 A . 34038 1 18 81 A . 34038 1 19 82 C . 34038 1 20 83 C . 34038 1 21 84 A . 34038 1 22 85 C . 34038 1 23 86 C . 34038 1 24 87 A . 34038 1 25 88 U . 34038 1 26 89 G . 34038 1 27 90 U . 34038 1 28 91 G . 34038 1 29 92 G . 34038 1 stop_ loop_ _Entity_poly_seq.Hetero _Entity_poly_seq.Mon_ID _Entity_poly_seq.Num _Entity_poly_seq.Comp_index_ID _Entity_poly_seq.Entry_ID _Entity_poly_seq.Entity_ID . C 1 1 34038 1 . C 2 2 34038 1 . U 3 3 34038 1 . C 4 4 34038 1 . G 5 5 34038 1 . U 6 6 34038 1 . G 7 7 34038 1 . G 8 8 34038 1 . U 9 9 34038 1 . G 10 10 34038 1 . G 11 11 34038 1 . U 12 12 34038 1 . U 13 13 34038 1 . G 14 14 34038 1 . U 15 15 34038 1 . G 16 16 34038 1 . A 17 17 34038 1 . A 18 18 34038 1 . C 19 19 34038 1 . C 20 20 34038 1 . A 21 21 34038 1 . C 22 22 34038 1 . C 23 23 34038 1 . A 24 24 34038 1 . U 25 25 34038 1 . G 26 26 34038 1 . U 27 27 34038 1 . G 28 28 34038 1 . G 29 29 34038 1 stop_ save_ #################### # Natural source # #################### save_natural_source _Entity_natural_src_list.Sf_category natural_source _Entity_natural_src_list.Sf_framecode natural_source _Entity_natural_src_list.Entry_ID 34038 _Entity_natural_src_list.ID 1 loop_ _Entity_natural_src.ID _Entity_natural_src.Entity_ID _Entity_natural_src.Entity_label _Entity_natural_src.Entity_chimera_segment_ID _Entity_natural_src.NCBI_taxonomy_ID _Entity_natural_src.Type _Entity_natural_src.Common _Entity_natural_src.Organism_name_scientific _Entity_natural_src.Organism_name_common _Entity_natural_src.Organism_acronym _Entity_natural_src.ICTVdb_decimal_code _Entity_natural_src.Superkingdom _Entity_natural_src.Kingdom _Entity_natural_src.Genus _Entity_natural_src.Species _Entity_natural_src.Strain _Entity_natural_src.Variant _Entity_natural_src.Organ _Entity_natural_src.Tissue _Entity_natural_src.Tissue_fraction _Entity_natural_src.Cell_line _Entity_natural_src.Cell_type _Entity_natural_src.ATCC_number _Entity_natural_src.Organelle _Entity_natural_src.Secretion _Entity_natural_src.Plasmid _Entity_natural_src.Gene_mnemonic _Entity_natural_src.Details _Entity_natural_src.Entry_ID _Entity_natural_src.Entity_natural_src_list_ID 1 1 $entity_1 . 10090 organism . 'Mus musculus' 'House Mouse' . . Eukaryota Metazoa Mus musculus . . . . . . . . . . . . . 34038 1 stop_ save_ ######################### # Experimental source # ######################### save_experimental_source _Entity_experimental_src_list.Sf_category experimental_source _Entity_experimental_src_list.Sf_framecode experimental_source _Entity_experimental_src_list.Entry_ID 34038 _Entity_experimental_src_list.ID 1 loop_ _Entity_experimental_src.ID _Entity_experimental_src.Entity_ID _Entity_experimental_src.Entity_label _Entity_experimental_src.Entity_chimera_segment_ID _Entity_experimental_src.Production_method _Entity_experimental_src.Host_org_scientific_name _Entity_experimental_src.Host_org_name_common _Entity_experimental_src.Host_org_details _Entity_experimental_src.Host_org_NCBI_taxonomy_ID _Entity_experimental_src.Host_org_genus _Entity_experimental_src.Host_org_species _Entity_experimental_src.Host_org_strain _Entity_experimental_src.Host_org_variant _Entity_experimental_src.Host_org_ATCC_number _Entity_experimental_src.Vector_type _Entity_experimental_src.PDBview_host_org_vector_name _Entity_experimental_src.PDBview_plasmid_name _Entity_experimental_src.Vector_name _Entity_experimental_src.Vector_details _Entity_experimental_src.Vendor_name _Entity_experimental_src.Details _Entity_experimental_src.Entry_ID _Entity_experimental_src.Entity_experimental_src_list_ID 1 1 $entity_1 . 'chemical synthesis' . . . . . . . . . . . . . . . . 