data_5371
#######################
# Entry information #
#######################
save_entry_information
_Entry.Sf_category entry_information
_Entry.Sf_framecode entry_information
_Entry.ID 5371
_Entry.Title
;
U6 RNA chemical shifts
;
_Entry.Type macromolecule
_Entry.Version_type original
_Entry.Submission_date 2002-05-09
_Entry.Accession_date 2002-05-09
_Entry.Last_release_date .
_Entry.Original_release_date .
_Entry.Origination author
_Entry.NMR_STAR_version 3.1.1.61
_Entry.Original_NMR_STAR_version 2.1
_Entry.Experimental_method NMR
_Entry.Experimental_method_subtype .
_Entry.Details .
_Entry.BMRB_internal_directory_name .
loop_
_Entry_author.Ordinal
_Entry_author.Given_name
_Entry_author.Family_name
_Entry_author.First_initial
_Entry_author.Middle_initials
_Entry_author.Family_title
_Entry_author.Entry_ID
1 Samuel Butcher . E. . 5371
stop_
loop_
_Data_set.Type
_Data_set.Count
_Data_set.Entry_ID
assigned_chemical_shifts 1 5371
stop_
loop_
_Datum.Type
_Datum.Count
_Datum.Entry_ID
'13C chemical shifts' 41 5371
'15N chemical shifts' 14 5371
'1H chemical shifts' 211 5371
stop_
loop_
_Release.Release_number
_Release.Format_type
_Release.Format_version
_Release.Date
_Release.Submission_date
_Release.Type
_Release.Author
_Release.Detail
_Release.Entry_ID
3 . . 2010-06-01 2002-05-09 update BMRB 'update entry citation' 5371
2 . . 2009-06-02 2002-05-09 update BMRB 'complete entry citation' 5371
1 . . 2002-08-22 2002-05-09 original author 'original release' 5371
stop_
loop_
_Related_entries.Database_name
_Related_entries.Database_accession_code
_Related_entries.Relationship
_Related_entries.Entry_ID
PDB 1LC6 'BMRB Entry Tracking System' 5371
stop_
save_
###############
# Citations #
###############
save_entry_citation
_Citation.Sf_category citations
_Citation.Sf_framecode entry_citation
_Citation.Entry_ID 5371
_Citation.ID 1
_Citation.Class 'entry citation'
_Citation.CAS_abstract_code .
_Citation.MEDLINE_UI_code .
_Citation.DOI .
_Citation.PubMed_ID 11992125
_Citation.Full_citation .
_Citation.Title
;
Metal binding and base ionization in the U6 RNA intramolecular stem-loop
structure
;
_Citation.Status published
_Citation.Type journal
_Citation.Journal_abbrev 'Nat. Struct. Biol.'
_Citation.Journal_name_full .
_Citation.Journal_volume 9
_Citation.Journal_issue 6
_Citation.Journal_ASTM .
_Citation.Journal_ISSN .
_Citation.Journal_CSD .
_Citation.Book_title .
_Citation.Book_chapter_title .
_Citation.Book_volume .
_Citation.Book_series .
_Citation.Book_publisher .
_Citation.Book_publisher_city .
_Citation.Book_ISBN .
_Citation.Conference_title .
_Citation.Conference_site .
_Citation.Conference_state_province .
_Citation.Conference_country .
_Citation.Conference_start_date .
_Citation.Conference_end_date .
_Citation.Conference_abstract_number .
_Citation.Thesis_institution .
_Citation.Thesis_institution_city .
_Citation.Thesis_institution_country .
_Citation.WWW_URL .
_Citation.Page_first 431
_Citation.Page_last 435
_Citation.Year 2002
_Citation.Details .
loop_
_Citation_author.Ordinal
_Citation_author.Given_name
_Citation_author.Family_name
_Citation_author.First_initial
_Citation_author.Middle_initials
_Citation_author.Family_title
_Citation_author.Entry_ID
_Citation_author.Citation_ID
1 Anna Huppler . E. . 5371 1
2 Laura Nikstad . J. . 5371 1
3 Anne Allmann . M. . 5371 1
4 David Brow . A. . 5371 1
5 Samuel Butcher . E. . 5371 1
stop_
loop_
_Citation_keyword.Keyword
_Citation_keyword.Entry_ID
_Citation_keyword.Citation_ID
RNA 5371 1
U6 5371 1
stop_
save_
#############################################
# Molecular system (assembly) description #
#############################################
save_system_U6_snRNA_ISL
_Assembly.Sf_category assembly
_Assembly.Sf_framecode system_U6_snRNA_ISL
_Assembly.Entry_ID 5371
_Assembly.ID 1
_Assembly.Name 'U6 RNA'
_Assembly.BMRB_code .
_Assembly.Number_of_components .
_Assembly.Organic_ligands .
_Assembly.Metal_ions .
_Assembly.Non_standard_bonds .
_Assembly.Ambiguous_conformational_states .
_Assembly.Ambiguous_chem_comp_sites .
_Assembly.Molecules_in_chemical_exchange .
_Assembly.Paramagnetic no
_Assembly.Thiol_state 'not present'
_Assembly.Molecular_mass .
_Assembly.Enzyme_commission_number .
_Assembly.Details .
_Assembly.DB_query_date .
_Assembly.DB_query_revised_last_date .
loop_
_Assembly_type.Type
_Assembly_type.Entry_ID
_Assembly_type.Assembly_ID
monomer 5371 1
stop_
loop_
_Entity_assembly.ID
_Entity_assembly.Entity_assembly_name
_Entity_assembly.Entity_ID
_Entity_assembly.Entity_label
_Entity_assembly.Asym_ID
_Entity_assembly.PDB_chain_ID
_Entity_assembly.Experimental_data_reported
_Entity_assembly.Physical_state
_Entity_assembly.Conformational_isomer
_Entity_assembly.Chemical_exchange_state
_Entity_assembly.Magnetic_equivalence_group_code
_Entity_assembly.Role
_Entity_assembly.Details
_Entity_assembly.Entry_ID
_Entity_assembly.Assembly_ID
1 'U6 RNA 1' 1 $ISL_monomer . . . native . . . . . 5371 1
stop_
loop_
_Assembly_db_link.Author_supplied
_Assembly_db_link.Database_code
_Assembly_db_link.Accession_code
_Assembly_db_link.Entry_mol_code
_Assembly_db_link.Entry_mol_name
_Assembly_db_link.Entry_experimental_method
_Assembly_db_link.Entry_structure_resolution
_Assembly_db_link.Entry_relation_type
_Assembly_db_link.Entry_details
_Assembly_db_link.Entry_ID
_Assembly_db_link.Assembly_ID
. PDB 1LC6 . . . . . . 5371 1
stop_
loop_
_Assembly_common_name.Name
_Assembly_common_name.Type
_Assembly_common_name.Entry_ID
_Assembly_common_name.Assembly_ID
'U6 RNA' system 5371 1
'U6 snRNA ISL' abbreviation 5371 1
stop_
loop_
_Assembly_bio_function.Biological_function
_Assembly_bio_function.Entry_ID
_Assembly_bio_function.Assembly_ID
'pre-mRNA splicing' 5371 1
stop_
save_
####################################
# Biological polymers and ligands #
####################################
save_ISL_monomer
_Entity.Sf_category entity
_Entity.Sf_framecode ISL_monomer
_Entity.Entry_ID 5371
_Entity.ID 1
_Entity.BMRB_code .
