data_5996 ####################### # Entry information # ####################### save_entry_information _Entry.Sf_category entry_information _Entry.Sf_framecode entry_information _Entry.ID 5996 _Entry.Title ; Temperature Dependent Spectral Density Analysis Applied to Monitoring Backbone Dynamics of Major Urinary Protein-I Complexed with the Pheromone 2-sec-Butyl-4,5-dihyrothiazole ; _Entry.Type macromolecule _Entry.Version_type original _Entry.Submission_date 2003-11-05 _Entry.Accession_date 2003-11-05 _Entry.Last_release_date 2004-04-07 _Entry.Original_release_date 2004-04-07 _Entry.Origination author _Entry.NMR_STAR_version 3.1.2.6 _Entry.Original_NMR_STAR_version 2.1 _Entry.Experimental_method NMR _Entry.Experimental_method_subtype . _Entry.Details . _Entry.BMRB_internal_directory_name . loop_ _Entry_author.Ordinal _Entry_author.Given_name _Entry_author.Family_name _Entry_author.First_initial _Entry_author.Middle_initials _Entry_author.Family_title _Entry_author.ORCID _Entry_author.Entry_ID 1 Hana Krizova . . . . 5996 2 Lukas Zidek . . . . 5996 3 Martin Stone . J. . . 5996 4 Milos Novotny . V. . . 5996 5 Vladimir Sklenar . . . . 5996 stop_ loop_ _Data_set.Type _Data_set.Count _Data_set.Entry_ID assigned_chemical_shifts 1 5996 heteronucl_NOEs 9 5996 heteronucl_T1_relaxation 9 5996 heteronucl_T2_relaxation 9 5996 stop_ loop_ _Datum.Type _Datum.Count _Datum.Entry_ID '15N chemical shifts' 159 5996 '1H chemical shifts' 159 5996 'T1 relaxation values' 979 5996 'T2 relaxation values' 979 5996 'heteronuclear NOE values' 979 5996 stop_ loop_ _Release.Release_number _Release.Format_type _Release.Format_version _Release.Date _Release.Submission_date _Release.Type _Release.Author _Release.Detail _Release.Entry_ID 2 . . 2017-06-15 2003-11-05 update author 'update t2 data' 5996 1 . . 2004-04-07 2003-11-05 original author 'original release' 5996 stop_ loop_ _Related_entries.Database_name _Related_entries.Database_accession_code _Related_entries.Relationship _Related_entries.Entry_ID BMRB 5995 'Relaxation data of free form' 5996 stop_ save_ ############### # Citations # ############### save_entry_citation _Citation.Sf_category citations _Citation.Sf_framecode entry_citation _Citation.Entry_ID 5996 _Citation.ID 1 _Citation.Class 'entry citation' _Citation.CAS_abstract_code . _Citation.MEDLINE_UI_code . _Citation.DOI . _Citation.PubMed_ID 14872128 _Citation.Full_citation . _Citation.Title ; Temperature Dependent Spectral Density Analysis Applied to Monitoring Backbone Dynamics of Major Urinary Protein-I Complexed with the Pheromone 2-sec-butyl-4,5-dihyrothiazole ; _Citation.Status published _Citation.Type journal _Citation.Journal_abbrev 'J. Biomol. NMR' _Citation.Journal_name_full . _Citation.Journal_volume 28 _Citation.Journal_issue 4 _Citation.Journal_ASTM . _Citation.Journal_ISSN . _Citation.Journal_CSD . _Citation.Book_title . _Citation.Book_chapter_title . _Citation.Book_volume . _Citation.Book_series . _Citation.Book_publisher . _Citation.Book_publisher_city . _Citation.Book_ISBN . _Citation.Conference_title . _Citation.Conference_site . _Citation.Conference_state_province . _Citation.Conference_country . _Citation.Conference_start_date . _Citation.Conference_end_date . _Citation.Conference_abstract_number . _Citation.Thesis_institution . _Citation.Thesis_institution_city . _Citation.Thesis_institution_country . _Citation.WWW_URL . _Citation.Page_first 369 _Citation.Page_last 384 _Citation.Year 2004 _Citation.Details . loop_ _Citation_author.Ordinal _Citation_author.Given_name _Citation_author.Family_name _Citation_author.First_initial _Citation_author.Middle_initials _Citation_author.Family_title _Citation_author.ORCID _Citation_author.Entry_ID _Citation_author.Citation_ID 1 Hana Krizova . . . . 5996 1 2 Lukas Zidek . . . . 5996 1 3 Martin Stone . J. . . 5996 1 4 Milos Novotny . V. . . 5996 1 5 Vladimir Sklenar . . . . 5996 1 stop_ save_ ############################################# # Molecular system (assembly) description # ############################################# save_system_MUP-I _Assembly.Sf_category assembly _Assembly.Sf_framecode system_MUP-I _Assembly.Entry_ID 5996 _Assembly.ID 1 _Assembly.Name 'Major Urinary Protein-I' _Assembly.BMRB_code . _Assembly.Number_of_components . _Assembly.Organic_ligands . _Assembly.Metal_ions . _Assembly.Non_standard_bonds . _Assembly.Ambiguous_conformational_states . _Assembly.Ambiguous_chem_comp_sites . _Assembly.Molecules_in_chemical_exchange . _Assembly.Paramagnetic no _Assembly.Thiol_state 'disulfide bound and free' _Assembly.Molecular_mass . _Assembly.Enzyme_commission_number . _Assembly.Details . _Assembly.DB_query_date . _Assembly.DB_query_revised_last_date . loop_ _Assembly_type.Type _Assembly_type.Entry_ID _Assembly_type.Assembly_ID monomer 5996 1 stop_ loop_ _Entity_assembly.ID _Entity_assembly.Entity_assembly_name _Entity_assembly.Entity_ID _Entity_assembly.Entity_label _Entity_assembly.Asym_ID _Entity_assembly.PDB_chain_ID _Entity_assembly.Experimental_data_reported _Entity_assembly.Physical_state _Entity_assembly.Conformational_isomer _Entity_assembly.Chemical_exchange_state _Entity_assembly.Magnetic_equivalence_group_code _Entity_assembly.Role _Entity_assembly.Details _Entity_assembly.Entry_ID _Entity_assembly.Assembly_ID 1 MUP-I 1 $MUP-I . . . native . . . . . 5996 1 2 2-sec-butyl-4,5-dihydrothiazole 2 $entity_ZBT . . . native . . . . . 5996 1 stop_ loop_ _Bond.ID _Bond.Type _Bond.Value_order _Bond.Assembly_atom_ID_1 _Bond.Entity_assembly_ID_1 _Bond.Entity_assembly_name_1 _Bond.Entity_ID_1 _Bond.Comp_ID_1 _Bond.Comp_index_ID_1 _Bond.Seq_ID_1 _Bond.Atom_ID_1 _Bond.Assembly_atom_ID_2 _Bond.Entity_assembly_ID_2 _Bond.Entity_assembly_name_2 _Bond.Entity_ID_2 _Bond.Comp_ID_2 _Bond.Comp_index_ID_2 _Bond.Seq_ID_2 _Bond.Atom_ID_2 _Bond.Auth_entity_assembly_ID_1 _Bond.Auth_entity_assembly_name_1 _Bond.Auth_seq_ID_1 _Bond.Auth_comp_ID_1 _Bond.Auth_atom_ID_1 _Bond.Auth_entity_assembly_ID_2 _Bond.Auth_entity_assembly_name_2 _Bond.Auth_seq_ID_2 _Bond.Auth_comp_ID_2 _Bond.Auth_atom_ID_2 _Bond.Entry_ID _Bond.Assembly_ID 1 disulfide single . 1 . 1 CYS 64 64 SG . 1 . 1 CYS 157 157 SG . . . . . . . . . . 5996 1 stop_ loop_ _Assembly_db_link.Author_supplied _Assembly_db_link.Database_code _Assembly_db_link.Accession_code _Assembly_db_link.Entry_mol_code _Assembly_db_link.Entry_mol_name _Assembly_db_link.Entry_experimental_method _Assembly_db_link.Entry_structure_resolution _Assembly_db_link.Entry_relation_type _Assembly_db_link.Entry_details _Assembly_db_link.Entry_ID _Assembly_db_link.Assembly_ID yes PDB 1I04 . . . . . 'Four C-terminal residues are missing in the PDB file.' 5996 1 stop_ loop_ _Assembly_common_name.Name _Assembly_common_name.Type _Assembly_common_name.Entry_ID _Assembly_common_name.Assembly_ID MUP-I abbreviation 5996 1 'Major Urinary Protein-I' system 5996 1 stop_ loop_ _Assembly_bio_function.Biological_function _Assembly_bio_function.Entry_ID _Assembly_bio_function.Assembly_ID 'pheromone binding' 5996 1 stop_ save_ #################################### # Biological polymers and ligands # #################################### save_MUP-I _Entity.Sf_category entity _Entity.Sf_framecode MUP-I _Entity.Entry_ID 5996 _Entity.ID 1 _Entity.BMRB_code . _Entity.Name 'Major Urinary Protein-I' _Entity.Type polymer _Entity.Polymer_common_type . _Entity.Polymer_type polypeptide(L) _Entity.Polymer_type_details . _Entity.Polymer_strand_ID . _Entity.Polymer_seq_one_letter_code_can . _Entity.Polymer_seq_one_letter_code ; EEASSTGRNFNVEKINGEWH TIILASDKREKIEDNGNFRL FLEQIHVLENSLVLKFHTVR DEECSELSMVADKTEKAGEY SVTYDGFNTFTIPKTDYDNF LMAHLINEKDGETFQLMGLY GREPDLSSDIKERFAQLCEK HGILRENIIDLSNANRCLQA RE ; _Entity.Target_identifier . _Entity.Polymer_author_defined_seq . _Entity.Polymer_author_seq_details . _Entity.Ambiguous_conformational_states . _Entity.Ambiguous_chem_comp_sites . _Entity.Nstd_monomer . _Entity.Nstd_chirality . _Entity.Nstd_linkage . _Entity.Nonpolymer_comp_ID . _Entity.Nonpolymer_comp_label . _Entity.Number_of_monomers 162 _Entity.Number_of_nonpolymer_components . _Entity.Paramagnetic no _Entity.Thiol_state 'disulfide bound and free' _Entity.Src_method . _Entity.Parent_entity_ID 1 _Entity.Fragment . _Entity.Mutation . _Entity.EC_number . _Entity.Calc_isoelectric_point . _Entity.Formula_weight . _Entity.Formula_weight_exptl . _Entity.Formula_weight_exptl_meth . _Entity.Details . _Entity.DB_query_date . _Entity.DB_query_revised_last_date 2015-01-28 loop_ _Entity_db_link.Ordinal _Entity_db_link.Author_supplied _Entity_db_link.Database_code _Entity_db_link.Accession_code _Entity_db_link.Entry_mol_code _Entity_db_link.Entry_mol_name _Entity_db_link.Entry_experimental_method _Entity_db_link.Entry_structure_resolution _Entity_db_link.Entry_relation_type _Entity_db_link.Entry_details _Entity_db_link.Chimera_segment_ID _Entity_db_link.Seq_query_to_submitted_percent _Entity_db_link.Seq_subject_length _Entity_db_link.Seq_identity _Entity_db_link.Seq_positive _Entity_db_link.Seq_homology_expectation_val _Entity_db_link.Seq_align_begin _Entity_db_link.Seq_align_end _Entity_db_link.Seq_difference_details _Entity_db_link.Seq_alignment_details _Entity_db_link.Entry_ID _Entity_db_link.Entity_ID 1 no BMRB 17447 . MUP11 . . . . . 100.00 176 99.38 100.00 6.22e-114 . . . . 5996 1 2 no BMRB 4340 . rMUP . . . . . 100.00 162 98.77 99.38 2.36e-113 . . . . 5996 1 3 no BMRB 5995 . MUP-I . . . . . 100.00 162 100.00 100.00 7.39e-115 . . . . 5996 1 4 no PDB 1DF3 . 'Solution Structure Of A Recombinant Mouse Major Urinary Protein' . . . . . 100.00 162 98.77 99.38 2.36e-113 . . . . 5996 1 5 no PDB 1I04 . 'Crystal Structure Of Mouse Major Urinary Protein-I From Mouse Liver' . . . . . 100.00 180 99.38 100.00 5.87e-114 . . . . 5996 1 6 no PDB 1I05 . 'Crystal Structure Of Mouse Major Urinary Protein (Mup-I) Complexed With Hydroxy-Methyl-Heptanone' . . . . . 100.00 180 99.38 100.00 5.87e-114 . . . . 5996 1 7 no PDB 1I06 . 'Crystal Structure Of Mouse Major Urinary Protein (Mup-I) Complexed With Sec-Butyl-Thiazoline' . . . . . 100.00 180 99.38 100.00 5.87e-114 . . . . 5996 1 8 no PDB 1JV4 . 'Crystal Structure Of Recombinant Major Mouse Urinary Protein (Rmup) At 1.75 A Resolution' . . . . . 100.00 162 98.77 99.38 2.36e-113 . . . . 5996 1 9 no PDB 1MUP . 'Pheromone Binding To Two Rodent Urinary Proteins Revealed By X-Ray Crystallography' . . . . . 100.00 166 99.38 100.00 5.44e-114 . . . . 5996 1 10 no PDB 1QY0 . 'Thermodynamics Of Binding Of 2-Methoxy-3-Isopropylpyrazine And 2- Methoxy-3-Isobutylpyrazine To The Major Urinary Protein' . . . . . 100.00 174 98.77 99.38 5.00e-113 . . . . 5996 1 11 no PDB 1QY1 . 'Thermodynamics Of Binding Of 2-Methoxy-3-Isopropylpyrazine And 2- Methoxy-3-Isobutylpyrazine To The Major Urinary Protein' . . . . . 100.00 174 98.77 99.38 5.00e-113 . . . . 5996 1 12 no PDB 1QY2 . 'Thermodynamics Of Binding Of 2-Methoxy-3-Isopropylpyrazine And 2- Methoxy-3-Isobutylpyrazine To The Major Urinary Protein' . . . . . 100.00 174 98.77 99.38 5.00e-113 . . . . 5996 1 13 no PDB 1YP6 . 'Van Der Waals Interactions Dominate Hydrophobic Association In A Protein Binding Site Occluded From Solvent Water' . . . . . 100.00 174 98.15 99.38 2.26e-112 . . . . 5996 1 14 no PDB 1YP7 . 'Van Der Waals Interactions Dominate Hydrophobic Association In A Protein Binding Site Occluded From Solvent Water' . . . . . 100.00 174 98.15 99.38 2.26e-112 . . . . 5996 1 15 no PDB 1ZND . 'Strong Solute-solute Dispersive Interactions In A Protein- Ligand Complex' . . . . . 100.00 174 98.77 99.38 5.00e-113 . . . . 5996 1 16 no PDB 1ZNE . 'Strong Solute-Solute Dispersive Interactions In A Protein- Ligand Complex' . . . . . 100.00 174 98.77 99.38 5.00e-113 . . . . 5996 1 17 no PDB 1ZNG . 'Strong Solute-Solute Dispersive Interactions In A Protein- Ligand Complex' . . . . . 100.00 174 98.77 99.38 5.00e-113 . . . . 5996 1 18 no PDB 1ZNH . 'Strong Solute-Solute Dispersive Interactions In A Protein- Ligand Complex' . . . . . 100.00 174 98.77 99.38 5.00e-113 . . . . 5996 1 19 no PDB 1ZNK . 'Strong Solute-Solute Dispersive Interactions In A Protein- Ligand Complex' . . . . . 100.00 174 98.77 99.38 5.00e-113 . . . . 5996 1 20 no PDB 1ZNL . 'Strong Solute-Solute Dispersive Interactions In A Protein- Ligand Complex' . . . . . 100.00 174 98.77 99.38 5.00e-113 . . . . 5996 1 21 no PDB 2DM5 . 'Thermodynamic Penalty Arising From Burial Of A Ligand Polar Group Within A Hydrophobic Pocket Of A Protein Receptor' . . . . . 100.00 174 98.77 99.38 5.00e-113 . . . . 5996 1 22 no PDB 2LB6 . 'Structure Of 18694da Mup, Typical To The Major Urinary Protein Family: Mup9, Mup11, Mup15, Mup18 & Mup19' . . . . . 100.00 176 99.38 100.00 6.22e-114 . . . . 5996 1 23 no PDB 2OZQ . 'Crystal Structure Of Apo-Mup' . . . . . 100.00 174 98.77 99.38 5.00e-113 . . . . 5996 1 24 no DBJ BAB28753 . 'unnamed protein product [Mus musculus]' . . . . . 100.00 180 99.38 100.00 5.87e-114 . . . . 5996 1 25 no DBJ BAB29093 . 'unnamed protein product [Mus musculus]' . . . . . 100.00 181 98.15 100.00 8.83e-113 . . . . 5996 1 26 no EMBL CAA26953 . 'major urinary protein [Mus musculus]' . . . . . 100.00 180 98.77 99.38 3.12e-113 . . . . 5996 1 27 no EMBL CAA27227 . 'MUP [Mus musculus]' . . . . . 92.59 151 99.33 100.00 4.32e-105 . . . . 5996 1 28 no EMBL CAA27729 . 'MUP [Mus musculus]' . . . . . 83.95 136 97.06 98.53 1.96e-91 . . . . 5996 1 29 no EMBL CAC34259 . 'Major Urinary Protein [Mus musculus]' . . . . . 100.00 180 98.77 99.38 3.97e-113 . . . . 5996 1 30 no EMBL CAQ11104 . 'novel member of the major urinary protein (Mup) gene family [Mus musculus]' . . . . . 100.00 180 97.53 98.15 4.55e-111 . . . . 5996 1 31 no GB AAA39764 . 'major urinary protein [Mus musculus]' . . . . . 100.00 178 98.77 98.77 1.01e-112 . . . . 5996 1 32 no GB AAA39765 . 'major urinary protein, partial [Mus musculus]' . . . . . 92.59 151 99.33 100.00 4.32e-105 . . . . 5996 1 33 no GB AAA39767 . 'major urinary protein I [Mus musculus domesticus]' . . . . . 100.00 180 100.00 100.00 1.10e-114 . . . . 5996 1 34 no GB AAA39768 . 'major urinary protein II [Mus musculus domesticus]' . . . . . 100.00 180 98.15 99.38 2.02e-112 . . . . 5996 1 35 no GB AAB47130 . 'uMUP-VIII=18.695 kda major urinary protein [mice, Balb/c, urine, Peptide, 162 aa]' . . . . . 100.00 162 99.38 100.00 3.16e-114 . . . . 5996 1 36 no REF NP_001039015 . 'major urinary protein 2 isoform 1 precursor [Mus musculus]' . . . . . 100.00 180 98.77 100.00 1.33e-113 . . . . 5996 1 37 no REF NP_001116119 . 'major urinary protein 10 precursor [Mus musculus]' . . . . . 100.00 180 98.77 99.38 3.56e-113 . . . . 5996 1 38 no REF NP_001128116 . 'major urinary protein LOC100048885 precursor [Mus musculus]' . . . . . 100.00 180 97.53 98.15 4.55e-111 . . . . 5996 1 39 no REF NP_001128147 . 'major urinary protein 7 precursor [Mus musculus]' . . . . . 95.06 235 99.35 99.35 3.25e-106 . . . . 5996 1 40 no REF NP_001128148 . 'major urinary protein 8 precursor [Mus musculus]' . . . . . 95.06 235 98.05 98.70 4.04e-104 . . . . 5996 1 41 no SP B5X0G2 . 'RecName: Full=Major urinary protein 17; Short=MUP 17; Flags: Precursor [Mus musculus]' . . . . . 100.00 180 97.53 99.38 1.16e-111 . . . . 5996 1 42 no SP P02762 . 'RecName: Full=Major urinary protein 6; Short=MUP 6; AltName: Full=Alpha-2U-globulin; AltName: Full=Group 1, BS6; AltName: Aller' . . . . . 100.00 180 99.38 100.00 5.87e-114 . . . . 5996 1 43 no SP P04938 . 'RecName: Full=Major urinary proteins 11 and 8; AltName: Full=MUP11 and MUP8, partial [Mus musculus]' . . . . . 92.59 151 99.33 100.00 4.32e-105 . . . . 5996 1 44 no SP P11588 . 'RecName: Full=Major urinary protein 1; Short=MUP 1; Flags: Precursor [Mus musculus]' . . . . . 100.00 180 100.00 100.00 1.10e-114 . . . . 5996 1 45 no SP P11589 . 