34038 1 stop_ save_ ##################################### # Sample contents and methodology # ##################################### ######################## # Sample description # ######################## save_sample_1 _Sample.Sf_category sample _Sample.Sf_framecode sample_1 _Sample.Entry_ID 34038 _Sample.ID 1 _Sample.Type solution _Sample.Sub_type . _Sample.Details '0.5 mM RNA (29-MER), 90% H2O/10% D2O' _Sample.Aggregate_sample_number . _Sample.Solvent_system '90% H2O/10% D2O' _Sample.Preparation_date . _Sample.Preparation_expiration_date . _Sample.Polycrystallization_protocol . _Sample.Single_crystal_protocol . _Sample.Crystal_grow_apparatus . _Sample.Crystal_grow_atmosphere . _Sample.Crystal_grow_details . _Sample.Crystal_grow_method . _Sample.Crystal_grow_method_cit_ID . _Sample.Crystal_grow_pH . _Sample.Crystal_grow_pH_range . _Sample.Crystal_grow_pressure . _Sample.Crystal_grow_pressure_esd . _Sample.Crystal_grow_seeding . _Sample.Crystal_grow_seeding_cit_ID . _Sample.Crystal_grow_temp . _Sample.Crystal_grow_temp_details . _Sample.Crystal_grow_temp_esd . _Sample.Crystal_grow_time . _Sample.Oriented_sample_prep_protocol . _Sample.Lyophilization_cryo_protectant . _Sample.Storage_protocol . loop_ _Sample_component.ID _Sample_component.Mol_common_name _Sample_component.Isotopic_labeling _Sample_component.Assembly_ID _Sample_component.Assembly_label _Sample_component.Entity_ID _Sample_component.Entity_label _Sample_component.Product_ID _Sample_component.Type _Sample_component.Concentration_val _Sample_component.Concentration_val_min _Sample_component.Concentration_val_max _Sample_component.Concentration_val_units _Sample_component.Concentration_val_err _Sample_component.Vendor _Sample_component.Vendor_product_name _Sample_component.Vendor_product_code _Sample_component.Entry_ID _Sample_component.Sample_ID 1 'RNA (29-MER)' 'natural abundance' . . 1 $entity_1 . . 0.5 . . mM . . . . 34038 1 stop_ save_ save_sample_2 _Sample.Sf_category sample _Sample.Sf_framecode sample_2 _Sample.Entry_ID 34038 _Sample.ID 2 _Sample.Type solution _Sample.Sub_type . _Sample.Details '0.5 mM RNA (29-MER), 100% D2O' _Sample.Aggregate_sample_number . _Sample.Solvent_system '100% D2O' _Sample.Preparation_date . _Sample.Preparation_expiration_date . _Sample.Polycrystallization_protocol . _Sample.Single_crystal_protocol . _Sample.Crystal_grow_apparatus . _Sample.Crystal_grow_atmosphere . _Sample.Crystal_grow_details . _Sample.Crystal_grow_method . _Sample.Crystal_grow_method_cit_ID . _Sample.Crystal_grow_pH . _Sample.Crystal_grow_pH_range . _Sample.Crystal_grow_pressure . _Sample.Crystal_grow_pressure_esd . _Sample.Crystal_grow_seeding . _Sample.Crystal_grow_seeding_cit_ID . _Sample.Crystal_grow_temp . _Sample.Crystal_grow_temp_details . _Sample.Crystal_grow_temp_esd . _Sample.Crystal_grow_time . _Sample.Oriented_sample_prep_protocol . _Sample.Lyophilization_cryo_protectant . _Sample.Storage_protocol . loop_ _Sample_component.ID _Sample_component.Mol_common_name _Sample_component.Isotopic_labeling _Sample_component.Assembly_ID _Sample_component.Assembly_label _Sample_component.Entity_ID _Sample_component.Entity_label _Sample_component.Product_ID _Sample_component.Type _Sample_component.Concentration_val _Sample_component.Concentration_val_min _Sample_component.Concentration_val_max _Sample_component.Concentration_val_units _Sample_component.Concentration_val_err _Sample_component.Vendor _Sample_component.Vendor_product_name _Sample_component.Vendor_product_code _Sample_component.Entry_ID _Sample_component.Sample_ID 1 'RNA (29-MER)' 'natural abundance' . . 1 $entity_1 . . 0.5 . . mM . . . . 