_Entity.Name 'U6 RNA'
_Entity.Type polymer
_Entity.Polymer_common_type .
_Entity.Polymer_type polyribonucleotide
_Entity.Polymer_type_details .
_Entity.Polymer_strand_ID .
_Entity.Polymer_seq_one_letter_code_can .
_Entity.Polymer_seq_one_letter_code
;
GGUUCCCCUGCAUAAGGAUG
AACC
;
_Entity.Target_identifier .
_Entity.Polymer_author_defined_seq .
_Entity.Polymer_author_seq_details .
_Entity.Ambiguous_conformational_states .
_Entity.Ambiguous_chem_comp_sites .
_Entity.Nstd_monomer .
_Entity.Nstd_chirality .
_Entity.Nstd_linkage .
_Entity.Nonpolymer_comp_ID .
_Entity.Nonpolymer_comp_label .
_Entity.Number_of_monomers 24
_Entity.Number_of_nonpolymer_components .
_Entity.Paramagnetic .
_Entity.Thiol_state 'not present'
_Entity.Src_method .
_Entity.Parent_entity_ID 1
_Entity.Fragment .
_Entity.Mutation .
_Entity.EC_number .
_Entity.Calc_isoelectric_point .
_Entity.Formula_weight .
_Entity.Formula_weight_exptl .
_Entity.Formula_weight_exptl_meth .
_Entity.Details .
_Entity.DB_query_date .
_Entity.DB_query_revised_last_date .
loop_
_Entity_common_name.Name
_Entity_common_name.Type
_Entity_common_name.Entry_ID
_Entity_common_name.Entity_ID
'U6 RNA' common 5371 1
'U6 snRNA ISL' abbreviation 5371 1
stop_
loop_
_Entity_comp_index.ID
_Entity_comp_index.Auth_seq_ID
_Entity_comp_index.Comp_ID
_Entity_comp_index.Comp_label
_Entity_comp_index.Entry_ID
_Entity_comp_index.Entity_ID
1 . G . 5371 1
2 . G . 5371 1
3 . U . 5371 1
4 . U . 5371 1
5 . C . 5371 1
6 . C . 5371 1
7 . C . 5371 1
8 . C . 5371 1
9 . U . 5371 1
10 . G . 5371 1
11 . C . 5371 1
12 . A . 5371 1
13 . U . 5371 1
14 . A . 5371 1
15 . A . 5371 1
16 . G . 5371 1
17 . G . 5371 1
18 . A . 5371 1
19 . U . 5371 1
20 . G . 5371 1
21 . A . 5371 1
22 . A . 5371 1
23 . C . 5371 1
24 . C . 5371 1
stop_
loop_
_Entity_poly_seq.Hetero
_Entity_poly_seq.Mon_ID
_Entity_poly_seq.Num
_Entity_poly_seq.Comp_index_ID
_Entity_poly_seq.Entry_ID
_Entity_poly_seq.Entity_ID
. G 1 1 5371 1
. G 2 2 5371 1
. U 3 3 5371 1
. U 4 4 5371 1
. C 5 5 5371 1
. C 6 6 5371 1
. C 7 7 5371 1
. C 8 8 5371 1
. U 9 9 5371 1
. G 10 10 5371 1
. C 11 11 5371 1
. A 12 12 5371 1
. U 13 13 5371 1
. A 14 14 5371 1
. A 15 15 5371 1
. G 16 16 5371 1
. G 17 17 5371 1
. A 18 18 5371 1
. U 19 19 5371 1
. G 20 20 5371 1
. A 21 21 5371 1
. A 22 22 5371 1
. C 23 23 5371 1
. C 24 24 5371 1
stop_
save_
####################
# Natural source #
####################
save_natural_source
_Entity_natural_src_list.Sf_category natural_source
_Entity_natural_src_list.Sf_framecode natural_source
_Entity_natural_src_list.Entry_ID 5371
_Entity_natural_src_list.ID 1
loop_
_Entity_natural_src.ID
_Entity_natural_src.Entity_ID
_Entity_natural_src.Entity_label
_Entity_natural_src.Entity_chimera_segment_ID
_Entity_natural_src.NCBI_taxonomy_ID
_Entity_natural_src.Type
_Entity_natural_src.Common
_Entity_natural_src.Organism_name_scientific
_Entity_natural_src.Organism_name_common
_Entity_natural_src.Organism_acronym
_Entity_natural_src.ICTVdb_decimal_code
_Entity_natural_src.Superkingdom
_Entity_natural_src.Kingdom
_Entity_natural_src.Genus
_Entity_natural_src.Species
_Entity_natural_src.Strain
_Entity_natural_src.Variant
_Entity_natural_src.Subvariant
_Entity_natural_src.Organ
_Entity_natural_src.Tissue
_Entity_natural_src.Tissue_fraction
_Entity_natural_src.Cell_line
_Entity_natural_src.Cell_type
_Entity_natural_src.ATCC_number
_Entity_natural_src.Organelle
_Entity_natural_src.Cellular_location
_Entity_natural_src.Fragment
_Entity_natural_src.Fraction
_Entity_natural_src.Secretion
_Entity_natural_src.Plasmid
_Entity_natural_src.Plasmid_details
_Entity_natural_src.Gene_mnemonic
_Entity_natural_src.Dev_stage
_Entity_natural_src.Details
_Entity_natural_src.Citation_ID
_Entity_natural_src.Citation_label
_Entity_natural_src.Entry_ID
_Entity_natural_src.Entity_natural_src_list_ID
1 1 $ISL_monomer . 4932 organism . 'Saccharomyces cerevisiae' 'Baker's yeast' . . Eukaryota Fungi Saccharomyces cerevisiae . . . . . . . . . . . . . . . . . . . . . 5371 1
stop_
save_
#########################
# Experimental source #
#########################
save_experimental_source
_Entity_experimental_src_list.Sf_category experimental_source
_Entity_experimental_src_list.Sf_framecode experimental_source
_Entity_experimental_src_list.Entry_ID 5371
_Entity_experimental_src_list.ID 1
loop_
_Entity_experimental_src.ID
_Entity_experimental_src.Entity_ID
_Entity_experimental_src.Entity_label
_Entity_experimental_src.Entity_chimera_segment_ID
_Entity_experimental_src.Production_method
_Entity_experimental_src.Host_org_scientific_name
_Entity_experimental_src.Host_org_name_common
_Entity_experimental_src.Host_org_details
_Entity_experimental_src.Host_org_NCBI_taxonomy_ID
_Entity_experimental_src.Host_org_genus
_Entity_experimental_src.Host_org_species
_Entity_experimental_src.Host_org_strain
_Entity_experimental_src.Host_org_variant
_Entity_experimental_src.Host_org_subvariant
_Entity_experimental_src.Host_org_organ
_Entity_experimental_src.Host_org_tissue
_Entity_experimental_src.Host_org_tissue_fraction
_Entity_experimental_src.Host_org_cell_line
_Entity_experimental_src.Host_org_cell_type
_Entity_experimental_src.Host_org_cellular_location
_Entity_experimental_src.Host_org_organelle
_Entity_experimental_src.Host_org_gene
_Entity_experimental_src.Host_org_culture_collection
_Entity_experimental_src.Host_org_ATCC_number
_Entity_experimental_src.Vector_type
_Entity_experimental_src.PDBview_host_org_vector_name
_Entity_experimental_src.PDBview_plasmid_name
_Entity_experimental_src.Vector_name
_Entity_experimental_src.Vector_details
_Entity_experimental_src.Vendor_name
_Entity_experimental_src.Host_org_dev_stage
_Entity_experimental_src.Details
_Entity_experimental_src.Citation_ID
_Entity_experimental_src.Citation_label
_Entity_experimental_src.Entry_ID
_Entity_experimental_src.Entity_experimental_src_list_ID
1 1 $ISL_monomer . 'recombinant technology' . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5371 1
stop_
save_
#####################################
# Sample contents and methodology #
#####################################
########################
# Sample description #
########################
save_sample_1
_Sample.Sf_category sample
_Sample.Sf_framecode sample_1
_Sample.Entry_ID 5371
_Sample.ID 1
_Sample.Type solution
_Sample.Sub_type .