'RecName: Full=Major urinary protein 2; Short=MUP 2; Flags: Precursor [Mus musculus]' . . . . . 100.00 180 98.15 99.38 2.02e-112 . . . . 5996 1 46 no TPG DAA06299 . 'TPA_inf: major urinary protein 3 [Mus musculus]' . . . . . 100.00 180 99.38 99.38 8.98e-114 . . . . 5996 1 47 no TPG DAA06300 . 'TPA_inf: major urinary protein 4 [Mus musculus]' . . . . . 100.00 180 98.77 100.00 1.33e-113 . . . . 5996 1 48 no TPG DAA06301 . 'TPA_inf: major urinary protein 5 [Mus musculus]' . . . . . 100.00 180 98.15 98.77 6.23e-112 . . . . 5996 1 49 no TPG DAA06302 . 'TPA_inf: major urinary protein 6 [Mus musculus]' . . . . . 100.00 180 99.38 100.00 5.87e-114 . . . . 5996 1 50 no TPG DAA06303 . 'TPA_inf: major urinary protein 7 [Mus musculus]' . . . . . 100.00 180 100.00 100.00 9.88e-115 . . . . 5996 1 stop_ loop_ _Entity_common_name.Name _Entity_common_name.Type _Entity_common_name.Entry_ID _Entity_common_name.Entity_ID MUP-I abbreviation 5996 1 'Major Urinary Protein-I' common 5996 1 stop_ loop_ _Entity_comp_index.ID _Entity_comp_index.Auth_seq_ID _Entity_comp_index.Comp_ID _Entity_comp_index.Comp_label _Entity_comp_index.Entry_ID _Entity_comp_index.Entity_ID 1 . GLU . 5996 1 2 . GLU . 5996 1 3 . ALA . 5996 1 4 . SER . 5996 1 5 . SER . 5996 1 6 . THR . 5996 1 7 . GLY . 5996 1 8 . ARG . 5996 1 9 . ASN . 5996 1 10 . PHE . 5996 1 11 . ASN . 5996 1 12 . VAL . 5996 1 13 . GLU . 5996 1 14 . LYS . 5996 1 15 . ILE . 5996 1 16 . ASN . 5996 1 17 . GLY . 5996 1 18 . GLU . 5996 1 19 . TRP . 5996 1 20 . HIS . 5996 1 21 . THR . 5996 1 22 . ILE . 5996 1 23 . ILE . 5996 1 24 . LEU . 5996 1 25 . ALA . 5996 1 26 . SER . 5996 1 27 . ASP . 5996 1 28 . LYS . 5996 1 29 . ARG . 5996 1 30 . GLU . 5996 1 31 . LYS . 5996 1 32 . ILE . 5996 1 33 . GLU . 5996 1 34 . ASP . 5996 1 35 . ASN . 5996 1 36 . GLY . 5996 1 37 . ASN . 5996 1 38 . PHE . 5996 1 39 . ARG . 5996 1 40 . LEU . 5996 1 41 . PHE . 5996 1 42 . LEU . 5996 1 43 . GLU . 5996 1 44 . GLN . 5996 1 45 . ILE . 5996 1 46 . HIS . 5996 1 47 . VAL . 5996 1 48 . LEU . 5996 1 49 . GLU . 5996 1 50 . ASN . 5996 1 51 . SER . 5996 1 52 . LEU . 5996 1 53 . VAL . 5996 1 54 . LEU . 5996 1 55 . LYS . 5996 1 56 . PHE . 5996 1 57 . HIS . 5996 1 58 . THR . 5996 1 59 . VAL . 5996 1 60 . ARG . 5996 1 61 . ASP . 5996 1 62 . GLU . 5996 1 63 . GLU . 5996 1 64 . CYS . 5996 1 65 . SER . 5996 1 66 . GLU . 5996 1 67 . LEU . 5996 1 68 . SER . 5996 1 69 . MET . 5996 1 70 . VAL . 5996 1 71 . ALA . 5996 1 72 . ASP . 5996 1 73 . LYS . 5996 1 74 . THR . 5996 1 75 . GLU . 5996 1 76 . LYS . 5996 1 77 . ALA . 5996 1 78 . GLY . 5996 1 79 . GLU . 5996 1 80 . TYR . 5996 1 81 . SER . 5996 1 82 . VAL . 5996 1 83 . THR . 5996 1 84 . TYR . 5996 1 85 . ASP . 5996 1 86 . GLY . 5996 1 87 . PHE . 5996 1 88 . ASN . 5996 1 89 . THR . 5996 1 90 . PHE . 5996 1 91 . THR . 5996 1 92 . ILE . 5996 1 93 . PRO . 5996 1 94 . LYS . 5996 1 95 . THR . 5996 1 96 . ASP . 5996 1 97 . TYR . 5996 1 98 . ASP . 5996 1 99 . ASN . 5996 1 100 . PHE . 5996 1 101 . LEU . 5996 1 102 . MET . 5996 1 103 . ALA . 5996 1 104 . HIS . 5996 1 105 . LEU . 5996 1 106 . ILE . 5996 1 107 . ASN . 5996 1 108 . GLU . 5996 1 109 . LYS . 5996 1 110 . ASP . 5996 1 111 . GLY . 5996 1 112 . GLU . 5996 1 113 . THR . 5996 1 114 . PHE . 5996 1 115 . GLN . 5996 1 116 . LEU . 5996 1 117 . MET . 5996 1 118 . GLY . 5996 1 119 . LEU . 5996 1 120 . TYR . 5996 1 121 . GLY . 5996 1 122 . ARG . 5996 1 123 . GLU . 5996 1 124 . PRO . 5996 1 125 . ASP . 5996 1 126 . LEU . 5996 1 127 . SER . 5996 1 128 . SER . 5996 1 129 . ASP . 5996 1 130 . ILE . 5996 1 131 . LYS . 5996 1 132 . GLU . 5996 1 133 . ARG . 5996 1 134 . PHE . 5996 1 135 . ALA . 5996 1 136 . GLN . 5996 1 137 . LEU . 5996 1 138 . CYS . 5996 1 139 . GLU . 5996 1 140 . LYS . 5996 1 141 . HIS . 5996 1 142 . GLY . 5996 1 143 . ILE . 5996 1 144 . LEU . 5996 1 145 . ARG . 5996 1 146 . GLU . 5996 1 147 . ASN . 5996 1 148 . ILE . 5996 1 149 . ILE . 5996 1 150 . ASP . 5996 1 151 . LEU . 5996 1 152 . SER . 5996 1 153 . ASN . 5996 1 154 . ALA . 5996 1 155 . ASN . 5996 1 156 . ARG . 5996 1 157 . CYS . 5996 1 158 . LEU . 5996 1 159 . GLN . 5996 1 160 . ALA . 5996 1 161 . ARG . 5996 1 162 . GLU . 5996 1 stop_ loop_ _Entity_poly_seq.Hetero _Entity_poly_seq.Mon_ID _Entity_poly_seq.Num _Entity_poly_seq.Comp_index_ID _Entity_poly_seq.Entry_ID _Entity_poly_seq.Entity_ID . GLU 1 1 5996 1 . GLU 2 2 5996 1 . ALA 3 3 5996 1 . SER 4 4 5996 1 . SER 5 5 5996 1 . THR 6 6 5996 1 . GLY 7 7 5996 1 . ARG 8 8 5996 1 . ASN 9 9 5996 1 . PHE 10 10 5996 1 . ASN 11 11 5996 1 . VAL 12 12 5996 1 . GLU 13 13 5996 1 . LYS 14 14 5996 1 . ILE 15 15 5996 1 . ASN 16 16 5996 1 . GLY 17 17 5996 1 . GLU 18 18 5996 1 . TRP 19 19 5996 1 . HIS 20 20 5996 1 . THR 21 21 5996 1 . ILE 22 22 5996 1 . ILE 23 23 5996 1 . LEU 24 24 5996 1 . ALA 25 25 5996 1 . SER 26 26 5996 1 . ASP 27 27 5996 1 . LYS 28 28 5996 1 . ARG 29 29 5996 1 . GLU 30 30 5996 1 . LYS 31 31 5996 1 . ILE 32 32 5996 1 . GLU 33 33 5996 1 . ASP 34 34 5996 1 . ASN 35 35 5996 1 . GLY 36 36 5996 1 . ASN 37 37 5996 1 . PHE 38 38 5996 1 . ARG 39 39 5996 1 . LEU 40 40 5996 1 . PHE 41 41 5996 1 . LEU 42 42 5996 1 . GLU 43 43 5996 1 . GLN 44 44 5996 1 . ILE 45 45 5996 1 . HIS 46 46 5996 1 . VAL 47 47 5996 1 . LEU 48 48 5996 1 . GLU 49 49 5996 1 . ASN 50 50 5996 1 . SER 51 51 5996 1 . LEU 52 52 5996 1 . VAL 53 53 5996 1 . LEU 54 54 5996 1 . LYS 55 55 5996 1 . PHE 56 56 5996 1 . HIS 57 57 5996 1 . THR 58 58 5996 1 . VAL 59 59 5996 1 . ARG 60 60 5996 1 . ASP 61 61 5996 1 . GLU 62 62 5996 1 . GLU 63 63 5996 1 . CYS 64 64 5996 1 . SER 65 65 5996 1 . GLU 66 66 5996 1 . LEU 67 67 5996 1 . SER 68 68 5996 1 . MET 69 69 5996 1 . VAL 70 70 5996 1 . ALA 71 71 5996 1 . ASP 72 72 5996 1 . LYS 73 73 5996 1 . THR 74 74 5996 1 . GLU 75 75 5996 1 . LYS 76 76 5996 1 . ALA 77 77 5996 1 . GLY 78 78 5996 1 . GLU 79 79 5996 1 . TYR 80 80 5996 1 . SER 81 81 5996 1 . VAL 82 82 5996 1 . THR 83 83 5996 1 . TYR 84 84 5996 1 . ASP 85 85 5996 1 . GLY 86 86 5996 1 . PHE 87 87 5996 1 . ASN 88 88 5996 1 . THR 89 89 5996 1 . PHE 90 90 5996 1 . THR 91 91 5996 1 . ILE 92 92 5996 1 . PRO 93 93 5996 1 . LYS 94 94 5996 1 . THR 95 95 5996 1 . ASP 96 96 5996 1 . TYR 97 97 5996 1 . ASP 98 98 5996 1 . ASN 99 99 5996 1 . PHE 100 100 5996 1 . LEU 101 101 5996 1 . MET 102 102 5996 1 . ALA 103 103 5996 1 . HIS 104 104 5996 1 . LEU 105 105 5996 1 . ILE 106 106 5996 1 . ASN 107 107 5996 1 . GLU 108 108 5996 1 . LYS 109 109 5996 1 . ASP 110 110 5996 1 . GLY 111 111 5996 1 . GLU 112 112 5996 1 . THR 113 113 5996 1 . PHE 114 114 5996 1 . GLN 115 115 5996 1 . LEU 116 116 5996 1 . MET 117 117 5996 1 . GLY 118 118 5996 1 . LEU 119 119 5996 1 . TYR 120 120 5996 1 . GLY 121 121 5996 1 . ARG 122 122 5996 1 . GLU 123 123 5996 1 . PRO 124 124 5996 1 . ASP 125 125 5996 1 . LEU 126 126 5996 1 . SER 127 127 5996 1 . SER 128 128 5996 1 . ASP 129 129 5996 1 . ILE 130 130 5996 1 . LYS 131 131 5996 1 . GLU 132 132 5996 1 . ARG 133 133 5996 1 . PHE 134 134 5996 1 . ALA 135 135 5996 1 . GLN 136 136 5996 1 . LEU 137 137 5996 1 . CYS 138 138 5996 1 . GLU 139 139 5996 1 . LYS 140 140 5996 1 . HIS 141 141 5996 1 . GLY 142 142 5996 1 . ILE 143 143 5996 1 . LEU 144 144 5996 1 . ARG 145 145 5996 1 . GLU 146 146 5996 1 . ASN 147 147 5996 1 . ILE 148 148 5996 1 . ILE 149 149 5996 1 . ASP 150 150 5996 1 . LEU 151 151 5996 1 . SER 152 152 5996 1 . ASN 153 153 5996 1 . ALA 154 154 5996 1 . ASN 155 155 5996 1 . ARG 156 156 5996 1 . CYS 157 157 5996 1 . LEU 158 158 5996 1 . GLN 159 159 5996 1 . ALA 160 160 5996 1 . ARG 161 161 5996 1 . GLU 162 162 5996 1 stop_ save_ save_entity_ZBT _Entity.Sf_category entity _Entity.Sf_framecode entity_ZBT _Entity.Entry_ID 5996 _Entity.ID 2 _Entity.BMRB_code ZBT _Entity.Name 2-[(1S)-1-methylpropyl]-4,5-dihydro-1,3-thiazole _Entity.Type non-polymer _Entity.Polymer_common_type . _Entity.Polymer_type . _Entity.Polymer_type_details . _Entity.Polymer_strand_ID . _Entity.Polymer_seq_one_letter_code_can . _Entity.Polymer_seq_one_letter_code . _Entity.Target_identifier . _Entity.Polymer_author_defined_seq . _Entity.Polymer_author_seq_details . _Entity.Ambiguous_conformational_states . _Entity.Ambiguous_chem_comp_sites . _Entity.Nstd_monomer . _Entity.Nstd_chirality . _Entity.Nstd_linkage . _Entity.Nonpolymer_comp_ID ZBT _Entity.Nonpolymer_comp_label $chem_comp_ZBT _Entity.Number_of_monomers . _Entity.Number_of_nonpolymer_components 1 _Entity.Paramagnetic . _Entity.Thiol_state . _Entity.Src_method . _Entity.Parent_entity_ID . _Entity.Fragment . _Entity.Mutation . _Entity.EC_number . _Entity.Calc_isoelectric_point . _Entity.Formula_weight 143.250 _Entity.Formula_weight_exptl . _Entity.Formula_weight_exptl_meth . _Entity.Details . _Entity.DB_query_date . _Entity.DB_query_revised_last_date . loop_ _Entity_common_name.Name _Entity_common_name.Type _Entity_common_name.Entry_ID _Entity_common_name.Entity_ID 2-[(1S)-1-methylpropyl]-4,5-dihydro-1,3-thiazole BMRB 5996 2 stop_ loop_ _Entity_systematic_name.Name _Entity_systematic_name.Naming_system _Entity_systematic_name.Entry_ID _Entity_systematic_name.Entity_ID 2-[(1S)-1-methylpropyl]-4,5-dihydro-1,3-thiazole BMRB 5996 2 ZBT 'Three letter code' 5996 2 stop_ loop_ _Entity_comp_index.ID _Entity_comp_index.Auth_seq_ID _Entity_comp_index.Comp_ID _Entity_comp_index.Comp_label _Entity_comp_index.Entry_ID _Entity_comp_index.Entity_ID 1 1 ZBT $chem_comp_ZBT 5996 2 stop_ save_ #################### # Natural source # #################### save_natural_source _Entity_natural_src_list.Sf_category natural_source _Entity_natural_src_list.Sf_framecode natural_source _Entity_natural_src_list.Entry_ID 5996 _Entity_natural_src_list.ID 1 loop_ _Entity_natural_src.ID _Entity_natural_src.Entity_ID _Entity_natural_src.Entity_label _Entity_natural_src.Entity_chimera_segment_ID _Entity_natural_src.NCBI_taxonomy_ID _Entity_natural_src.Type _Entity_natural_src.Common _Entity_natural_src.Organism_name_scientific _Entity_natural_src.Organism_name_common _Entity_natural_src.Organism_acronym _Entity_natural_src.ICTVdb_decimal_code _Entity_natural_src.Superkingdom _Entity_natural_src.Kingdom _Entity_natural_src.Genus _Entity_natural_src.Species _Entity_natural_src.Strain _Entity_natural_src.Variant _Entity_natural_src.Organ _Entity_natural_src.Tissue _Entity_natural_src.Tissue_fraction _Entity_natural_src.Cell_line _Entity_natural_src.Cell_type _Entity_natural_src.ATCC_number _Entity_natural_src.Organelle _Entity_natural_src.Secretion _Entity_natural_src.Plasmid _Entity_natural_src.Gene_mnemonic _Entity_natural_src.Details _Entity_natural_src.Entry_ID _Entity_natural_src.Entity_natural_src_list_ID 1 1 $MUP-I . 10090 organism . 'Mus musculus' 'House mouse' . . Eukaryota Metazoa Mus musculus . . . . . . . . . . . . domesticus 5996 1 stop_ save_ ######################### # Experimental source # ######################### save_experimental_source _Entity_experimental_src_list.Sf_category experimental_source _Entity_experimental_src_list.Sf_framecode experimental_source _Entity_experimental_src_list.Entry_ID 5996 _Entity_experimental_src_list.ID 1 loop_ _Entity_experimental_src.ID _Entity_experimental_src.Entity_ID _Entity_experimental_src.Entity_label _Entity_experimental_src.Entity_chimera_segment_ID _Entity_experimental_src.Production_method _Entity_experimental_src.Host_org_scientific_name _Entity_experimental_src.Host_org_name_common _Entity_experimental_src.Host_org_details _Entity_experimental_src.Host_org_NCBI_taxonomy_ID _Entity_experimental_src.Host_org_genus _Entity_experimental_src.Host_org_species _Entity_experimental_src.Host_org_strain _Entity_experimental_src.Host_org_variant _Entity_experimental_src.Host_org_ATCC_number _Entity_experimental_src.Vector_type _Entity_experimental_src.PDBview_host_org_vector_name _Entity_experimental_src.PDBview_plasmid_name _Entity_experimental_src.Vector_name _Entity_experimental_src.Vector_details _Entity_experimental_src.Vendor_name _Entity_experimental_src.Details _Entity_experimental_src.Entry_ID _Entity_experimental_src.Entity_experimental_src_list_ID 1 1 $MUP-I . 'recombinant technology' . . . . . . . . . . . . . . . . 5996 1 stop_ save_ ################################# # Polymer residues and ligands # ################################# save_chem_comp_ZBT _Chem_comp.Sf_category chem_comp _Chem_comp.Sf_framecode chem_comp_ZBT _Chem_comp.Entry_ID 5996 _Chem_comp.ID ZBT _Chem_comp.Provenance PDB _Chem_comp.Name 2-[(1S)-1-methylpropyl]-4,5-dihydro-1,3-thiazole _Chem_comp.Type NON-POLYMER _Chem_comp.BMRB_code ZBT _Chem_comp.PDB_code ZBT _Chem_comp.Ambiguous_flag no _Chem_comp.Initial_date 2012-11-20 _Chem_comp.Modified_date 2012-11-20 _Chem_comp.Release_status REL _Chem_comp.Replaced_by . _Chem_comp.Replaces . _Chem_comp.One_letter_code . _Chem_comp.Three_letter_code ZBT _Chem_comp.Number_atoms_all 22 _Chem_comp.Number_atoms_nh 9 _Chem_comp.PubChem_code . _Chem_comp.Subcomponent_list . _Chem_comp.InChI_code InChI=1S/C7H13NS/c1-3-6(2)7-8-4-5-9-7/h6H,3-5H2,1-2H3/t6-/m0/s1 _Chem_comp.Mon_nstd_flag . _Chem_comp.Mon_nstd_class . _Chem_comp.Mon_nstd_details . _Chem_comp.Mon_nstd_parent . _Chem_comp.Mon_nstd_parent_comp_ID . _Chem_comp.Std_deriv_one_letter_code . _Chem_comp.Std_deriv_three_letter_code . _Chem_comp.Std_deriv_BMRB_code . _Chem_comp.Std_deriv_PDB_code . _Chem_comp.Std_deriv_chem_comp_name . _Chem_comp.Synonyms 2-sec-butyl-4,5-dihydrothiazole _Chem_comp.Formal_charge 0 _Chem_comp.Paramagnetic . _Chem_comp.Aromatic no _Chem_comp.Formula 'C7 H13 N S' _Chem_comp.Formula_weight 143.250 _Chem_comp.Formula_mono_iso_wt_nat . _Chem_comp.Formula_mono_iso_wt_13C . _Chem_comp.Formula_mono_iso_wt_15N . _Chem_comp.Formula_mono_iso_wt_13C_15N . _Chem_comp.Image_file_name . _Chem_comp.Image_file_format . _Chem_comp.Topo_file_name . _Chem_comp.Topo_file_format . _Chem_comp.Struct_file_name . _Chem_comp.Struct_file_format . _Chem_comp.Stereochem_param_file_name . _Chem_comp.Stereochem_param_file_format . _Chem_comp.Model_details . _Chem_comp.Model_erf . _Chem_comp.Model_source . _Chem_comp.Model_coordinates_details . _Chem_comp.Model_coordinates_missing_flag no _Chem_comp.Ideal_coordinates_details Corina _Chem_comp.Ideal_coordinates_missing_flag no _Chem_comp.Model_coordinates_db_code 3KFF _Chem_comp.Processing_site RCSB _Chem_comp.Vendor . _Chem_comp.Vendor_product_code . _Chem_comp.Details . _Chem_comp.DB_query_date . _Chem_comp.DB_last_query_revised_last_date . loop_ _Chem_comp_descriptor.Descriptor _Chem_comp_descriptor.Type _Chem_comp_descriptor.Program _Chem_comp_descriptor.Program_version _Chem_comp_descriptor.Entry_ID _Chem_comp_descriptor.Comp_ID CCC(C)C1=NCCS1 SMILES 'OpenEye OEToolkits' 1.7.0 5996 ZBT CC[C@H](C)C1=NCCS1 SMILES_CANONICAL CACTVS 3.352 5996 ZBT CC[C@H](C)C1=NCCS1 SMILES_CANONICAL 'OpenEye OEToolkits' 1.7.0 5996 ZBT CC[CH](C)C1=NCCS1 SMILES CACTVS 3.352 5996 ZBT InChI=1S/C7H13NS/c1-3-6(2)7-8-4-5-9-7/h6H,3-5H2,1-2H3/t6-/m0/s1 InChI InChI 1.03 5996 ZBT SAWWKXMIPYUIBW-LURJTMIESA-N InChIKey InChI 1.03 5996 ZBT stop_ loop_ _Chem_comp_identifier.Identifier _Chem_comp_identifier.Type _Chem_comp_identifier.Program _Chem_comp_identifier.Program_version _Chem_comp_identifier.Entry_ID _Chem_comp_identifier.Comp_ID 2-[(2S)-butan-2-yl]-4,5-dihydro-1,3-thiazole 'SYSTEMATIC NAME' 'OpenEye OEToolkits' 1.6.1 5996 ZBT stop_ loop_ _Chem_comp_atom.Atom_ID _Chem_comp_atom.BMRB_code _Chem_comp_atom.PDB_atom_ID _Chem_comp_atom.Alt_atom_ID _Chem_comp_atom.Auth_atom_ID _Chem_comp_atom.Type_symbol _Chem_comp_atom.Isotope_number _Chem_comp_atom.Chirality _Chem_comp_atom.Stereo_config _Chem_comp_atom.Charge _Chem_comp_atom.Partial_charge _Chem_comp_atom.Oxidation_number _Chem_comp_atom.Unpaired_electron_number _Chem_comp_atom.Align _Chem_comp_atom.Aromatic_flag _Chem_comp_atom.Leaving_atom_flag _Chem_comp_atom.Substruct_code _Chem_comp_atom.Ionizable _Chem_comp_atom.Drawing_2D_coord_x _Chem_comp_atom.Drawing_2D_coord_y _Chem_comp_atom.Model_Cartn_x _Chem_comp_atom.Model_Cartn_x_esd _Chem_comp_atom.Model_Cartn_y _Chem_comp_atom.Model_Cartn_y_esd _Chem_comp_atom.Model_Cartn_z _Chem_comp_atom.Model_Cartn_z_esd _Chem_comp_atom.Model_Cartn_x_ideal _Chem_comp_atom.Model_Cartn_y_ideal _Chem_comp_atom.Model_Cartn_z_ideal _Chem_comp_atom.PDBX_ordinal _Chem_comp_atom.Details _Chem_comp_atom.Entry_ID _Chem_comp_atom.Comp_ID S1 S1 S1 S1 . S . . N 0 . . . 