34038 2 stop_ save_ save_sample_3 _Sample.Sf_category sample _Sample.Sf_framecode sample_3 _Sample.Entry_ID 34038 _Sample.ID 3 _Sample.Type solution _Sample.Sub_type . _Sample.Details '0.5 mM [U-99% 13C; U-99% 15N] RNA (29-MER), 100% D2O' _Sample.Aggregate_sample_number . _Sample.Solvent_system '100% D2O' _Sample.Preparation_date . _Sample.Preparation_expiration_date . _Sample.Polycrystallization_protocol . _Sample.Single_crystal_protocol . _Sample.Crystal_grow_apparatus . _Sample.Crystal_grow_atmosphere . _Sample.Crystal_grow_details . _Sample.Crystal_grow_method . _Sample.Crystal_grow_method_cit_ID . _Sample.Crystal_grow_pH . _Sample.Crystal_grow_pH_range . _Sample.Crystal_grow_pressure . _Sample.Crystal_grow_pressure_esd . _Sample.Crystal_grow_seeding . _Sample.Crystal_grow_seeding_cit_ID . _Sample.Crystal_grow_temp . _Sample.Crystal_grow_temp_details . _Sample.Crystal_grow_temp_esd . _Sample.Crystal_grow_time . _Sample.Oriented_sample_prep_protocol . _Sample.Lyophilization_cryo_protectant . _Sample.Storage_protocol . loop_ _Sample_component.ID _Sample_component.Mol_common_name _Sample_component.Isotopic_labeling _Sample_component.Assembly_ID _Sample_component.Assembly_label _Sample_component.Entity_ID _Sample_component.Entity_label _Sample_component.Product_ID _Sample_component.Type _Sample_component.Concentration_val _Sample_component.Concentration_val_min _Sample_component.Concentration_val_max _Sample_component.Concentration_val_units _Sample_component.Concentration_val_err _Sample_component.Vendor _Sample_component.Vendor_product_name _Sample_component.Vendor_product_code _Sample_component.Entry_ID _Sample_component.Sample_ID 1 'RNA (29-MER)' '[U-99% 13C; U-99% 15N]' . . 1 $entity_1 . . 0.5 . . mM . . . . 34038 3 stop_ save_ ####################### # Sample conditions # ####################### save_sample_conditions_1 _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode sample_conditions_1 _Sample_condition_list.Entry_ID 34038 _Sample_condition_list.ID 1 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID pH 7 . pH 34038 1 pressure 1 . atm 34038 1 temperature 298 . K 34038 1 stop_ save_ save_sample_conditions_2 _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode sample_conditions_2 _Sample_condition_list.Entry_ID 34038 _Sample_condition_list.ID 2 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID pH 7 . pH 34038 2 pressure 1 . atm 34038 2 temperature 273 . K 34038 2 stop_ save_ ############################ # Computer software used # ############################ save_software_1 _Software.Sf_category software _Software.Sf_framecode software_1 _Software.Entry_ID 34038 _Software.ID 1 _Software.Type . _Software.Name AMBER _Software.Version . _Software.DOI . _Software.Details . loop_ _Vendor.Name _Vendor.Address _Vendor.Electronic_address _Vendor.Entry_ID _Vendor.Software_ID 'Case, Darden, Cheatham III, Simmerling, Wang, Duke, Luo, ... and Kollman' . . 34038 1 stop_ loop_ _Task.Task _Task.Entry_ID _Task.Software_ID 'structure calculation' 34038 1 stop_ save_ save_software_2 _Software.Sf_category software _Software.Sf_framecode software_2 _Software.Entry_ID 34038 _Software.ID 2 _Software.Type . _Software.Name NMRPipe _Software.Version . _Software.DOI . _Software.Details . loop_ _Vendor.Name _Vendor.Address _Vendor.Electronic_address _Vendor.Entry_ID _Vendor.Software_ID 'Delaglio, Grzesiek, Vuister, Zhu, Pfeifer and Bax' . . 34038 2 stop_ loop_ _Task.Task _Task.Entry_ID _Task.Software_ID processing 34038 2 stop_ save_ save_software_3 _Software.Sf_category software _Software.Sf_framecode software_3 _Software.Entry_ID 34038 _Software.ID 3 _Software.Type . _Software.Name SPARKY _Software.Version . _Software.DOI . _Software.Details . loop_ _Vendor.Name _Vendor.Address _Vendor.Electronic_address _Vendor.Entry_ID _Vendor.Software_ID Goddard . . 34038 3 stop_ loop_ _Task.Task _Task.Entry_ID _Task.Software_ID 'chemical shift assignment' 34038 3 stop_ save_ save_software_4 _Software.Sf_category software _Software.Sf_framecode software_4 _Software.Entry_ID 34038 _Software.ID 4 _Software.Type . _Software.Name VNMR _Software.Version . _Software.DOI . _Software.Details . loop_ _Vendor.Name _Vendor.Address _Vendor.Electronic_address _Vendor.Entry_ID _Vendor.Software_ID Varian . . 