_Sample.Details .
_Sample.Aggregate_sample_number .
_Sample.Solvent_system .
_Sample.Preparation_date .
_Sample.Preparation_expiration_date .
_Sample.Polycrystallization_protocol .
_Sample.Single_crystal_protocol .
_Sample.Crystal_grow_apparatus .
_Sample.Crystal_grow_atmosphere .
_Sample.Crystal_grow_details .
_Sample.Crystal_grow_method .
_Sample.Crystal_grow_method_cit_ID .
_Sample.Crystal_grow_pH .
_Sample.Crystal_grow_pH_range .
_Sample.Crystal_grow_pressure .
_Sample.Crystal_grow_pressure_esd .
_Sample.Crystal_grow_seeding .
_Sample.Crystal_grow_seeding_cit_ID .
_Sample.Crystal_grow_temp .
_Sample.Crystal_grow_temp_details .
_Sample.Crystal_grow_temp_esd .
_Sample.Crystal_grow_time .
_Sample.Oriented_sample_prep_protocol .
_Sample.Lyophilization_cryo_protectant .
_Sample.Storage_protocol .
loop_
_Sample_component.ID
_Sample_component.Mol_common_name
_Sample_component.Isotopic_labeling
_Sample_component.Assembly_ID
_Sample_component.Assembly_label
_Sample_component.Entity_ID
_Sample_component.Entity_label
_Sample_component.Product_ID
_Sample_component.Type
_Sample_component.Concentration_val
_Sample_component.Concentration_val_min
_Sample_component.Concentration_val_max
_Sample_component.Concentration_val_units
_Sample_component.Concentration_val_err
_Sample_component.Vendor
_Sample_component.Vendor_product_name
_Sample_component.Vendor_product_code
_Sample_component.Entry_ID
_Sample_component.Sample_ID
1 'U6 RNA' '[U-100% 13C; U-15N]' . . 1 $ISL_monomer . . 1.0 0.5 1.5 mM . . . . 5371 1
stop_
save_
#######################
# Sample conditions #
#######################
save_cond_1
_Sample_condition_list.Sf_category sample_conditions
_Sample_condition_list.Sf_framecode cond_1
_Sample_condition_list.Entry_ID 5371
_Sample_condition_list.ID 1
_Sample_condition_list.Details .
loop_
_Sample_condition_variable.Type
_Sample_condition_variable.Val
_Sample_condition_variable.Val_err
_Sample_condition_variable.Val_units
_Sample_condition_variable.Entry_ID
_Sample_condition_variable.Sample_condition_list_ID
'ionic strength' 0.05 0.01 M 5371 1
pH 7.0 0.1 n/a 5371 1
temperature 303 0.5 K 5371 1
stop_
save_
#########################
# Experimental detail #
#########################
##################################
# NMR Spectrometer definitions #
##################################
save_spectrometer_1
_NMR_spectrometer.Sf_category NMR_spectrometer
_NMR_spectrometer.Sf_framecode spectrometer_1
_NMR_spectrometer.Entry_ID 5371
_NMR_spectrometer.ID 1
_NMR_spectrometer.Details 'spectrometer information not available'
_NMR_spectrometer.Manufacturer unknown
_NMR_spectrometer.Model unknown
_NMR_spectrometer.Serial_number .
_NMR_spectrometer.Field_strength 0
save_
save_spectrometer_list
_NMR_spectrometer_list.Sf_category NMR_spectrometer_list
_NMR_spectrometer_list.Sf_framecode spectrometer_list
_NMR_spectrometer_list.Entry_ID 5371
_NMR_spectrometer_list.ID 1
loop_
_NMR_spectrometer_view.ID
_NMR_spectrometer_view.Name
_NMR_spectrometer_view.Manufacturer
_NMR_spectrometer_view.Model
_NMR_spectrometer_view.Serial_number
_NMR_spectrometer_view.Field_strength
_NMR_spectrometer_view.Details
_NMR_spectrometer_view.Citation_ID
_NMR_spectrometer_view.Citation_label
_NMR_spectrometer_view.Entry_ID
_NMR_spectrometer_view.NMR_spectrometer_list_ID
1 spectrometer_1 unknown unknown . 0 'spectrometer information not available' . . 5371 1
stop_
save_
#############################
# NMR applied experiments #
#############################
save_experiment_list
_Experiment_list.Sf_category experiment_list
_Experiment_list.Sf_framecode experiment_list
_Experiment_list.Entry_ID 5371
_Experiment_list.ID 1
_Experiment_list.Details .
loop_
_Experiment.ID
_Experiment.Name
_Experiment.Raw_data_flag
_Experiment.NMR_spec_expt_ID
_Experiment.NMR_spec_expt_label
_Experiment.MS_expt_ID
_Experiment.MS_expt_label
_Experiment.SAXS_expt_ID
_Experiment.SAXS_expt_label
_Experiment.FRET_expt_ID
_Experiment.FRET_expt_label
_Experiment.EMR_expt_ID
_Experiment.EMR_expt_label
_Experiment.Sample_ID
_Experiment.Sample_label
_Experiment.Sample_state
_Experiment.Sample_volume
_Experiment.Sample_volume_units
_Experiment.Sample_condition_list_ID
_Experiment.Sample_condition_list_label
_Experiment.Sample_spinning_rate
_Experiment.Sample_angle
_Experiment.NMR_tube_type
_Experiment.NMR_spectrometer_ID
_Experiment.NMR_spectrometer_label
_Experiment.NMR_spectrometer_probe_ID
_Experiment.NMR_spectrometer_probe_label
_Experiment.NMR_spectral_processing_ID
_Experiment.NMR_spectral_processing_label
_Experiment.Mass_spectrometer_ID
_Experiment.Mass_spectrometer_label
_Experiment.Xray_instrument_ID
_Experiment.Xray_instrument_label
_Experiment.Fluorescence_instrument_ID
_Experiment.Fluorescence_instrument_label
_Experiment.EMR_instrument_ID
_Experiment.EMR_instrument_label
_Experiment.Chromatographic_system_ID
_Experiment.Chromatographic_system_label
_Experiment.Chromatographic_column_ID
_Experiment.Chromatographic_column_label
_Experiment.Entry_ID
_Experiment.Experiment_list_ID
1 . . . . . . . . . . . . 1 $sample_1 . . . 1 $cond_1 . . . 1 $spectrometer_1 . . . . . . . . . . . . . . . . 5371 1
stop_
save_
####################
# NMR parameters #
####################
##############################
# Assigned chemical shifts #
##############################
################################
# Chemical shift referencing #
################################
save_chemical_shift_reference
_Chem_shift_reference.Sf_category chem_shift_reference
_Chem_shift_reference.Sf_framecode chemical_shift_reference
_Chem_shift_reference.Entry_ID 5371
_Chem_shift_reference.ID 1
_Chem_shift_reference.Details .