1 no no . . . . 13.047 . -30.365 . 8.027 . 1.536 -1.051 -0.413 1 . 5996 ZBT C2 C2 C2 C2 . C . . N 0 . . . 1 no no . . . . 11.502 . -31.006 . 8.222 . 0.158 -0.013 -0.026 2 . 5996 ZBT N3 N3 N3 N3 . N . . N 0 . . . 1 no no . . . . 11.069 . -30.825 . 9.386 . 0.566 1.141 0.329 3 . 5996 ZBT C4 C4 C4 C4 . C . . N 0 . . . 1 no no . . . . 11.884 . -30.109 . 10.366 . 1.982 1.429 0.367 4 . 5996 ZBT C5 C5 C5 C5 . C . . N 0 . . . 1 no no . . . . 13.215 . -29.863 . 9.703 . 2.809 0.204 -0.059 5 . 5996 ZBT C6 C6 C6 C6 . C . . S 0 . . . 1 no no . . . . 10.726 . -31.672 . 7.145 . -1.288 -0.432 -0.105 6 . 5996 ZBT C7 C7 C7 C7 . C . . N 0 . . . 1 no no . . . . 10.810 . -30.852 . 5.856 . -2.166 0.804 -0.314 7 . 5996 ZBT C8 C8 C8 C8 . C . . N 0 . . . 1 no no . . . . 10.379 . -31.792 . 4.738 . -3.618 0.369 -0.519 8 . 5996 ZBT C9 C9 C9 C9 . C . . N 0 . . . 1 no no . . . . 9.261 . -31.884 . 7.493 . -1.689 -1.128 1.197 9 . 5996 ZBT H4 H4 H4 H4 . H . . N 0 . . . 1 no no . . . . 11.408 . -29.157 . 10.644 . 2.197 2.257 -0.308 10 . 5996 ZBT H5 H5 H5 H5 . H . . N 0 . . . 1 no no . . . . 14.004 . -30.446 . 10.200 . 3.457 -0.124 0.753 11 . 5996 ZBT H6 H6 H6 H6 . H . . N 0 . . . 1 no no . . . . 11.180 . -32.665 . 7.014 . -1.422 -1.118 -0.941 12 . 5996 ZBT H7 H7 H7 H7 . H . . N 0 . . . 1 no no . . . . 10.145 . -29.977 . 5.907 . -2.100 1.449 0.562 13 . 5996 ZBT H7A H7A H7A H7A . H . . N 0 . . . 1 no no . . . . 11.836 . -30.494 . 5.689 . -1.822 1.349 -1.193 14 . 5996 ZBT H8 H8 H8 H8 . H . . N 0 . . . 1 no no . . . . 10.417 . -31.260 . 3.776 . -4.244 1.249 -0.668 15 . 5996 ZBT H8A H8A H8A H8A . H . . N 0 . . . 1 no no . . . . 11.057 . -32.658 . 4.705 . -3.684 -0.276 -1.395 16 . 5996 ZBT H8B H8B H8B H8B . H . . N 0 . . . 1 no no . . . . 9.352 . -32.137 . 4.925 . -3.961 -0.176 0.361 17 . 5996 ZBT H9 H9 H9 H9 . H . . N 0 . . . 1 no no . . . . 8.752 . -32.379 . 6.653 . -2.735 -1.431 1.140 18 . 5996 ZBT H9A H9A H9A H9A . H . . N 0 . . . 1 no no . . . . 9.185 . -32.515 . 8.391 . -1.064 -2.008 1.346 19 . 5996 ZBT H9B H9B H9B H9B . H . . N 0 . . . 1 no no . . . . 8.786 . -30.911 . 7.687 . -1.555 -0.441 2.033 20 . 5996 ZBT H12 H12 H12 H12 . H . . N 0 . . . 1 no no . . . . 12.011 . -30.711 . 11.278 . 2.263 1.714 1.381 21 . 5996 ZBT H13 H13 H13 H13 . H . . N 0 . . . 1 no no . . . . 13.480 . -28.797 . 9.759 . 3.391 0.425 -0.954 22 . 5996 ZBT stop_ loop_ _Chem_comp_bond.ID _Chem_comp_bond.Type _Chem_comp_bond.Value_order _Chem_comp_bond.Atom_ID_1 _Chem_comp_bond.Atom_ID_2 _Chem_comp_bond.Aromatic_flag _Chem_comp_bond.Stereo_config _Chem_comp_bond.Ordinal _Chem_comp_bond.Details _Chem_comp_bond.Entry_ID _Chem_comp_bond.Comp_ID 1 . SING S1 C2 no N 1 . 5996 ZBT 2 . SING S1 C5 no N 2 . 5996 ZBT 3 . DOUB C2 N3 no N 3 . 5996 ZBT 4 . SING C2 C6 no N 4 . 5996 ZBT 5 . SING N3 C4 no N 5 . 5996 ZBT 6 . SING C4 C5 no N 6 . 5996 ZBT 7 . SING C4 H4 no N 7 . 5996 ZBT 8 . SING C5 H5 no N 8 . 5996 ZBT 9 . SING C6 C7 no N 9 . 5996 ZBT 10 . SING C6 C9 no N 10 . 5996 ZBT 11 . SING C6 H6 no N 11 . 5996 ZBT 12 . SING C7 C8 no N 12 . 5996 ZBT 13 . SING C7 H7 no N 13 . 5996 ZBT 14 . SING C7 H7A no N 14 . 5996 ZBT 15 . SING C8 H8 no N 15 . 5996 ZBT 16 . SING C8 H8A no N 16 . 5996 ZBT 17 . SING C8 H8B no N 17 . 5996 ZBT 18 . SING C9 H9 no N 18 . 5996 ZBT 19 . SING C9 H9A no N 19 . 5996 ZBT 20 . SING C9 H9B no N 20 . 5996 ZBT 21 . SING C4 H12 no N 21 . 5996 ZBT 22 . SING C5 H13 no N 22 . 5996 ZBT stop_ save_ ##################################### # Sample contents and methodology # ##################################### ######################## # Sample description # ######################## save_sample_1 _Sample.Sf_category sample _Sample.Sf_framecode sample_1 _Sample.Entry_ID 5996 _Sample.ID 1 _Sample.Type solution _Sample.Sub_type . _Sample.Details . _Sample.Aggregate_sample_number . _Sample.Solvent_system . _Sample.Preparation_date . _Sample.Preparation_expiration_date . _Sample.Polycrystallization_protocol . _Sample.Single_crystal_protocol . _Sample.Crystal_grow_apparatus . _Sample.Crystal_grow_atmosphere . _Sample.Crystal_grow_details . _Sample.Crystal_grow_method . _Sample.Crystal_grow_method_cit_ID . _Sample.Crystal_grow_pH . _Sample.Crystal_grow_pH_range . _Sample.Crystal_grow_pressure . _Sample.Crystal_grow_pressure_esd . _Sample.Crystal_grow_seeding . _Sample.Crystal_grow_seeding_cit_ID . _Sample.Crystal_grow_temp . _Sample.Crystal_grow_temp_details . _Sample.Crystal_grow_temp_esd . _Sample.Crystal_grow_time . _Sample.Oriented_sample_prep_protocol . _Sample.Lyophilization_cryo_protectant . _Sample.Storage_protocol . loop_ _Sample_component.ID _Sample_component.Mol_common_name _Sample_component.Isotopic_labeling _Sample_component.Assembly_ID _Sample_component.Assembly_label _Sample_component.Entity_ID _Sample_component.Entity_label _Sample_component.Product_ID _Sample_component.Type _Sample_component.Concentration_val _Sample_component.Concentration_val_min _Sample_component.Concentration_val_max _Sample_component.Concentration_val_units _Sample_component.Concentration_val_err _Sample_component.Vendor _Sample_component.Vendor_product_name _Sample_component.Vendor_product_code _Sample_component.Entry_ID _Sample_component.Sample_ID 1 'Major Urinary Protein-I' '[U-95% 15N]' . . 1 $MUP-I . . 1.8 . . mM . . . . 5996 1 2 2-(SEC-BUTYL)-4,5-DIHYDROTHIAZOLE . . . 2 $entity_ZBT . . 1.8 . . mM . . . . 5996 1 stop_ save_ ####################### # Sample conditions # ####################### save_283K _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode 283K _Sample_condition_list.Entry_ID 5996 _Sample_condition_list.ID 1 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID pH 6.3 0.2 n/a 5996 1 temperature 283 1 K 5996 1 stop_ save_ save_288K _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode 288K _Sample_condition_list.Entry_ID 5996 _Sample_condition_list.ID 2 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID pH 6.3 0.2 n/a 5996 2 temperature 288 1 K 5996 2 stop_ save_ save_293K _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode 293K _Sample_condition_list.Entry_ID 5996 _Sample_condition_list.ID 3 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID pH 6.3 0.2 n/a 5996 3 temperature 293 1 K 5996 3 stop_ save_ save_298K _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode 298K _Sample_condition_list.Entry_ID 5996 _Sample_condition_list.ID 4 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID pH 6.3 0.2 n/a 5996 4 temperature 298 1 K 5996 4 stop_ save_ save_303K _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode 303K _Sample_condition_list.Entry_ID 5996 _Sample_condition_list.ID 5 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID pH 6.3 0.2 n/a 5996 5 temperature 303 1 K 5996 5 stop_ save_ save_308K _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode 308K _Sample_condition_list.Entry_ID 5996 _Sample_condition_list.ID 6 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID pH 6.3 0.2 n/a 5996 6 temperature 308 1 K 5996 6 stop_ save_ save_291K _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode 291K _Sample_condition_list.Entry_ID 5996 _Sample_condition_list.ID 7 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID pH 6.3 0.2 n/a 5996 7 temperature 291 1 K 5996 7 stop_ save_ save_297K _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode 297K _Sample_condition_list.Entry_ID 5996 _Sample_condition_list.ID 8 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID pH 6.3 0.2 n/a 5996 8 temperature 297 1 K 5996 8 stop_ save_ save_302K _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode 302K _Sample_condition_list.Entry_ID 5996 _Sample_condition_list.ID 9 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID pH 6.3 0.2 n/a 5996 9 temperature 302 1 K 5996 9 stop_ save_ ############################ # Computer software used # ############################ save_NMRPipe _Software.Sf_category software _Software.Sf_framecode NMRPipe _Software.Entry_ID 5996 _Software.ID 1 _Software.Name NMRPipe _Software.Version . _Software.Details . save_ ######################### # Experimental detail # ######################### ################################## # NMR Spectrometer definitions # ################################## save_NMR_spectrometer_1 _NMR_spectrometer.Sf_category NMR_spectrometer _NMR_spectrometer.Sf_framecode NMR_spectrometer_1 _NMR_spectrometer.Entry_ID 5996 _NMR_spectrometer.ID 1 _NMR_spectrometer.Details . _NMR_spectrometer.Manufacturer Bruker _NMR_spectrometer.Model Avance _NMR_spectrometer.Serial_number . _NMR_spectrometer.Field_strength 600 save_ save_NMR_spectrometer_2 _NMR_spectrometer.Sf_category NMR_spectrometer _NMR_spectrometer.Sf_framecode NMR_spectrometer_2 _NMR_spectrometer.Entry_ID 5996 _NMR_spectrometer.ID 2 _NMR_spectrometer.Details . _NMR_spectrometer.Manufacturer Bruker _NMR_spectrometer.Model DRX _NMR_spectrometer.Serial_number . _NMR_spectrometer.Field_strength 500 save_ save_spectrometer_list _NMR_spectrometer_list.Sf_category NMR_spectrometer_list _NMR_spectrometer_list.Sf_framecode spectrometer_list _NMR_spectrometer_list.Entry_ID 5996 _NMR_spectrometer_list.ID 1 loop_ _NMR_spectrometer_view.ID _NMR_spectrometer_view.Name _NMR_spectrometer_view.Manufacturer _NMR_spectrometer_view.Model _NMR_spectrometer_view.Serial_number _NMR_spectrometer_view.Field_strength _NMR_spectrometer_view.Details _NMR_spectrometer_view.Citation_ID _NMR_spectrometer_view.Citation_label _NMR_spectrometer_view.Entry_ID _NMR_spectrometer_view.NMR_spectrometer_list_ID 1 NMR_spectrometer_1 Bruker Avance . 600 . . . 5996 1 2 NMR_spectrometer_2 Bruker DRX . 500 . . . 5996 1 stop_ save_ ############################# # NMR applied experiments # ############################# save_experiment_list _Experiment_list.Sf_category experiment_list _Experiment_list.Sf_framecode experiment_list _Experiment_list.Entry_ID 5996 _Experiment_list.ID 1 _Experiment_list.Details . loop_ _Experiment.ID _Experiment.Name _Experiment.Raw_data_flag _Experiment.NMR_spec_expt_ID _Experiment.NMR_spec_expt_label _Experiment.MS_expt_ID _Experiment.MS_expt_label _Experiment.SAXS_expt_ID _Experiment.SAXS_expt_label _Experiment.FRET_expt_ID _Experiment.FRET_expt_label _Experiment.EMR_expt_ID _Experiment.EMR_expt_label _Experiment.Sample_ID _Experiment.Sample_label _Experiment.Sample_state _Experiment.Sample_volume _Experiment.Sample_volume_units _Experiment.Sample_condition_list_ID _Experiment.Sample_condition_list_label _Experiment.Sample_spinning_rate _Experiment.Sample_angle _Experiment.NMR_tube_type _Experiment.NMR_spectrometer_ID _Experiment.NMR_spectrometer_label _Experiment.NMR_spectrometer_probe_ID _Experiment.NMR_spectrometer_probe_label _Experiment.NMR_spectral_processing_ID _Experiment.NMR_spectral_processing_label _Experiment.Mass_spectrometer_ID _Experiment.Mass_spectrometer_label _Experiment.Xray_instrument_ID _Experiment.Xray_instrument_label _Experiment.Fluorescence_instrument_ID _Experiment.Fluorescence_instrument_label _Experiment.EMR_instrument_ID _Experiment.EMR_instrument_label _Experiment.Chromatographic_system_ID _Experiment.Chromatographic_system_label _Experiment.Chromatographic_column_ID _Experiment.Chromatographic_column_label _Experiment.Entry_ID _Experiment.Experiment_list_ID 1 '15N T1' . . . . . . . . . . . 1 $sample_1 . . . . . . . . . . . . . . . . . . . . . . . . . . 5996 1 2 '15N T2' . . . . . . . . . . . 1 $sample_1 . . . . . . . . . . . . . . . . . . . . . . . . . . 5996 1 3 '{1H}-15N NOE' . . . . . . . . . . . 1 $sample_1 . . . . . . . . . . . . . . . . . . . . . . . . . . 5996 1 stop_ save_ #################### # NMR parameters # #################### ############################## # Assigned chemical shifts # ############################## ################################ # Chemical shift referencing # ################################ save_chemical_shift_reference _Chem_shift_reference.Sf_category chem_shift_reference _Chem_shift_reference.Sf_framecode chemical_shift_reference _Chem_shift_reference.Entry_ID 5996 _Chem_shift_reference.ID 1 _Chem_shift_reference.Details . loop_ _Chem_shift_ref.Atom_type _Chem_shift_ref.Atom_isotope_number _Chem_shift_ref.Mol_common_name _Chem_shift_ref.Atom_group _Chem_shift_ref.Concentration_val _Chem_shift_ref.Concentration_units _Chem_shift_ref.Solvent _Chem_shift_ref.Rank _Chem_shift_ref.Chem_shift_units _Chem_shift_ref.Chem_shift_val _Chem_shift_ref.Ref_method _Chem_shift_ref.Ref_type _Chem_shift_ref.Indirect_shift_ratio _Chem_shift_ref.External_ref_loc _Chem_shift_ref.External_ref_sample_geometry _Chem_shift_ref.External_ref_axis _Chem_shift_ref.Ref_correction_type _Chem_shift_ref.Correction_val _Chem_shift_ref.Entry_ID _Chem_shift_ref.Chem_shift_reference_ID H 1 DSS 'methyl protons' . . . . ppm 0.0 internal direct 1.0 . . . . . 5996 1 N 15 DSS 'methyl protons' . . . . ppm 0.0 . indirect 0.101329118 . . . . . 5996 1 stop_ save_ ################################### # Assigned chemical shift lists # ################################### ################################################################### # Chemical Shift Ambiguity Index Value Definitions # # # # The values other than 1 are used for those atoms with different # # chemical shifts that cannot be assigned to stereospecific atoms # # or to specific residues or chains. # # # # Index Value Definition # # # # 1 Unique (including isolated methyl protons, # # geminal atoms, and geminal methyl # # groups with identical chemical shifts) # # (e.g. ILE HD11, HD12, HD13 protons) # # 2 Ambiguity of geminal atoms or geminal methyl # # proton groups (e.g. ASP HB2 and HB3 # # protons, LEU CD1 and CD2 carbons, or # # LEU HD11, HD12, HD13 and HD21, HD22, # # HD23 methyl protons) # # 3 Aromatic atoms on opposite sides of # # symmetrical rings (e.g. TYR HE1 and HE2 # # protons) # # 4 Intraresidue ambiguities (e.g. LYS HG and # # HD protons or TRP HZ2 and HZ3 protons) # # 5 Interresidue ambiguities (LYS 12 vs. LYS 27) # # 6 Intermolecular ambiguities (e.g. ASP 31 CA # # in monomer 1 and ASP 31 CA in monomer 2 # # of an asymmetrical homodimer, duplex # # DNA assignments, or other assignments # # that may apply to atoms in one or more # # molecule in the molecular assembly) # # 9 Ambiguous, specific ambiguity not defined # # # ################################################################### save_chemical_shift_1 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode chemical_shift_1 _Assigned_chem_shift_list.Entry_ID 5996 _Assigned_chem_shift_list.ID 1 _Assigned_chem_shift_list.Sample_condition_list_ID 1 _Assigned_chem_shift_list.Sample_condition_list_label $283K _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chemical_shift_reference _Assigned_chem_shift_list.Chem_shift_1H_err . _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err . _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID 1 '15N T1' 1 $sample_1 . 5996 1 2 '15N T2' 1 $sample_1 . 5996 1 3 '{1H}-15N NOE' 1 $sample_1 . 5996 1 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 1 2 2 GLU H H 1 8.538 0.01 . 1 . . . . . . . . 5996 1 2 . 1 1 2 2 GLU N N 15 119.871 0.10 . 1 . . . . . . . . 5996 1 3 . 1 1 3 3 ALA H H 1 8.879 0.01 . 1 . . . . . . . . 5996 1 4 . 1 1 3 3 ALA N N 15 125.550 0.10 . 1 . . . . . . . . 5996 1 5 . 1 1 4 4 SER H H 1 8.128 0.01 . 1 . . . . . . . . 5996 1 6 . 1 1 4 4 SER N N 15 111.891 0.10 . 