34038 4 stop_ loop_ _Task.Task _Task.Entry_ID _Task.Software_ID collection 34038 4 stop_ save_ ######################### # Experimental detail # ######################### ################################## # NMR Spectrometer definitions # ################################## save_NMR_spectrometer_1 _NMR_spectrometer.Sf_category NMR_spectrometer _NMR_spectrometer.Sf_framecode NMR_spectrometer_1 _NMR_spectrometer.Entry_ID 34038 _NMR_spectrometer.ID 1 _NMR_spectrometer.Details . _NMR_spectrometer.Manufacturer Agilent _NMR_spectrometer.Model VNMRS _NMR_spectrometer.Serial_number . _NMR_spectrometer.Field_strength 600 save_ save_NMR_spectrometer_list _NMR_spectrometer_list.Sf_category NMR_spectrometer_list _NMR_spectrometer_list.Sf_framecode NMR_spectrometer_list _NMR_spectrometer_list.Entry_ID 34038 _NMR_spectrometer_list.ID 1 loop_ _NMR_spectrometer_view.ID _NMR_spectrometer_view.Name _NMR_spectrometer_view.Manufacturer _NMR_spectrometer_view.Model _NMR_spectrometer_view.Serial_number _NMR_spectrometer_view.Field_strength _NMR_spectrometer_view.Details _NMR_spectrometer_view.Citation_ID _NMR_spectrometer_view.Citation_label _NMR_spectrometer_view.Entry_ID _NMR_spectrometer_view.NMR_spectrometer_list_ID 1 NMR_spectrometer_1 Agilent VNMRS . 600 . . . 34038 1 stop_ save_ ############################# # NMR applied experiments # ############################# save_experiment_list _Experiment_list.Sf_category experiment_list _Experiment_list.Sf_framecode experiment_list _Experiment_list.Entry_ID 34038 _Experiment_list.ID 1 _Experiment_list.Details . loop_ _Experiment.ID _Experiment.Name _Experiment.Raw_data_flag _Experiment.NMR_spec_expt_ID _Experiment.NMR_spec_expt_label _Experiment.MS_expt_ID _Experiment.MS_expt_label _Experiment.SAXS_expt_ID _Experiment.SAXS_expt_label _Experiment.FRET_expt_ID _Experiment.FRET_expt_label _Experiment.EMR_expt_ID _Experiment.EMR_expt_label _Experiment.Sample_ID _Experiment.Sample_label _Experiment.Sample_state _Experiment.Sample_volume _Experiment.Sample_volume_units _Experiment.Sample_condition_list_ID _Experiment.Sample_condition_list_label _Experiment.Sample_spinning_rate _Experiment.Sample_angle _Experiment.NMR_tube_type _Experiment.NMR_spectrometer_ID _Experiment.NMR_spectrometer_label _Experiment.NMR_spectrometer_probe_ID _Experiment.NMR_spectrometer_probe_label _Experiment.NMR_spectral_processing_ID _Experiment.NMR_spectral_processing_label _Experiment.Mass_spectrometer_ID _Experiment.Mass_spectrometer_label _Experiment.Xray_instrument_ID _Experiment.Xray_instrument_label _Experiment.Fluorescence_instrument_ID _Experiment.Fluorescence_instrument_label _Experiment.EMR_instrument_ID _Experiment.EMR_instrument_label _Experiment.Chromatographic_system_ID _Experiment.Chromatographic_system_label _Experiment.Chromatographic_column_ID _Experiment.Chromatographic_column_label _Experiment.Entry_ID _Experiment.Experiment_list_ID 1 '2D 1H-1H NOESY' no . . . . . . . . . . 1 $sample_1 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . 34038 1 2 '2D 1H-15N HSQC' no . . . . . . . . . . 3 $sample_3 isotropic . . 2 $sample_conditions_2 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . 34038 1 3 '2D 1H-13C HSQC' no . . . . . . . . . . 3 $sample_3 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . 34038 1 4 '2D DQF-COSY' no . . . . . . . . . . 2 $sample_2 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . 34038 1 5 '2D 1H-1H TOCSY' no . . . . . . . . . . 2 $sample_2 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . 34038 1 6 '2D HCN' no . . . . . . . . . . 3 $sample_3 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . 34038 1 stop_ save_ #################### # NMR parameters # #################### ############################## # Assigned chemical shifts # ############################## ################################ # Chemical shift referencing # ################################ save_chem_shift_reference_1 _Chem_shift_reference.Sf_category chem_shift_reference _Chem_shift_reference.Sf_framecode chem_shift_reference_1 _Chem_shift_reference.Entry_ID 34038 _Chem_shift_reference.ID 1 _Chem_shift_reference.Details . loop_ _Chem_shift_ref.Atom_type _Chem_shift_ref.Atom_isotope_number _Chem_shift_ref.Mol_common_name _Chem_shift_ref.Atom_group _Chem_shift_ref.Concentration_val _Chem_shift_ref.Concentration_units _Chem_shift_ref.Solvent _Chem_shift_ref.Rank _Chem_shift_ref.Chem_shift_units _Chem_shift_ref.Chem_shift_val _Chem_shift_ref.Ref_method _Chem_shift_ref.Ref_type _Chem_shift_ref.Indirect_shift_ratio _Chem_shift_ref.External_ref_loc _Chem_shift_ref.External_ref_sample_geometry _Chem_shift_ref.External_ref_axis _Chem_shift_ref.Ref_correction_type _Chem_shift_ref.Correction_val _Chem_shift_ref.Entry_ID _Chem_shift_ref.Chem_shift_reference_ID H 1 water protons . . . . ppm 4.78 internal direct 1.0 . . . . . 34038 1 stop_ save_ ################################### # Assigned chemical shift lists # ################################### ################################################################### # Chemical Shift Ambiguity Index Value Definitions # # # # The values other than 1 are used for those atoms with different # # chemical shifts that cannot be assigned to stereospecific atoms # # or to specific residues or chains. # # # # Index Value Definition # # # # 1 Unique (including isolated methyl protons, # # geminal atoms, and geminal methyl # # groups with identical chemical shifts) # # (e.g. ILE HD11, HD12, HD13 protons) # # 2 Ambiguity of geminal atoms or geminal methyl # # proton groups (e.g. ASP HB2 and HB3 # # protons, LEU CD1 and CD2 carbons, or # # LEU HD11, HD12, HD13 and HD21, HD22, # # HD23 methyl protons) # # 3 Aromatic atoms on opposite sides of # # symmetrical rings (e.g. TYR HE1 and HE2 # # protons) # # 4 Intraresidue ambiguities (e.g. LYS HG and # # HD protons or TRP HZ2 and HZ3 protons) # # 5 Interresidue ambiguities (LYS 12 vs. LYS 27) # # 6 Intermolecular ambiguities (e.g. ASP 31 CA # # in monomer 1 and ASP 31 CA in monomer 2 # # of an asymmetrical homodimer, duplex # # DNA assignments, or other assignments # # that may apply to atoms in one or more # # molecule in the molecular assembly) # # 9 Ambiguous, specific ambiguity not defined # # # ################################################################### save_assigned_chemical_shifts_1 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode assigned_chemical_shifts_1 _Assigned_chem_shift_list.Entry_ID 34038 _Assigned_chem_shift_list.ID 1 _Assigned_chem_shift_list.Sample_condition_list_ID 1 _Assigned_chem_shift_list.Sample_condition_list_label $sample_conditions_1 _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chem_shift_reference_1 _Assigned_chem_shift_list.Chem_shift_1H_err . _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err . _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID 1 '2D 1H-1H NOESY' . . . 34038 1 2 '2D 1H-15N HSQC' . . . 34038 1 3 '2D 1H-13C HSQC' . . . 34038 1 stop_ loop_ _Chem_shift_software.Software_ID _Chem_shift_software.Software_label _Chem_shift_software.Method_ID _Chem_shift_software.Method_label _Chem_shift_software.Entry_ID _Chem_shift_software.Assigned_chem_shift_list_ID 3 $software_3 . . 34038 1 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Ambiguity_set_ID _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 1 1 1 C H1' H 1 5.338 0.02 . 1 . . . . A 64 C H1' . 34038 1 2 . 1 1 1 1 C H5 H 1 5.563 0.02 . 1 . . . . A 64 C H5 . 34038 1 3 . 1 1 1 1 C H6 H 1 7.596 0.02 . 1 . . . . A 64 C H6 . 34038 1 4 . 1 1 1 1 C C1' C 13 94.212 0.20 . 1 . . . . A 64 C C1' . 34038 1 5 . 1 1 1 1 C C5 C 13 98.142 0.20 . 1 . . . . A 64 C C5 . 34038 1 6 . 1 1 1 1 C C6 C 13 141.538 0.20 . 1 . . . . A 64 C C6 . 34038 1 7 . 1 1 1 1 C N1 N 15 151.242 0.10 . 