loop_
_Chem_shift_ref.Atom_type
_Chem_shift_ref.Atom_isotope_number
_Chem_shift_ref.Mol_common_name
_Chem_shift_ref.Atom_group
_Chem_shift_ref.Concentration_val
_Chem_shift_ref.Concentration_units
_Chem_shift_ref.Solvent
_Chem_shift_ref.Rank
_Chem_shift_ref.Chem_shift_units
_Chem_shift_ref.Chem_shift_val
_Chem_shift_ref.Ref_method
_Chem_shift_ref.Ref_type
_Chem_shift_ref.Indirect_shift_ratio
_Chem_shift_ref.External_ref_loc
_Chem_shift_ref.External_ref_sample_geometry
_Chem_shift_ref.External_ref_axis
_Chem_shift_ref.Indirect_shift_ratio_cit_ID
_Chem_shift_ref.Indirect_shift_ratio_cit_label
_Chem_shift_ref.Ref_correction_type
_Chem_shift_ref.Correction_val
_Chem_shift_ref.Correction_val_cit_ID
_Chem_shift_ref.Correction_val_cit_label
_Chem_shift_ref.Entry_ID
_Chem_shift_ref.Chem_shift_reference_ID
H 1 TSP 'methyl protons' . . . . ppm 0 internal indirect 1.0 internal cylindrical parallel 1 $entry_citation . . 1 $entry_citation 5371 1
stop_
save_
###################################
# Assigned chemical shift lists #
###################################
###################################################################
# Chemical Shift Ambiguity Index Value Definitions #
# #
# The values other than 1 are used for those atoms with different #
# chemical shifts that cannot be assigned to stereospecific atoms #
# or to specific residues or chains. #
# #
# Index Value Definition #
# #
# 1 Unique (including isolated methyl protons, #
# geminal atoms, and geminal methyl #
# groups with identical chemical shifts) #
# (e.g. ILE HD11, HD12, HD13 protons) #
# 2 Ambiguity of geminal atoms or geminal methyl #
# proton groups (e.g. ASP HB2 and HB3 #
# protons, LEU CD1 and CD2 carbons, or #
# LEU HD11, HD12, HD13 and HD21, HD22, #
# HD23 methyl protons) #
# 3 Aromatic atoms on opposite sides of #
# symmetrical rings (e.g. TYR HE1 and HE2 #
# protons) #
# 4 Intraresidue ambiguities (e.g. LYS HG and #
# HD protons or TRP HZ2 and HZ3 protons) #
# 5 Interresidue ambiguities (LYS 12 vs. LYS 27) #
# 6 Intermolecular ambiguities (e.g. ASP 31 CA #
# in monomer 1 and ASP 31 CA in monomer 2 #
# of an asymmetrical homodimer, duplex #
# DNA assignments, or other assignments #
# that may apply to atoms in one or more #
# molecule in the molecular assembly) #
# 9 Ambiguous, specific ambiguity not defined #
# #
###################################################################
save_shift_set_1
_Assigned_chem_shift_list.Sf_category assigned_chemical_shifts
_Assigned_chem_shift_list.Sf_framecode shift_set_1
_Assigned_chem_shift_list.Entry_ID 5371
_Assigned_chem_shift_list.ID 1
_Assigned_chem_shift_list.Sample_condition_list_ID 1
_Assigned_chem_shift_list.Sample_condition_list_label $cond_1
_Assigned_chem_shift_list.Chem_shift_reference_ID 1
_Assigned_chem_shift_list.Chem_shift_reference_label $chemical_shift_reference
_Assigned_chem_shift_list.Chem_shift_1H_err .
_Assigned_chem_shift_list.Chem_shift_13C_err .
_Assigned_chem_shift_list.Chem_shift_15N_err .
_Assigned_chem_shift_list.Chem_shift_31P_err .
_Assigned_chem_shift_list.Chem_shift_2H_err .
_Assigned_chem_shift_list.Chem_shift_19F_err .
_Assigned_chem_shift_list.Error_derivation_method .
_Assigned_chem_shift_list.Details .
_Assigned_chem_shift_list.Text_data_format .
_Assigned_chem_shift_list.Text_data .