1 . . . . . . . . 5996 1 7 . 1 1 5 5 SER H H 1 9.302 0.01 . 1 . . . . . . . . 5996 1 8 . 1 1 5 5 SER N N 15 120.847 0.10 . 1 . . . . . . . . 5996 1 9 . 1 1 6 6 THR H H 1 7.146 0.01 . 1 . . . . . . . . 5996 1 10 . 1 1 6 6 THR N N 15 108.519 0.10 . 1 . . . . . . . . 5996 1 11 . 1 1 7 7 GLY H H 1 7.660 0.01 . 1 . . . . . . . . 5996 1 12 . 1 1 7 7 GLY N N 15 110.645 0.10 . 1 . . . . . . . . 5996 1 13 . 1 1 8 8 ARG H H 1 8.632 0.01 . 1 . . . . . . . . 5996 1 14 . 1 1 8 8 ARG N N 15 120.526 0.10 . 1 . . . . . . . . 5996 1 15 . 1 1 9 9 ASN H H 1 8.673 0.01 . 1 . . . . . . . . 5996 1 16 . 1 1 9 9 ASN N N 15 115.302 0.10 . 1 . . . . . . . . 5996 1 17 . 1 1 10 10 PHE H H 1 7.832 0.01 . 1 . . . . . . . . 5996 1 18 . 1 1 10 10 PHE N N 15 121.842 0.10 . 1 . . . . . . . . 5996 1 19 . 1 1 11 11 ASN H H 1 7.710 0.01 . 1 . . . . . . . . 5996 1 20 . 1 1 11 11 ASN N N 15 127.727 0.10 . 1 . . . . . . . . 5996 1 21 . 1 1 12 12 VAL H H 1 8.172 0.01 . 1 . . . . . . . . 5996 1 22 . 1 1 12 12 VAL N N 15 123.609 0.10 . 1 . . . . . . . . 5996 1 23 . 1 1 13 13 GLU H H 1 8.097 0.01 . 1 . . . . . . . . 5996 1 24 . 1 1 13 13 GLU N N 15 118.489 0.10 . 1 . . . . . . . . 5996 1 25 . 1 1 14 14 LYS H H 1 7.351 0.01 . 1 . . . . . . . . 5996 1 26 . 1 1 14 14 LYS N N 15 115.140 0.10 . 1 . . . . . . . . 5996 1 27 . 1 1 15 15 ILE H H 1 7.681 0.01 . 1 . . . . . . . . 5996 1 28 . 1 1 15 15 ILE N N 15 110.300 0.10 . 1 . . . . . . . . 5996 1 29 . 1 1 16 16 ASN H H 1 7.137 0.01 . 1 . . . . . . . . 5996 1 30 . 1 1 16 16 ASN N N 15 119.523 0.10 . 1 . . . . . . . . 5996 1 31 . 1 1 17 17 GLY H H 1 9.401 0.01 . 1 . . . . . . . . 5996 1 32 . 1 1 17 17 GLY N N 15 111.924 0.10 . 1 . . . . . . . . 5996 1 33 . 1 1 18 18 GLU H H 1 8.386 0.01 . 1 . . . . . . . . 5996 1 34 . 1 1 18 18 GLU N N 15 121.661 0.10 . 1 . . . . . . . . 5996 1 35 . 1 1 19 19 TRP H H 1 7.476 0.01 . 1 . . . . . . . . 5996 1 36 . 1 1 19 19 TRP N N 15 122.365 0.10 . 1 . . . . . . . . 5996 1 37 . 1 1 20 20 HIS H H 1 8.932 0.01 . 1 . . . . . . . . 5996 1 38 . 1 1 20 20 HIS N N 15 112.684 0.10 . 1 . . . . . . . . 5996 1 39 . 1 1 21 21 THR H H 1 10.389 0.01 . 1 . . . . . . . . 5996 1 40 . 1 1 21 21 THR N N 15 122.737 0.10 . 1 . . . . . . . . 5996 1 41 . 1 1 22 22 ILE H H 1 8.971 0.01 . 1 . . . . . . . . 5996 1 42 . 1 1 22 22 ILE N N 15 127.793 0.10 . 1 . . . . . . . . 5996 1 43 . 1 1 23 23 ILE H H 1 7.534 0.01 . 1 . . . . . . . . 5996 1 44 . 1 1 23 23 ILE N N 15 115.011 0.10 . 1 . . . . . . . . 5996 1 45 . 1 1 24 24 LEU H H 1 8.272 0.01 . 1 . . . . . . . . 5996 1 46 . 1 1 24 24 LEU N N 15 123.133 0.10 . 1 . . . . . . . . 5996 1 47 . 1 1 25 25 ALA H H 1 9.113 0.01 . 1 . . . . . . . . 5996 1 48 . 1 1 25 25 ALA N N 15 122.592 0.10 . 1 . . . . . . . . 5996 1 49 . 1 1 26 26 SER H H 1 7.370 0.01 . 1 . . . . . . . . 5996 1 50 . 1 1 26 26 SER N N 15 112.728 0.10 . 1 . . . . . . . . 5996 1 51 . 1 1 27 27 ASP H H 1 8.695 0.01 . 1 . . . . . . . . 5996 1 52 . 1 1 27 27 ASP N N 15 123.016 0.10 . 1 . . . . . . . . 5996 1 53 . 1 1 28 28 LYS H H 1 8.263 0.01 . 1 . . . . . . . . 5996 1 54 . 1 1 28 28 LYS N N 15 122.827 0.10 . 1 . . . . . . . . 5996 1 55 . 1 1 29 29 ARG H H 1 8.619 0.01 . 1 . . . . . . . . 5996 1 56 . 1 1 29 29 ARG N N 15 127.156 0.10 . 1 . . . . . . . . 5996 1 57 . 1 1 30 30 GLU H H 1 9.403 0.01 . 1 . . . . . . . . 5996 1 58 . 1 1 30 30 GLU N N 15 115.068 0.10 . 1 . . . . . . . . 5996 1 59 . 1 1 31 31 LYS H H 1 7.483 0.01 . 1 . . . . . . . . 5996 1 60 . 1 1 31 31 LYS N N 15 116.324 0.10 . 1 . . . . . . . . 5996 1 61 . 1 1 32 32 ILE H H 1 7.545 0.01 . 1 . . . . . . . . 5996 1 62 . 1 1 32 32 ILE N N 15 106.532 0.10 . 1 . . . . . . . . 5996 1 63 . 1 1 33 33 GLU H H 1 6.633 0.01 . 1 . . . . . . . . 5996 1 64 . 1 1 33 33 GLU N N 15 121.398 0.10 . 1 . . . . . . . . 5996 1 65 . 1 1 34 34 ASP H H 1 8.440 0.01 . 1 . . . . . . . . 5996 1 66 . 1 1 34 34 ASP N N 15 118.288 0.10 . 1 . . . . . . . . 5996 1 67 . 1 1 35 35 ASN H H 1 8.888 0.01 . 1 . . . . . . . . 5996 1 68 . 1 1 35 35 ASN N N 15 116.847 0.10 . 1 . . . . . . . . 5996 1 69 . 1 1 36 36 GLY H H 1 8.792 0.01 . 1 . . . . . . . . 5996 1 70 . 1 1 36 36 GLY N N 15 109.966 0.10 . 1 . . . . . . . . 5996 1 71 . 1 1 37 37 ASN H H 1 9.336 0.01 . 1 . . . . . . . . 5996 1 72 . 1 1 37 37 ASN N N 15 121.331 0.10 . 1 . . . . . . . . 5996 1 73 . 1 1 38 38 PHE H H 1 8.670 0.01 . 1 . . . . . . . . 5996 1 74 . 1 1 38 38 PHE N N 15 115.519 0.10 . 1 . . . . . . . . 5996 1 75 . 1 1 39 39 ARG H H 1 7.131 0.01 . 1 . . . . . . . . 5996 1 76 . 1 1 39 39 ARG N N 15 123.979 0.10 . 1 . . . . . . . . 5996 1 77 . 1 1 40 40 LEU H H 1 6.782 0.01 . 1 . . . . . . . . 5996 1 78 . 1 1 40 40 LEU N N 15 124.226 0.10 . 1 . . . . . . . . 5996 1 79 . 1 1 41 41 PHE H H 1 8.503 0.01 . 1 . . . . . . . . 5996 1 80 . 1 1 41 41 PHE N N 15 123.051 0.10 . 1 . . . . . . . . 5996 1 81 . 1 1 42 42 LEU H H 1 8.491 0.01 . 1 . . . . . . . . 5996 1 82 . 1 1 42 42 LEU N N 15 129.122 0.10 . 1 . . . . . . . . 5996 1 83 . 1 1 43 43 GLU H H 1 9.025 0.01 . 1 . . . . . . . . 5996 1 84 . 1 1 43 43 GLU N N 15 121.331 0.10 . 1 . . . . . . . . 5996 1 85 . 1 1 44 44 GLN H H 1 7.359 0.01 . 1 . . . . . . . . 5996 1 86 . 1 1 44 44 GLN N N 15 115.165 0.10 . 1 . . . . . . . . 5996 1 87 . 1 1 45 45 ILE H H 1 8.792 0.01 . 1 . . . . . . . . 5996 1 88 . 1 1 45 45 ILE N N 15 120.966 0.10 . 1 . . . . . . . . 5996 1 89 . 1 1 46 46 HIS H H 1 9.413 0.01 . 1 . . . . . . . . 5996 1 90 . 1 1 46 46 HIS N N 15 127.214 0.10 . 1 . . . . . . . . 5996 1 91 . 1 1 47 47 VAL H H 1 8.836 0.01 . 1 . . . . . . . . 5996 1 92 . 1 1 47 47 VAL N N 15 128.058 0.10 . 1 . . . . . . . . 5996 1 93 . 1 1 48 48 LEU H H 1 8.245 0.01 . 1 . . . . . . . . 5996 1 94 . 1 1 48 48 LEU N N 15 130.193 0.10 . 1 . . . . . . . . 5996 1 95 . 1 1 49 49 GLU H H 1 8.469 0.01 . 1 . . . . . . . . 5996 1 96 . 1 1 49 49 GLU N N 15 120.118 0.10 . 1 . . . . . . . . 5996 1 97 . 1 1 50 50 ASN H H 1 8.640 0.01 . 1 . . . . . . . . 5996 1 98 . 1 1 50 50 ASN N N 15 114.900 0.10 . 1 . . . . . . . . 5996 1 99 . 1 1 51 51 SER H H 1 7.503 0.01 . 1 . . . . . . . . 5996 1 100 . 1 1 51 51 SER N N 15 112.365 0.10 . 1 . . . . . . . . 5996 1 101 . 1 1 52 52 LEU H H 1 9.227 0.01 . 1 . . . . . . . . 5996 1 102 . 1 1 52 52 LEU N N 15 119.055 0.10 . 1 . . . . . . . . 5996 1 103 . 1 1 53 53 VAL H H 1 9.246 0.01 . 1 . . . . . . . . 5996 1 104 . 1 1 53 53 VAL N N 15 123.001 0.10 . 1 . . . . . . . . 5996 1 105 . 1 1 54 54 LEU H H 1 9.118 0.01 . 1 . . . . . . . . 5996 1 106 . 1 1 54 54 LEU N N 15 129.357 0.10 . 1 . . . . . . . . 5996 1 107 . 1 1 55 55 LYS H H 1 8.013 0.01 . 1 . . . . . . . . 5996 1 108 . 1 1 55 55 LYS N N 15 122.330 0.10 . 1 . . . . . . . . 5996 1 109 . 1 1 56 56 PHE H H 1 9.253 0.01 . 1 . . . . . . . . 5996 1 110 . 1 1 56 56 PHE N N 15 122.623 0.10 . 1 . . . . . . . . 5996 1 111 . 1 1 57 57 HIS H H 1 9.065 0.01 . 1 . . . . . . . . 5996 1 112 . 1 1 57 57 HIS N N 15 113.986 0.10 . 1 . . . . . . . . 5996 1 113 . 1 1 58 58 THR H H 1 9.072 0.01 . 1 . . . . . . . . 5996 1 114 . 1 1 58 58 THR N N 15 113.296 0.10 . 1 . . . . . . . . 5996 1 115 . 1 1 59 59 VAL H H 1 8.939 0.01 . 1 . . . . . . . . 5996 1 116 . 1 1 59 59 VAL N N 15 122.952 0.10 . 1 . . . . . . . . 5996 1 117 . 1 1 60 60 ARG H H 1 8.427 0.01 . 1 . . . . . . . . 5996 1 118 . 1 1 60 60 ARG N N 15 127.731 0.10 . 1 . . . . . . . . 5996 1 119 . 1 1 61 61 ASP H H 1 9.454 0.01 . 1 . . . . . . . . 5996 1 120 . 1 1 61 61 ASP N N 15 127.479 0.10 . 1 . . . . . . . . 5996 1 121 . 1 1 62 62 GLU H H 1 8.422 0.01 . 1 . . . . . . . . 5996 1 122 . 1 1 62 62 GLU N N 15 110.639 0.10 . 1 . . . . . . . . 5996 1 123 . 1 1 63 63 GLU H H 1 8.017 0.01 . 1 . . . . . . . . 5996 1 124 . 1 1 63 63 GLU N N 15 120.381 0.10 . 1 . . . . . . . . 5996 1 125 . 1 1 64 64 CYS H H 1 8.973 0.01 . 1 . . . . . . . . 5996 1 126 . 1 1 64 64 CYS N N 15 124.454 0.10 . 1 . . . . . . . . 5996 1 127 . 1 1 65 65 SER H H 1 8.848 0.01 . 1 . . . . . . . . 5996 1 128 . 