1 . . . . A 64 C N1 . 34038 1 8 . 1 1 2 2 C H1' H 1 5.433 0.02 . 1 . . . . A 65 C H1' . 34038 1 9 . 1 1 2 2 C H5 H 1 5.428 0.02 . 1 . . . . A 65 C H5 . 34038 1 10 . 1 1 2 2 C H6 H 1 7.665 0.02 . 1 . . . . A 65 C H6 . 34038 1 11 . 1 1 2 2 C C5 C 13 97.998 0.20 . 1 . . . . A 65 C C5 . 34038 1 12 . 1 1 2 2 C C6 C 13 141.268 0.20 . 1 . . . . A 65 C C6 . 34038 1 13 . 1 1 2 2 C N1 N 15 151.254 0.10 . 1 . . . . A 65 C N1 . 34038 1 14 . 1 1 3 3 U H1' H 1 5.490 0.02 . 1 . . . . A 66 U H1' . 34038 1 15 . 1 1 3 3 U H5 H 1 5.502 0.02 . 1 . . . . A 66 U H5 . 34038 1 16 . 1 1 3 3 U H6 H 1 7.776 0.02 . 1 . . . . A 66 U H6 . 34038 1 17 . 1 1 3 3 U C1' C 13 93.779 0.20 . 1 . . . . A 66 U C1' . 34038 1 18 . 1 1 3 3 U C5 C 13 104.105 0.20 . 1 . . . . A 66 U C5 . 34038 1 19 . 1 1 3 3 U C6 C 13 141.476 0.20 . 1 . . . . A 66 U C6 . 34038 1 20 . 1 1 3 3 U N1 N 15 145.882 0.10 . 1 . . . . A 66 U N1 . 34038 1 21 . 1 1 4 4 C H1' H 1 5.732 0.02 . 1 . . . . A 67 C H1' . 34038 1 22 . 1 1 4 4 C H5 H 1 5.662 0.02 . 1 . . . . A 67 C H5 . 34038 1 23 . 1 1 4 4 C H6 H 1 7.934 0.02 . 1 . . . . A 67 C H6 . 34038 1 24 . 1 1 4 4 C C1' C 13 92.572 0.20 . 1 . . . . A 67 C C1' . 34038 1 25 . 1 1 4 4 C C5 C 13 97.593 0.20 . 1 . . . . A 67 C C5 . 34038 1 26 . 1 1 4 4 C C6 C 13 142.489 0.20 . 1 . . . . A 67 C C6 . 34038 1 27 . 1 1 4 4 C N1 N 15 151.445 0.10 . 1 . . . . A 67 C N1 . 34038 1 28 . 1 1 5 5 G H1' H 1 5.677 0.02 . 1 . . . . A 68 G H1' . 34038 1 29 . 1 1 5 5 G H8 H 1 7.553 0.02 . 1 . . . . A 68 G H8 . 34038 1 30 . 1 1 5 5 G C1' C 13 92.919 0.20 . 1 . . . . A 68 G C1' . 34038 1 31 . 1 1 5 5 G C8 C 13 137.519 0.20 . 1 . . . . A 68 G C8 . 34038 1 32 . 1 1 6 6 U H1' H 1 5.495 0.02 . 1 . . . . A 69 U H1' . 34038 1 33 . 1 1 6 6 U H5 H 1 5.090 0.02 . 1 . . . . A 69 U H5 . 34038 1 34 . 1 1 6 6 U H6 H 1 7.637 0.02 . 1 . . . . A 69 U H6 . 34038 1 35 . 1 1 6 6 U C5 C 13 103.039 0.20 . 1 . . . . A 69 U C5 . 34038 1 36 . 1 1 6 6 U C6 C 13 141.734 0.20 . 1 . . . . A 69 U C6 . 34038 1 37 . 1 1 6 6 U N1 N 15 146.315 0.10 . 1 . . . . A 69 U N1 . 34038 1 38 . 1 1 7 7 G H1 H 1 11.990 0.02 . 1 . . . . A 70 G H1 . 34038 1 39 . 1 1 7 7 G H1' H 1 5.796 0.02 . 1 . . . . A 70 G H1' . 34038 1 40 . 1 1 7 7 G H8 H 1 7.706 0.02 . 1 . . . . A 70 G H8 . 34038 1 41 . 1 1 7 7 G C1' C 13 92.524 0.20 . 1 . . . . A 70 G C1' . 34038 1 42 . 1 1 7 7 G C8 C 13 136.447 0.20 . 1 . . . . A 70 G C8 . 34038 1 43 . 1 1 8 8 G H1 H 1 13.167 0.02 . 1 . . . . A 71 G H1 . 34038 1 44 . 1 1 8 8 G H1' H 1 5.684 0.02 . 1 . . . . A 71 G H1' . 34038 1 45 . 1 1 8 8 G H8 H 1 7.175 0.02 . 1 . . . . A 71 G H8 . 34038 1 46 . 1 1 8 8 G C1' C 13 89.328 0.20 . 1 . . . . A 71 G C1' . 34038 1 47 . 1 1 8 8 G C8 C 13 136.284 0.20 . 1 . . . . A 71 G C8 . 34038 1 48 . 1 1 9 9 U H1' H 1 5.502 0.02 . 1 . . . . A 72 U H1' . 34038 1 49 . 1 1 9 9 U H3 H 1 13.600 0.02 . 1 . . . . A 72 U H3 . 34038 1 50 . 1 1 9 9 U H5 H 1 4.993 0.02 . 1 . . . . A 72 U H5 . 34038 1 51 . 1 1 9 9 U H6 H 1 7.617 0.02 . 1 . . . . A 72 U H6 . 34038 1 52 . 1 1 9 9 U C5 C 13 105.637 0.20 . 1 . . . . A 72 U C5 . 34038 1 53 . 1 1 9 9 U C6 C 13 141.594 0.20 . 1 . . . . A 72 U C6 . 34038 1 54 . 1 1 10 10 G H1 H 1 12.093 0.02 . 1 . . . . A 73 G H1 . 34038 1 55 . 1 1 10 10 G H1' H 1 5.791 0.02 . 1 . . . . A 73 G H1' . 34038 1 56 . 1 1 10 10 G H8 H 1 7.679 0.02 . 1 . . . . A 73 G H8 . 34038 1 57 . 1 1 10 10 G C1' C 13 92.666 0.20 . 1 . . . . A 73 G C1' . 34038 1 58 . 1 1 10 10 G C8 C 13 136.333 0.20 . 1 . . . . A 73 G C8 . 34038 1 59 . 1 1 10 10 G N9 N 15 169.935 0.10 . 1 . . . . A 73 G N9 . 34038 1 60 . 1 1 11 11 G H1 H 1 13.219 0.02 . 1 . . . . A 74 G H1 . 34038 1 61 . 1 1 11 11 G H1' H 1 5.637 0.02 . 1 . . . . A 74 G H1' . 34038 1 62 . 1 1 11 11 G H8 H 1 7.168 0.02 . 1 . . . . A 74 G H8 . 34038 1 63 . 1 1 11 11 G C8 C 13 136.277 0.20 . 1 . . . . A 74 G C8 . 34038 1 64 . 1 1 12 12 U H1' H 1 5.542 0.02 . 