loop_
_Chem_shift_experiment.Experiment_ID
_Chem_shift_experiment.Experiment_name
_Chem_shift_experiment.Sample_ID
_Chem_shift_experiment.Sample_label
_Chem_shift_experiment.Sample_state
_Chem_shift_experiment.Entry_ID
_Chem_shift_experiment.Assigned_chem_shift_list_ID
. . 1 $sample_1 . 5371 1
stop_
loop_
_Atom_chem_shift.ID
_Atom_chem_shift.Assembly_atom_ID
_Atom_chem_shift.Entity_assembly_ID
_Atom_chem_shift.Entity_ID
_Atom_chem_shift.Comp_index_ID
_Atom_chem_shift.Seq_ID
_Atom_chem_shift.Comp_ID
_Atom_chem_shift.Atom_ID
_Atom_chem_shift.Atom_type
_Atom_chem_shift.Atom_isotope_number
_Atom_chem_shift.Val
_Atom_chem_shift.Val_err
_Atom_chem_shift.Assign_fig_of_merit
_Atom_chem_shift.Ambiguity_code
_Atom_chem_shift.Occupancy
_Atom_chem_shift.Resonance_ID
_Atom_chem_shift.Auth_entity_assembly_ID
_Atom_chem_shift.Auth_asym_ID
_Atom_chem_shift.Auth_seq_ID
_Atom_chem_shift.Auth_comp_ID
_Atom_chem_shift.Auth_atom_ID
_Atom_chem_shift.Details
_Atom_chem_shift.Entry_ID
_Atom_chem_shift.Assigned_chem_shift_list_ID
1 . 1 1 1 1 G H1' H 1 5.834 0.001 . . . . . . . . . . 5371 1
2 . 1 1 1 1 G H2' H 1 4.969 0.013 . . . . . . . . . . 5371 1
3 . 1 1 1 1 G H3' H 1 4.756 0.001 . . . . . . . . . . 5371 1
4 . 1 1 1 1 G H4' H 1 4.553 0.001 . . . . . . . . . . 5371 1
5 . 1 1 1 1 G H5' H 1 4.441 0.009 . . . . . . . . . . 5371 1
6 . 1 1 1 1 G H5'' H 1 4.268 0.007 . . . . . . . . . . 5371 1
7 . 1 1 1 1 G H8 H 1 8.169 0.001 . . . . . . . . . . 5371 1
8 . 1 1 1 1 G H1 H 1 12.852 0.014 . . . . . . . . . . 5371 1
9 . 1 1 1 1 G C8 C 13 138.7 0.020 . . . . . . . . . . 5371 1
10 . 1 1 1 1 G N1 N 15 146.9 0.020 . . . . . . . . . . 5371 1
11 . 1 1 2 2 G H1' H 1 5.933 0.003 . . . . . . . . . . 5371 1
12 . 1 1 2 2 G H2' H 1 4.592 0.001 . . . . . . . . . . 5371 1
13 . 1 1 2 2 G H3' H 1 4.559 0.006 . . . . . . . . . . 5371 1
14 . 1 1 2 2 G H4' H 1 4.534 0.006 . . . . . . . . . . 5371 1
15 . 1 1 2 2 G H5' H 1 4.502 0.010 . . . . . . . . . . 5371 1
16 . 1 1 2 2 G H5'' H 1 4.245 0.005 . . . . . . . . . . 5371 1
17 . 1 1 2 2 G H8 H 1 7.588 0.003 . . . . . . . . . . 5371 1
18 . 1 1 2 2 G H1 H 1 13.454 0.005 . . . . . . . . . . 5371 1
19 . 1 1 2 2 G H21 H 1 8.594 0.000 . . . . . . . . . . 5371 1
20 . 1 1 2 2 G H22 H 1 6.188 0.000 . . . . . . . . . . 5371 1
21 . 1 1 2 2 G N1 N 15 148 0.020 . . . . . . . . . . 5371 1
22 . 1 1 3 3 U H1' H 1 5.606 0.005 . . . . . . . . . . 5371 1
23 . 1 1 3 3 U H2' H 1 4.531 0.017 . . . . . . . . . . 5371 1
24 . 1 1 3 3 U H3' H 1 4.537 0.007 . . . . . . . . . . 5371 1
25 . 1 1 3 3 U H4' H 1 4.450 0.000 . . . . . . . . . . 5371 1
26 . 1 1 3 3 U H5 H 1 5.147 0.003 . . . . . . . . . . 5371 1
27 . 1 1 3 3 U H5' H 1 4.590 0.001 . . . . . . . . . . 5371 1
28 . 1 1 3 3 U H5'' H 1 4.148 0.007 . . . . . . . . . . 5371 1
29 . 1 1 3 3 U H6 H 1 7.828 0.009 . . . . . . . . . . 5371 1
30 . 1 1 3 3 U H3 H 1 14.458 0.005 . . . . . . . . . . 5371 1
31 . 1 1 3 3 U C6 C 13 141.1 0.020 . . . . . . . . . . 5371 1
32 . 1 1 3 3 U C5 C 13 102.3 0.020 . . . . . . . . . . 5371 1
33 . 1 1 3 3 U N3 N 15 162.3 0.020 . . . . . . . . . . 5371 1
34 . 1 1 4 4 U H1' H 1 5.694 0.007 . . . . . . . . . . 5371 1
35 . 1 1 4 4 U H2' H 1 4.513 0.008 . . . . . . . . . . 5371 1
36 . 1 1 4 4 U H3' H 1 4.526 0.001 . . . . . . . . . . 5371 1
37 . 1 1 4 4 U H4' H 1 4.507 0.000 . . . . . . . . . . 5371 1
38 . 1 1 4 4 U H5 H 1 5.631 0.006 . . . . . . . . . . 5371 1
39 . 1 1 4 4 U H5' H 1 4.554 0.005 . . . . . . . . . . 5371 1
40 . 1 1 4 4 U H5'' H 1 4.141 0.001 . . . . . . . . . . 5371 1
41 . 1 1 4 4 U H6 H 1 8.028 0.003 . . . . . . . . . . 5371 1
42 . 1 1 4 4 U H3 H 1 13.795 0.005 . . . . . . . . . . 5371 1
43 . 1 1 4 4 U N3 N 15 162.4 0.020 . . . . . . . . . . 5371 1
44 . 1 1 4 4 U C6 C 13 142 0.020 . . . . . . . . . . 5371 1
45 . 1 1 4 4 U C5 C 13 102.7 0.020 . . . . . . . . . . 5371 1
46 . 1 1 5 5 C H1' H 1 5.599 0.006 . . . . . . . . . . 5371 1
47 . 1 1 5 5 C H2' H 1 4.275 0.002 . . . . . . . . . . 5371 1
48 . 1 1 5 5 C H3' H 1 4.466 0.007 . . . . . . . . . . 5371 1
49 . 1 1 5 5 C H4' H 1 4.460 0.000 . . . . . . . . . . 5371 1
50 . 1 1 5 5 C H5 H 1 5.734 0.021 . . . . . . . . . . 5371 1
51 . 1 1 5 5 C H5' H 1 4.562 0.007 . . . . . . . . . . 5371 1
52 . 1 1 5 5 C H5'' H 1 4.130 0.004 . . . . . . . . . . 5371 1
53 . 1 1 5 5 C H6 H 1 7.859 0.007 . . . . . . . . . . 5371 1
54 . 1 1 5 5 C H41 H 1 8.438 0.001 . . . . . . . . . . 5371 1
55 . 1 1 5 5 C H42 H 1 7.130 0.000 . . . . . . . . . . 5371 1
56 . 1 1 5 5 C C6 C 13 141.4 0.020 . . . . . . . . . . 5371 1
57 . 1 1 5 5 C C5 C 13 97.1 0.020 . . . . . . . . . . 5371 1
58 . 1 1 5 5 C N4 N 15 98.4 0.020 . . . . . . . . . . 5371 1
59 . 1 1 6 6 C H3' H 1 4.601 0.003 . . . . . . . . . . 5371 1
60 . 1 1 6 6 C H4' H 1 4.354 0.001 . . . . . . . . . . 5371 1
61 . 1 1 6 6 C H5 H 1 5.656 0.004 . . . . . . . . . . 5371 1
62 . 1 1 6 6 C H5' H 1 4.550 0.002 . . . . . . . . . . 5371 1
63 . 1 1 6 6 C H5'' H 1 4.109 0.010 . . . . . . . . . . 5371 1
64 . 1 1 6 6 C H6 H 1 7.773 0.004 . . . . . . . . . . 5371 1
65 . 1 1 6 6 C C6 C 13 141.5 0.020 . . . . . . . . . . 5371 1
66 . 1 1 6 6 C C5 C 13 97 0.020 . . . . . . . . . . 5371 1
67 . 1 1 7 7 C H1' H 1 5.413 0.003 . . . . . . . . . . 5371 1
68 . 1 1 7 7 C H2' H 1 4.397 0.006 . . . . . . . . . . 5371 1
69 . 1 1 7 7 C H3' H 1 4.519 0.006 . . . . . . . . . . 5371 1
70 . 1 1 7 7 C H4' H 1 4.417 0.004 . . . . . . . . . . 5371 1
71 . 1 1 7 7 C H5 H 1 5.721 0.004 . . . . . . . . . . 5371 1
72 . 1 1 7 7 C H5' H 1 4.470 0.002 . . . . . . . . . . 5371 1
73 . 1 1 7 7 C H5'' H 1 4.063 0.014 . . . . . . . . . . 5371 1
74 . 1 1 7 7 C H6 H 1 7.907 0.003 . . . . . . . . . . 5371 1
75 . 1 1 7 7 C H41 H 1 8.452 0.000 . . . . . . . . . . 5371 1
76 . 1 1 7 7 C H42 H 1 7.155 0.002 . . . . . . . . . . 5371 1
77 . 1 1 7 7 C C6 C 13 140.7 0.020 . . . . . . . . . . 5371 1
78 . 1 1 7 7 C C5 C 13 97 0.020 . . . . . . . . . . 5371 1
79 . 1 1 7 7 C N4 N 15 97.4 0.020 . . . . . . . . . . 5371 1
80 . 1 1 8 8 C H1' H 1 5.391 0.005 . . . . . . . . . . 5371 1
81 . 1 1 8 8 C H2' H 1 4.288 0.005 . . . . . . . . . . 5371 1
82 . 1 1 8 8 C H3' H 1 4.325 0.005 . . . . . . . . . . 5371 1
83 . 1 1 8 8 C H4' H 1 4.369 0.004 . . . . . . . . . . 5371 1
84 . 1 1 8 8 C H5 H 1 5.538 0.005 . . . . . . . . . . 5371 1
85 . 1 1 8 8 C H5' H 1 4.482 0.007 . . . . . . . . . . 5371 1
86 . 1 1 8 8 C H5'' H 1 4.005 0.006 . . . . . . . . . . 5371 1
87 . 1 1 8 8 C H6 H 1 7.770 0.006 . . . . . . . . . . 5371 1
88 . 1 1 8 8 C H41 H 1 8.404 0.000 . . . . . . . . . . 5371 1
89 . 1 1 8 8 C H42 H 1 6.977 0.007 . . . . . . . . . . 5371 1
90 . 1 1 8 8 C C6 C 13 141.5 0.020 . . . . . . . . . . 5371 1
91 . 1 1 8 8 C C5 C 13 97.3 0.020 . . . . . . . . . . 5371 1
92 . 1 1 8 8 C N4 N 15 97.3 0.020 . . . . . . . . . . 5371 1
93 . 1 1 9 9 U H1' H 1 5.582 0.003 . . . . . . . . . . 5371 1
94 . 1 1 9 9 U H2' H 1 4.477 0.004 . . . . . . . . . . 5371 1
95 . 1 1 9 9 U H3' H 1 4.353 0.007 . . . . . . . . . . 5371 1
96 . 1 1 9 9 U H5 H 1 5.303 0.004 . . . . . . . . . . 5371 1
97 . 1 1 9 9 U H5' H 1 4.497 0.020 . . . . . . . . . . 5371 1
98 . 1 1 9 9 U H5'' H 1 4.085 0.004 . . . . . . . . . . 5371 1
99 . 1 1 9 9 U H6 H 1 7.621 0.005 . . . . . . . . . . 5371 1
100 . 1 1 9 9 U H4' H 1 4.450 0.000 . . . . . . . . . . 5371 1
101 . 1 1 9 9 U H3 H 1 13.691 0.009 . . . . . . . . . . 5371 1
102 . 1 1 9 9 U C6 C 13 140.1 0.020 . . . . . . . . . . 5371 1
103 . 1 1 9 9 U C5 C 13 103.6 0.020 . . . . . . . . . . 5371 1
104 . 1 1 9 9 U N3 N 15 160.7 0.020 . . . . . . . . . . 5371 1
105 . 1 1 10 10 G H1' H 1 5.552 0.004 . . . . . . . . . . 5371 1
106 . 1 1 10 10 G H2' H 1 4.418 0.001 . . . . . . . . . . 5371 1
107 . 1 1 10 10 G H3' H 1 4.530 0.002 . . . . . . . . . . 5371 1
108 . 1 1 10 10 G H4' H 1 4.386 0.006 . . . . . . . . . . 5371 1
109 . 1 1 10 10 G H5' H 1 4.336 0.006 . . . . . . . . . . 5371 1
110 . 1 1 10 10 G H5'' H 1 4.083 0.004 . . . . . . . . . . 5371 1
111 . 1 1 10 10 G H8 H 1 7.677 0.003 . . . . . . . . . . 5371 1
112 . 1 1 10 10 G H1 H 1 10.881 0.010 . . . . . . . . . . 5371 1
113 . 1 1 10 10 G H22 H 1 7.131 0.000 . . . . . . . . . . 5371 1
114 . 1 1 10 10 G C8 C 13 136.6 0.020 . . . . . . . . . . 5371 1
115 . 1 1 10 10 G N1 N 15 145.8 0.020 . . . . . . . . . . 5371 1
116 . 1 1 11 11 C H1' H 1 5.279 0.004 . . . . . . . . . . 5371 1
117 . 1 1 11 11 C H2' H 1 3.900 0.003 . . . . . . . . . . 5371 1
118 . 1 1 11 11 C H3' H 1 4.214 0.007 . . . . . . . . . . 5371 1
119 . 1 1 11 11 C H4' H 1 3.875 0.012 . . . . . . . . . . 5371 1
120 . 1 1 11 11 C H5 H 1 5.493 0.003 . . . . . . . . . . 5371 1
121 . 1 1 11 11 C H5' H 1 4.067 0.013 . . . . . . . . . . 5371 1
122 . 1 1 11 11 C H5'' H 1 3.856 0.017 . . . . . . . . . . 5371 1
123 . 1 1 11 11 C H6 H 1 7.462 0.006 . . . . . . . . . . 5371 1
124 . 1 1 11 11 C C6 C 13 141.8 0.020 . . . . . . . . . . 5371 1
125 . 1 1 11 11 C C5 C 13 97.4 0.020 . . . . . . . . . . 5371 1
126 . 1 1 12 12 A H1' H 1 5.952 0.002 . . . . . . . . . . 5371 1
127 . 1 1 12 12 A H2 H 1 8.042 0.000 . . . . . . . . . . 5371 1
128 . 1 1 12 12 A H2' H 1 4.698 0.007 . . . . . . . . . . 5371 1