1 . . . . A 75 U H1' . 34038 1 65 . 1 1 12 12 U H5 H 1 4.983 0.02 . 1 . . . . A 75 U H5 . 34038 1 66 . 1 1 12 12 U H6 H 1 7.628 0.02 . 1 . . . . A 75 U H6 . 34038 1 67 . 1 1 12 12 U C5 C 13 102.816 0.20 . 1 . . . . A 75 U C5 . 34038 1 68 . 1 1 13 13 U H1' H 1 5.850 0.02 . 1 . . . . A 76 U H1' . 34038 1 69 . 1 1 13 13 U H5 H 1 5.526 0.02 . 1 . . . . A 76 U H5 . 34038 1 70 . 1 1 13 13 U H6 H 1 7.727 0.02 . 1 . . . . A 76 U H6 . 34038 1 71 . 1 1 13 13 U C6 C 13 142.239 0.20 . 1 . . . . A 76 U C6 . 34038 1 72 . 1 1 13 13 U N1 N 15 146.048 0.10 . 1 . . . . A 76 U N1 . 34038 1 73 . 1 1 14 14 G H1' H 1 5.688 0.02 . 1 . . . . A 77 G H1' . 34038 1 74 . 1 1 14 14 G H8 H 1 7.975 0.02 . 1 . . . . A 77 G H8 . 34038 1 75 . 1 1 14 14 G C8 C 13 139.815 0.20 . 1 . . . . A 77 G C8 . 34038 1 76 . 1 1 14 14 G N9 N 15 166.521 0.10 . 1 . . . . A 77 G N9 . 34038 1 77 . 1 1 15 15 U H1' H 1 5.450 0.02 . 1 . . . . A 78 U H1' . 34038 1 78 . 1 1 15 15 U H2' H 1 4.378 0.02 . 1 . . . . A 78 U H2' . 34038 1 79 . 1 1 15 15 U H3' H 1 4.019 0.02 . 1 . . . . A 78 U H3' . 34038 1 80 . 1 1 15 15 U H4' H 1 3.892 0.02 . 1 . . . . A 78 U H4' . 34038 1 81 . 1 1 15 15 U H5 H 1 5.681 0.02 . 1 . . . . A 78 U H5 . 34038 1 82 . 1 1 15 15 U H6 H 1 7.499 0.02 . 1 . . . . A 78 U H6 . 34038 1 83 . 1 1 15 15 U C1' C 13 88.945 0.20 . 1 . . . . A 78 U C1' . 34038 1 84 . 1 1 15 15 U C2' C 13 78.028 0.20 . 1 . . . . A 78 U C2' . 34038 1 85 . 1 1 15 15 U C3' C 13 75.873 0.20 . 1 . . . . A 78 U C3' . 34038 1 86 . 1 1 15 15 U C4' C 13 84.560 0.20 . 1 . . . . A 78 U C4' . 34038 1 87 . 1 1 15 15 U C5 C 13 105.637 0.20 . 1 . . . . A 78 U C5 . 34038 1 88 . 1 1 15 15 U C6 C 13 143.243 0.20 . 1 . . . . A 78 U C6 . 34038 1 89 . 1 1 15 15 U N1 N 15 142.901 0.10 . 1 . . . . A 78 U N1 . 34038 1 90 . 1 1 16 16 G H1' H 1 5.406 0.02 . 1 . . . . A 79 G H1' . 34038 1 91 . 1 1 16 16 G H8 H 1 7.392 0.02 . 1 . . . . A 79 G H8 . 34038 1 92 . 1 1 16 16 G C1' C 13 89.954 0.20 . 1 . . . . A 79 G C1' . 34038 1 93 . 1 1 16 16 G C8 C 13 138.986 0.20 . 1 . . . . A 79 G C8 . 34038 1 94 . 1 1 17 17 A H1' H 1 5.682 0.02 . 1 . . . . A 80 A H1' . 34038 1 95 . 1 1 17 17 A H2 H 1 7.190 0.02 . 1 . . . . A 80 A H2 . 34038 1 96 . 1 1 17 17 A H8 H 1 8.296 0.02 . 1 . . . . A 80 A H8 . 34038 1 97 . 1 1 17 17 A C1' C 13 87.526 0.20 . 1 . . . . A 80 A C1' . 34038 1 98 . 1 1 17 17 A C2 C 13 153.217 0.20 . 1 . . . . A 80 A C2 . 34038 1 99 . 1 1 17 17 A C8 C 13 141.578 0.20 . 1 . . . . A 80 A C8 . 34038 1 100 . 1 1 17 17 A N9 N 15 165.413 0.10 . 1 . . . . A 80 A N9 . 34038 1 101 . 1 1 18 18 A H1' H 1 5.961 0.02 . 1 . . . . A 81 A H1' . 34038 1 102 . 1 1 18 18 A H2 H 1 7.845 0.02 . 1 . . . . A 81 A H2 . 34038 1 103 . 1 1 18 18 A H8 H 1 7.965 0.02 . 1 . . . . A 81 A H8 . 34038 1 104 . 1 1 18 18 A C1' C 13 92.994 0.20 . 1 . . . . A 81 A C1' . 34038 1 105 . 1 1 18 18 A C2 C 13 154.152 0.20 . 1 . . . . A 81 A C2 . 34038 1 106 . 1 1 18 18 A C8 C 13 139.740 0.20 . 1 . . . . A 81 A C8 . 34038 1 107 . 1 1 18 18 A N9 N 15 170.157 0.10 . 1 . . . . A 81 A N9 . 34038 1 108 . 1 1 19 19 C H1' H 1 5.418 0.02 . 1 . . . . A 82 C H1' . 34038 1 109 . 1 1 19 19 C H5 H 1 5.100 0.02 . 1 . . . . A 82 C H5 . 34038 1 110 . 1 1 19 19 C H6 H 1 7.504 0.02 . 1 . . . . A 82 C H6 . 34038 1 111 . 1 1 19 19 C H41 H 1 8.231 0.02 . 1 . . . . A 82 C H41 . 34038 1 112 . 1 1 19 19 C H42 H 1 6.743 0.02 . 1 . . . . A 82 C H42 . 34038 1 113 . 1 1 19 19 C C5 C 13 97.102 0.20 . 1 . . . . A 82 C C5 . 34038 1 114 . 1 1 19 19 C C6 C 13 140.919 0.20 . 1 . . . . A 82 C C6 . 34038 1 115 . 1 1 19 19 C N1 N 15 151.501 0.10 . 1 . . . . A 82 C N1 . 34038 1 116 . 1 1 20 20 C H1' H 1 5.413 0.02 . 1 . . . . A 83 C H1' . 34038 1 117 . 1 1 20 20 C H5 H 1 5.392 0.02 . 1 . . . . A 83 C H5 . 34038 1 118 . 1 1 20 20 C H6 H 1 7.692 0.02 . 1 . . . . A 83 C H6 . 34038 1 119 . 1 1 20 20 C H41 H 1 8.328 0.02 . 1 . . . . A 83 C H41 . 34038 1 120 . 1 1 20 20 C H42 H 1 6.749 0.02 . 1 . . . . A 83 C H42 . 34038 1 121 . 1 1 20 20 C C1' C 13 93.801 0.20 . 1 . . . . A 83 C C1' . 34038 1 122 . 1 1 20 20 C C5 C 13 97.792 0.20 . 1 . . . . A 83 C C5 . 34038 1 123 . 1 1 20 20 C C6 C 13 141.156 0.20 . 1 . . . . A 83 C C6 . 34038 1 124 . 1 1 20 20 C N1 N 15 150.636 0.10 . 1 . . . . A 83 C N1 . 34038 1 125 . 1 1 21 21 A H1' H 1 5.882 0.02 . 1 . . . . A 84 A H1' . 34038 1 126 . 1 1 21 21 A H2 H 1 7.316 0.02 . 1 . . . . A 84 A H2 . 34038 1 127 . 1 1 21 21 A H8 H 1 8.020 0.02 . 1 . . . . A 84 A H8 . 34038 1 128 . 1 1 21 21 A C1' C 13 92.992 0.20 . 1 . . . . A 84 A C1' . 34038 1 129 . 1 1 21 21 A C2 C 13 153.223 0.20 . 1 . . . . A 84 A C2 . 34038 1 130 . 1 1 21 21 A C8 C 13 139.636 0.20 . 1 . . . . A 84 A C8 . 34038 1 131 . 1 1 21 21 A N9 N 15 170.619 0.10 . 1 . . . . A 84 A N9 . 34038 1 132 . 1 1 22 22 C H1' H 1 5.367 0.02 . 1 . . . . A 85 C H1' . 34038 1 133 . 1 1 22 22 C H5 H 1 5.122 0.02 . 1 . . . . A 85 C H5 . 34038 1 134 . 1 1 22 22 C H6 H 1 7.496 0.02 . 1 . . . . A 85 C H6 . 34038 1 135 . 1 1 22 22 C H41 H 1 8.261 0.02 . 1 . . . . A 85 C H41 . 34038 1 136 . 1 1 22 22 C H42 H 1 6.855 0.02 . 1 . . . . A 85 C H42 . 34038 1 137 . 1 1 22 22 C C1' C 13 93.739 0.20 . 1 . . . . A 85 C C1' . 34038 1 138 . 1 1 22 22 C C5 C 13 97.145 0.20 . 1 . . . . A 85 C C5 . 34038 1 139 . 1 1 22 22 C C6 C 13 140.751 0.20 . 1 . . . . A 85 C C6 . 34038 1 140 . 1 1 22 22 C N1 N 15 151.222 0.10 . 1 . . . . A 85 C N1 . 34038 1 141 . 1 1 23 23 C H1' H 1 5.420 0.02 . 1 . . . . A 86 C H1' . 34038 1 142 . 1 1 23 23 C H5 H 1 5.394 0.02 . 1 . . . . A 86 C H5 . 34038 1 143 . 1 1 23 23 C H6 H 1 7.676 0.02 . 1 . . . . A 86 C H6 . 34038 1 144 . 1 1 23 23 C H41 H 1 8.238 0.02 . 1 . . . . A 86 C H41 . 34038 1 145 . 1 1 23 23 C H42 H 1 6.772 0.02 . 1 . . . . A 86 C H42 . 34038 1 146 . 1 1 23 23 C C5 C 13 97.755 0.20 . 1 . . . . A 86 C C5 . 34038 1 147 . 1 1 23 23 C N1 N 15 150.601 0.10 . 1 . . . . A 86 C N1 . 34038 1 148 . 1 1 24 24 A H1' H 1 5.901 0.02 . 1 . . . . A 87 A H1' . 34038 1 149 . 1 1 24 24 A H2 H 1 7.308 0.02 . 1 . . . . A 87 A H2 . 34038 1 150 . 1 1 24 24 A H8 H 1 7.886 0.02 . 1 . . . . A 87 A H8 . 34038 1 151 . 1 1 24 24 A C1' C 13 93.417 0.20 . 1 . . . . A 87 A C1' . 34038 1 152 . 1 1 24 24 A C2 C 13 153.294 0.20 . 1 . . . . A 87 A C2 . 34038 1 153 . 1 1 24 24 A C8 C 13 139.367 0.20 . 1 . . . . A 87 A C8 . 34038 1 154 . 1 1 24 24 A N9 N 15 171.102 0.10 . 1 . . . . A 87 A N9 . 34038 1 155 . 1 1 25 25 U H1' H 1 5.296 0.02 . 1 . . . . A 88 U H1' . 34038 1 156 . 1 1 25 25 U H5 H 1 5.287 0.02 . 1 . . . . A 88 U H5 . 34038 1 157 . 1 1 25 25 U H6 H 1 7.420 0.02 . 1 . . . . A 88 U H6 . 34038 1 158 . 1 1 25 25 U C1' C 13 92.781 0.20 . 1 . . . . A 88 U C1' . 34038 1 159 . 1 1 25 25 U C6 C 13 140.372 0.20 . 1 . . . . A 88 U C6 . 34038 1 160 . 1 1 25 25 U N1 N 15 144.772 0.10 . 1 . . . . A 88 U N1 . 34038 1 161 . 1 1 26 26 G H1' H 1 5.758 0.02 . 1 . . . . A 89 G H1' . 34038 1 162 . 1 1 26 26 G H8 H 1 7.817 0.02 . 1 . . . . A 89 G H8 . 34038 1 163 . 1 1 26 26 G C1' C 13 92.657 0.20 . 1 . . . . A 89 G C1' . 34038 1 164 . 1 1 26 26 G C8 C 13 137.715 0.20 . 1 . . . . A 89 G C8 . 34038 1 165 . 1 1 27 27 U H1' H 1 5.455 0.02 . 1 . . . . A 90 U H1' . 34038 1 166 . 1 1 27 27 U H5 H 1 5.079 0.02 . 1 . . . . A 90 U H5 . 34038 1 167 . 1 1 27 27 U H6 H 1 7.311 0.02 . 1 . . . . A 90 U H6 . 34038 1 168 . 1 1 27 27 U C5 C 13 103.285 0.20 . 1 . . . . A 90 U C5 . 34038 1 169 . 1 1 27 27 U C6 C 13 141.170 0.20 . 1 . . . . A 90 U C6 . 34038 1 170 . 1 1 28 28 G H1' H 1 5.775 0.02 . 1 . . . . A 91 G H1' . 34038 1 171 . 1 1 28 28 G H8 H 1 7.652 0.02 . 1 . . . . A 91 G H8 . 34038 1 172 . 1 1 29 29 G H1' H 1 5.702 0.02 . 1 . . . . A 92 G H1' . 34038 1 173 . 1 1 29 29 G H8 H 1 7.179 0.02 . 1 . . . . A 92 G H8 . 34038 1 174 . 1 1 29 29 G C8 C 13 136.430 0.20 . 1 . . . . A 92 G C8 . 34038 1 stop_ save_