129 . 1 1 12 12 A H3' H 1 4.713 0.002 . . . . . . . . . . 5371 1
130 . 1 1 12 12 A H4' H 1 4.403 0.005 . . . . . . . . . . 5371 1
131 . 1 1 12 12 A H5' H 1 4.078 0.003 . . . . . . . . . . 5371 1
132 . 1 1 12 12 A H5'' H 1 3.961 0.009 . . . . . . . . . . 5371 1
133 . 1 1 12 12 A H8 H 1 8.217 0.004 . . . . . . . . . . 5371 1
134 . 1 1 12 12 A C8 C 13 141.4 0.020 . . . . . . . . . . 5371 1
135 . 1 1 12 12 A C2 C 13 156.6 0.020 . . . . . . . . . . 5371 1
136 . 1 1 13 13 U H1' H 1 5.904 0.003 . . . . . . . . . . 5371 1
137 . 1 1 13 13 U H2' H 1 4.423 0.008 . . . . . . . . . . 5371 1
138 . 1 1 13 13 U H3' H 1 4.706 0.003 . . . . . . . . . . 5371 1
139 . 1 1 13 13 U H4' H 1 4.458 0.001 . . . . . . . . . . 5371 1
140 . 1 1 13 13 U H5 H 1 5.843 0.003 . . . . . . . . . . 5371 1
141 . 1 1 13 13 U H5' H 1 4.221 0.004 . . . . . . . . . . 5371 1
142 . 1 1 13 13 U H5'' H 1 4.181 0.001 . . . . . . . . . . 5371 1
143 . 1 1 13 13 U H6 H 1 7.782 0.004 . . . . . . . . . . 5371 1
144 . 1 1 13 13 U C6 C 13 143.3 0.020 . . . . . . . . . . 5371 1
145 . 1 1 13 13 U C5 C 13 104.7 0.020 . . . . . . . . . . 5371 1
146 . 1 1 14 14 A H1' H 1 5.951 0.001 . . . . . . . . . . 5371 1
147 . 1 1 14 14 A H2 H 1 8.112 0.001 . . . . . . . . . . 5371 1
148 . 1 1 14 14 A H2' H 1 4.851 0.001 . . . . . . . . . . 5371 1
149 . 1 1 14 14 A H3' H 1 4.597 0.005 . . . . . . . . . . 5371 1
150 . 1 1 14 14 A H4' H 1 4.621 0.014 . . . . . . . . . . 5371 1
151 . 1 1 14 14 A H5' H 1 4.360 0.004 . . . . . . . . . . 5371 1
152 . 1 1 14 14 A H5'' H 1 4.237 0.005 . . . . . . . . . . 5371 1
153 . 1 1 14 14 A H8 H 1 8.042 0.006 . . . . . . . . . . 5371 1
154 . 1 1 14 14 A C8 C 13 139.6 0.020 . . . . . . . . . . 5371 1
155 . 1 1 14 14 A C2 C 13 154.8 0.020 . . . . . . . . . . 5371 1
156 . 1 1 15 15 A H2 H 1 7.595 0.001 . . . . . . . . . . 5371 1
157 . 1 1 15 15 A H2' H 1 4.671 0.000 . . . . . . . . . . 5371 1
158 . 1 1 15 15 A H3' H 1 4.481 0.007 . . . . . . . . . . 5371 1
159 . 1 1 15 15 A H4' H 1 4.471 0.006 . . . . . . . . . . 5371 1
160 . 1 1 15 15 A H5' H 1 4.371 0.006 . . . . . . . . . . 5371 1
161 . 1 1 15 15 A H5'' H 1 4.300 0.003 . . . . . . . . . . 5371 1
162 . 1 1 15 15 A H8 H 1 8.042 0.005 . . . . . . . . . . 5371 1
163 . 1 1 15 15 A H62 H 1 6.633 0.009 . . . . . . . . . . 5371 1
164 . 1 1 15 15 A C8 C 13 141.3 0.020 . . . . . . . . . . 5371 1
165 . 1 1 15 15 A C2 C 13 153 0.020 . . . . . . . . . . 5371 1
166 . 1 1 16 16 G H1' H 1 5.583 0.006 . . . . . . . . . . 5371 1
167 . 1 1 16 16 G H2' H 1 4.498 0.006 . . . . . . . . . . 5371 1
168 . 1 1 16 16 G H3' H 1 4.506 0.004 . . . . . . . . . . 5371 1
169 . 1 1 16 16 G H4' H 1 4.402 0.023 . . . . . . . . . . 5371 1
170 . 1 1 16 16 G H5' H 1 4.366 0.009 . . . . . . . . . . 5371 1
171 . 1 1 16 16 G H5'' H 1 4.057 0.004 . . . . . . . . . . 5371 1
172 . 1 1 16 16 G H8 H 1 7.089 0.003 . . . . . . . . . . 5371 1
173 . 1 1 16 16 G H1 H 1 12.746 0.008 . . . . . . . . . . 5371 1
174 . 1 1 16 16 G H22 H 1 6.094 0.000 . . . . . . . . . . 5371 1
175 . 1 1 16 16 G C8 C 13 135.4 0.020 . . . . . . . . . . 5371 1
176 . 1 1 16 16 G N1 N 15 146.7 0.020 . . . . . . . . . . 5371 1
177 . 1 1 17 17 G H1' H 1 5.716 0.005 . . . . . . . . . . 5371 1
178 . 1 1 17 17 G H2' H 1 4.457 0.001 . . . . . . . . . . 5371 1
179 . 1 1 17 17 G H3' H 1 4.505 0.005 . . . . . . . . . . 5371 1
180 . 1 1 17 17 G H4' H 1 4.408 0.003 . . . . . . . . . . 5371 1
181 . 1 1 17 17 G H5' H 1 4.470 0.001 . . . . . . . . . . 5371 1
182 . 1 1 17 17 G H5'' H 1 4.050 0.002 . . . . . . . . . . 5371 1
183 . 1 1 17 17 G H8 H 1 7.211 0.004 . . . . . . . . . . 5371 1
184 . 1 1 17 17 G H1 H 1 12.665 0.005 . . . . . . . . . . 5371 1
185 . 1 1 17 17 G C8 C 13 135.8 0.020 . . . . . . . . . . 5371 1
186 . 1 1 17 17 G N1 N 15 147.7 0.020 . . . . . . . . . . 5371 1
187 . 1 1 18 18 A H1' H 1 5.922 0.004 . . . . . . . . . . 5371 1
188 . 1 1 18 18 A H2 H 1 7.776 0.000 . . . . . . . . . . 5371 1
189 . 1 1 18 18 A H2' H 1 4.457 0.011 . . . . . . . . . . 5371 1
190 . 1 1 18 18 A H3' H 1 4.350 0.007 . . . . . . . . . . 5371 1
191 . 1 1 18 18 A H4' H 1 4.462 0.001 . . . . . . . . . . 5371 1
192 . 1 1 18 18 A H5' H 1 4.395 0.007 . . . . . . . . . . 5371 1
193 . 1 1 18 18 A H5'' H 1 4.029 0.014 . . . . . . . . . . 5371 1
194 . 1 1 18 18 A H8 H 1 7.706 0.007 . . . . . . . . . . 5371 1
195 . 1 1 18 18 A C8 C 13 139.3 0.020 . . . . . . . . . . 5371 1
196 . 1 1 18 18 A C2 C 13 153.7 0.020 . . . . . . . . . . 5371 1
197 . 1 1 19 19 U H1' H 1 5.300 0.003 . . . . . . . . . . 5371 1
198 . 1 1 19 19 U H2' H 1 4.094 0.007 . . . . . . . . . . 5371 1
199 . 1 1 19 19 U H3' H 1 4.363 0.002 . . . . . . . . . . 5371 1
200 . 1 1 19 19 U H4' H 1 4.300 0.009 . . . . . . . . . . 5371 1
201 . 1 1 19 19 U H5 H 1 5.190 0.004 . . . . . . . . . . 5371 1
202 . 1 1 19 19 U H5' H 1 4.322 0.006 . . . . . . . . . . 5371 1
203 . 1 1 19 19 U H5'' H 1 4.026 0.001 . . . . . . . . . . 5371 1
204 . 1 1 19 19 U H6 H 1 7.281 0.002 . . . . . . . . . . 5371 1
205 . 1 1 19 19 U C6 C 13 140.7 0.020 . . . . . . . . . . 5371 1
206 . 1 1 19 19 U C5 C 13 103.2 0.020 . . . . . . . . . . 5371 1
207 . 1 1 20 20 G H1' H 1 5.738 0.003 . . . . . . . . . . 5371 1
208 . 1 1 20 20 G H2' H 1 4.745 0.002 . . . . . . . . . . 5371 1
209 . 1 1 20 20 G H3' H 1 4.610 0.007 . . . . . . . . . . 5371 1
210 . 1 1 20 20 G H4' H 1 4.467 0.000 . . . . . . . . . . 5371 1
211 . 1 1 20 20 G H5' H 1 4.322 0.006 . . . . . . . . . . 5371 1
212 . 1 1 20 20 G H5'' H 1 4.114 0.019 . . . . . . . . . . 5371 1
213 . 1 1 20 20 G H8 H 1 7.678 0.014 . . . . . . . . . . 5371 1
214 . 1 1 20 20 G H1 H 1 12.492 0.006 . . . . . . . . . . 5371 1
215 . 1 1 20 20 G H21 H 1 7.920 0.000 . . . . . . . . . . 5371 1
216 . 1 1 20 20 G H22 H 1 5.937 0.002 . . . . . . . . . . 5371 1
217 . 1 1 20 20 G C8 C 13 136.7 0.020 . . . . . . . . . . 5371 1
218 . 1 1 20 20 G N1 N 15 147 0.020 . . . . . . . . . . 5371 1
219 . 1 1 21 21 A H1' H 1 5.940 0.003 . . . . . . . . . . 5371 1
220 . 1 1 21 21 A H2 H 1 7.190 0.001 . . . . . . . . . . 5371 1
221 . 1 1 21 21 A H2' H 1 4.642 0.001 . . . . . . . . . . 5371 1
222 . 1 1 21 21 A H3' H 1 4.596 0.013 . . . . . . . . . . 5371 1
223 . 1 1 21 21 A H4' H 1 5.288 0.003 . . . . . . . . . . 5371 1
224 . 1 1 21 21 A H5' H 1 4.479 0.007 . . . . . . . . . . 5371 1
225 . 1 1 21 21 A H5'' H 1 4.315 0.004 . . . . . . . . . . 5371 1
226 . 1 1 21 21 A H8 H 1 7.889 0.006 . . . . . . . . . . 5371 1
227 . 1 1 21 21 A H61 H 1 8.069 0.007 . . . . . . . . . . 5371 1
228 . 1 1 21 21 A H62 H 1 6.581 0.003 . . . . . . . . . . 5371 1
229 . 1 1 21 21 A C8 C 13 141.4 0.020 . . . . . . . . . . 5371 1
230 . 1 1 21 21 A C2 C 13 152.5 0.020 . . . . . . . . . . 5371 1
231 . 1 1 22 22 A H1' H 1 5.946 0.002 . . . . . . . . . . 5371 1
232 . 1 1 22 22 A H2 H 1 7.796 0.002 . . . . . . . . . . 5371 1
233 . 1 1 22 22 A H2' H 1 4.506 0.002 . . . . . . . . . . 5371 1
234 . 1 1 22 22 A H3' H 1 4.603 0.001 . . . . . . . . . . 5371 1
235 . 1 1 22 22 A H4' H 1 4.600 0.000 . . . . . . . . . . 5371 1
236 . 1 1 22 22 A H5' H 1 4.601 0.013 . . . . . . . . . . 5371 1
237 . 1 1 22 22 A H5'' H 1 4.136 0.006 . . . . . . . . . . 5371 1
238 . 1 1 22 22 A H8 H 1 7.845 0.005 . . . . . . . . . . 5371 1
239 . 1 1 22 22 A H61 H 1 8.306 0.010 . . . . . . . . . . 5371 1
240 . 1 1 22 22 A H62 H 1 6.734 0.006 . . . . . . . . . . 5371 1
241 . 1 1 22 22 A C8 C 13 140 0.020 . . . . . . . . . . 5371 1
242 . 1 1 22 22 A C2 C 13 153.6 0.020 . . . . . . . . . . 5371 1
243 . 1 1 23 23 C H1' H 1 5.392 0.004 . . . . . . . . . . 5371 1
244 . 1 1 23 23 C H2' H 1 4.111 0.000 . . . . . . . . . . 5371 1
245 . 1 1 23 23 C H3' H 1 4.356 0.009 . . . . . . . . . . 5371 1
246 . 1 1 23 23 C H4' H 1 4.482 0.003 . . . . . . . . . . 5371 1
247 . 1 1 23 23 C H5 H 1 5.178 0.004 . . . . . . . . . . 5371 1
248 . 1 1 23 23 C H5' H 1 4.044 0.013 . . . . . . . . . . 5371 1
249 . 1 1 23 23 C H5'' H 1 4.013 0.010 . . . . . . . . . . 5371 1
250 . 1 1 23 23 C H6 H 1 7.447 0.003 . . . . . . . . . . 5371 1
251 . 1 1 23 23 C H41 H 1 8.388 0.000 . . . . . . . . . . 5371 1
252 . 1 1 23 23 C H42 H 1 7.050 0.002 . . . . . . . . . . 5371 1
253 . 1 1 23 23 C C6 C 13 140.2 0.020 . . . . . . . . . . 5371 1
254 . 1 1 23 23 C C5 C 13 96.6 0.020 . . . . . . . . . . 5371 1
255 . 1 1 23 23 C N4 N 15 98.9 0.020 . . . . . . . . . . 5371 1
256 . 1 1 24 24 C H1' H 1 5.777 0.004 . . . . . . . . . . 5371 1
257 . 1 1 24 24 C H2' H 1 3.999 0.002 . . . . . . . . . . 5371 1
258 . 1 1 24 24 C H3' H 1 4.161 0.000 . . . . . . . . . . 5371 1
259 . 1 1 24 24 C H4' H 1 4.141 0.000 . . . . . . . . . . 5371 1
260 . 1 1 24 24 C H5 H 1 5.453 0.006 . . . . . . . . . . 5371 1
261 . 1 1 24 24 C H5' H 1 4.448 0.004 . . . . . . . . . . 5371 1
262 . 1 1 24 24 C H5'' H 1 4.008 0.008 . . . . . . . . . . 5371 1
263 . 1 1 24 24 C H6 H 1 7.637 0.004 . . . . . . . . . . 5371 1
264 . 1 1 24 24 C C6 C 13 141.5 0.020 . . . . . . . . . . 5371 1
265 . 1 1 24 24 C C5 C 13 97.6 0.020 . . . . . . . . . . 5371 1
266 . 1 1 24 24 C N4 N 15 98.3 0.020 . . . . . . . . . . 5371 1
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