1 1 65 65 SER N N 15 118.342 0.10 . 1 . . . . . . . . 5996 1 129 . 1 1 66 66 GLU H H 1 8.700 0.01 . 1 . . . . . . . . 5996 1 130 . 1 1 66 66 GLU N N 15 123.806 0.10 . 1 . . . . . . . . 5996 1 131 . 1 1 67 67 LEU H H 1 8.607 0.01 . 1 . . . . . . . . 5996 1 132 . 1 1 67 67 LEU N N 15 124.866 0.10 . 1 . . . . . . . . 5996 1 133 . 1 1 68 68 SER H H 1 8.580 0.01 . 1 . . . . . . . . 5996 1 134 . 1 1 68 68 SER N N 15 118.844 0.10 . 1 . . . . . . . . 5996 1 135 . 1 1 69 69 MET H H 1 9.093 0.01 . 1 . . . . . . . . 5996 1 136 . 1 1 69 69 MET N N 15 120.332 0.10 . 1 . . . . . . . . 5996 1 137 . 1 1 70 70 VAL H H 1 8.592 0.01 . 1 . . . . . . . . 5996 1 138 . 1 1 70 70 VAL N N 15 121.766 0.10 . 1 . . . . . . . . 5996 1 139 . 1 1 71 71 ALA H H 1 9.493 0.01 . 1 . . . . . . . . 5996 1 140 . 1 1 71 71 ALA N N 15 130.490 0.10 . 1 . . . . . . . . 5996 1 141 . 1 1 72 72 ASP H H 1 8.931 0.01 . 1 . . . . . . . . 5996 1 142 . 1 1 72 72 ASP N N 15 123.306 0.10 . 1 . . . . . . . . 5996 1 143 . 1 1 73 73 LYS H H 1 8.166 0.01 . 1 . . . . . . . . 5996 1 144 . 1 1 73 73 LYS N N 15 121.068 0.10 . 1 . . . . . . . . 5996 1 145 . 1 1 74 74 THR H H 1 7.836 0.01 . 1 . . . . . . . . 5996 1 146 . 1 1 74 74 THR N N 15 114.949 0.10 . 1 . . . . . . . . 5996 1 147 . 1 1 75 75 GLU H H 1 8.699 0.01 . 1 . . . . . . . . 5996 1 148 . 1 1 75 75 GLU N N 15 116.983 0.10 . 1 . . . . . . . . 5996 1 149 . 1 1 76 76 LYS H H 1 8.050 0.01 . 1 . . . . . . . . 5996 1 150 . 1 1 76 76 LYS N N 15 122.350 0.10 . 1 . . . . . . . . 5996 1 151 . 1 1 77 77 ALA H H 1 8.275 0.01 . 1 . . . . . . . . 5996 1 152 . 1 1 77 77 ALA N N 15 127.559 0.10 . 1 . . . . . . . . 5996 1 153 . 1 1 78 78 GLY H H 1 8.417 0.01 . 1 . . . . . . . . 5996 1 154 . 1 1 78 78 GLY N N 15 108.321 0.10 . 1 . . . . . . . . 5996 1 155 . 1 1 79 79 GLU H H 1 7.279 0.01 . 1 . . . . . . . . 5996 1 156 . 1 1 79 79 GLU N N 15 120.481 0.10 . 1 . . . . . . . . 5996 1 157 . 1 1 80 80 TYR H H 1 8.447 0.01 . 1 . . . . . . . . 5996 1 158 . 1 1 80 80 TYR N N 15 125.783 0.10 . 1 . . . . . . . . 5996 1 159 . 1 1 81 81 SER H H 1 9.623 0.01 . 1 . . . . . . . . 5996 1 160 . 1 1 81 81 SER N N 15 114.459 0.10 . 1 . . . . . . . . 5996 1 161 . 1 1 82 82 VAL H H 1 8.593 0.01 . 1 . . . . . . . . 5996 1 162 . 1 1 82 82 VAL N N 15 117.228 0.10 . 1 . . . . . . . . 5996 1 163 . 1 1 83 83 THR H H 1 9.337 0.01 . 1 . . . . . . . . 5996 1 164 . 1 1 83 83 THR N N 15 129.089 0.10 . 1 . . . . . . . . 5996 1 165 . 1 1 84 84 TYR H H 1 8.727 0.01 . 1 . . . . . . . . 5996 1 166 . 1 1 84 84 TYR N N 15 128.752 0.10 . 1 . . . . . . . . 5996 1 167 . 1 1 85 85 ASP H H 1 8.617 0.01 . 1 . . . . . . . . 5996 1 168 . 1 1 85 85 ASP N N 15 129.989 0.10 . 1 . . . . . . . . 5996 1 169 . 1 1 86 86 GLY H H 1 7.860 0.01 . 1 . . . . . . . . 5996 1 170 . 1 1 86 86 GLY N N 15 103.311 0.10 . 1 . . . . . . . . 5996 1 171 . 1 1 87 87 PHE H H 1 8.781 0.01 . 1 . . . . . . . . 5996 1 172 . 1 1 87 87 PHE N N 15 120.195 0.10 . 1 . . . . . . . . 5996 1 173 . 1 1 88 88 ASN H H 1 7.897 0.01 . 1 . . . . . . . . 5996 1 174 . 1 1 88 88 ASN N N 15 123.436 0.10 . 1 . . . . . . . . 5996 1 175 . 1 1 89 89 THR H H 1 8.741 0.01 . 1 . . . . . . . . 5996 1 176 . 1 1 89 89 THR N N 15 112.689 0.10 . 1 . . . . . . . . 5996 1 177 . 1 1 90 90 PHE H H 1 9.410 0.01 . 1 . . . . . . . . 5996 1 178 . 1 1 90 90 PHE N N 15 117.966 0.10 . 1 . . . . . . . . 5996 1 179 . 1 1 91 91 THR H H 1 8.784 0.01 . 1 . . . . . . . . 5996 1 180 . 1 1 91 91 THR N N 15 108.472 0.10 . 1 . . . . . . . . 5996 1 181 . 1 1 92 92 ILE H H 1 8.293 0.01 . 1 . . . . . . . . 5996 1 182 . 1 1 92 92 ILE N N 15 119.496 0.10 . 1 . . . . . . . . 5996 1 183 . 1 1 93 93 PRO N N 15 111.893 0.10 . 1 . . . . . . . . 5996 1 184 . 1 1 94 94 LYS H H 1 6.983 0.01 . 1 . . . . . . . . 5996 1 185 . 1 1 95 95 THR H H 1 8.821 0.01 . 1 . . . . . . . . 5996 1 186 . 1 1 95 95 THR N N 15 119.165 0.10 . 1 . . . . . . . . 5996 1 187 . 1 1 96 96 ASP H H 1 6.928 0.01 . 1 . . . . . . . . 5996 1 188 . 1 1 96 96 ASP N N 15 124.991 0.10 . 1 . . . . . . . . 5996 1 189 . 1 1 97 97 TYR H H 1 8.769 0.01 . 1 . . . . . . . . 5996 1 190 . 1 1 97 97 TYR N N 15 115.881 0.10 . 1 . . . . . . . . 5996 1 191 . 1 1 98 98 ASP H H 1 9.319 0.01 . 1 . . . . . . . . 5996 1 192 . 1 1 98 98 ASP N N 15 119.910 0.10 . 1 . . . . . . . . 5996 1 193 . 1 1 99 99 ASN H H 1 9.025 0.01 . 1 . . . . . . . . 5996 1 194 . 1 1 99 99 ASN N N 15 116.859 0.10 . 1 . . . . . . . . 5996 1 195 . 1 1 100 100 PHE H H 1 9.793 0.01 . 1 . . . . . . . . 5996 1 196 . 1 1 100 100 PHE N N 15 117.749 0.10 . 1 . . . . . . . . 5996 1 197 . 1 1 101 101 LEU H H 1 9.338 0.01 . 1 . . . . . . . . 5996 1 198 . 1 1 101 101 LEU N N 15 126.418 0.10 . 1 . . . . . . . . 5996 1 199 . 1 1 102 102 MET H H 1 9.159 0.01 . 1 . . . . . . . . 5996 1 200 . 1 1 102 102 MET N N 15 125.394 0.10 . 1 . . . . . . . . 5996 1 201 . 1 1 103 103 ALA H H 1 9.431 0.01 . 1 . . . . . . . . 5996 1 202 . 1 1 103 103 ALA N N 15 122.811 0.10 . 1 . . . . . . . . 5996 1 203 . 1 1 104 104 HIS H H 1 8.626 0.01 . 1 . . . . . . . . 5996 1 204 . 1 1 104 104 HIS N N 15 120.857 0.10 . 1 . . . . . . . . 5996 1 205 . 1 1 105 105 LEU H H 1 9.727 0.01 . 1 . . . . . . . . 5996 1 206 . 1 1 105 105 LEU N N 15 132.297 0.10 . 1 . . . . . . . . 5996 1 207 . 1 1 106 106 ILE H H 1 9.111 0.01 . 1 . . . . . . . . 5996 1 208 . 1 1 106 106 ILE N N 15 125.500 0.10 . 1 . . . . . . . . 5996 1 209 . 1 1 107 107 ASN H H 1 8.329 0.01 . 1 . . . . . . . . 5996 1 210 . 1 1 107 107 ASN N N 15 128.527 0.10 . 1 . . . . . . . . 5996 1 211 . 1 1 108 108 GLU H H 1 8.835 0.01 . 1 . . . . . . . . 5996 1 212 . 1 1 108 108 GLU N N 15 124.089 0.10 . 1 . . . . . . . . 5996 1 213 . 1 1 109 109 LYS H H 1 8.672 0.01 . 1 . . . . . . . . 5996 1 214 . 1 1 109 109 LYS N N 15 126.291 0.10 . 1 . . . . . . . . 5996 1 215 . 1 1 110 110 ASP H H 1 9.490 0.01 . 1 . . . . . . . . 5996 1 216 . 1 1 110 110 ASP N N 15 128.992 0.10 . 1 . . . . . . . . 5996 1 217 . 1 1 111 111 GLY H H 1 8.797 0.01 . 1 . . . . . . . . 5996 1 218 . 1 1 111 111 GLY N N 15 104.767 0.10 . 1 . . . . . . . . 5996 1 219 . 1 1 112 112 GLU H H 1 7.973 0.01 . 1 . . . . . . . . 5996 1 220 . 1 1 112 112 GLU N N 15 120.606 0.10 . 1 . . . . . . . . 5996 1 221 . 1 1 113 113 THR H H 1 8.716 0.01 . 1 . . . . . . . . 5996 1 222 . 1 1 113 113 THR N N 15 117.578 0.10 . 1 . . . . . . . . 5996 1 223 . 1 1 114 114 PHE H H 1 8.368 0.01 . 1 . . . . . . . . 5996 1 224 . 1 1 114 114 PHE N N 15 120.362 0.10 . 1 . . . . . . . . 5996 1 225 . 1 1 115 115 GLN H H 1 10.024 0.01 . 1 . . . . . . . . 5996 1 226 . 1 1 115 115 GLN N N 15 118.461 0.10 . 1 . . . . . . . . 5996 1 227 . 1 1 116 116 LEU H H 1 9.392 0.01 . 1 . . . . . . . . 5996 1 228 . 1 1 116 116 LEU N N 15 126.172 0.10 . 1 . . . . . . . . 5996 1 229 . 1 1 117 117 MET H H 1 9.534 0.01 . 1 . . . . . . . . 5996 1 230 . 1 1 117 117 MET N N 15 125.059 0.10 . 1 . . . . . . . . 5996 1 231 . 1 1 118 118 GLY H H 1 8.903 0.01 . 1 . . . . . . . . 5996 1 232 . 1 1 118 118 GLY N N 15 108.770 0.10 . 1 . . . . . . . . 5996 1 233 . 1 1 119 119 LEU H H 1 8.345 0.01 . 1 . . . . . . . . 5996 1 234 . 1 1 119 119 LEU N N 15 124.278 0.10 . 1 . . . . . . . . 5996 1 235 . 1 1 120 120 TYR H H 1 9.388 0.01 . 1 . . . . . . . . 5996 1 236 . 1 1 120 120 TYR N N 15 126.582 0.10 . 1 . . . . . . . . 5996 1 237 . 1 1 121 121 GLY H H 1 9.560 0.01 . 1 . . . . . . . . 5996 1 238 . 1 1 121 121 GLY N N 15 108.387 0.10 . 1 . . . . . . . . 5996 1 239 . 1 1 122 122 ARG H H 1 8.369 0.01 . 1 . . . . . . . . 5996 1 240 . 1 1 122 122 ARG N N 15 122.565 0.10 . 1 . . . . . . . . 5996 1 241 . 1 1 123 123 GLU H H 1 8.442 0.01 . 1 . . . . . . . . 5996 1 242 . 1 1 123 123 GLU N N 15 118.673 0.10 . 1 . . . . . . . . 5996 1 243 . 1 1 125 125 ASP H H 1 7.188 0.01 . 1 . . . . . . . . 5996 1 244 . 1 1 125 125 ASP N N 15 113.878 0.10 . 1 . . . . . . . . 5996 1 245 . 1 1 126 126 LEU H H 1 8.511 0.01 . 1 . . . . . . . . 5996 1 246 . 1 1 126 126 LEU N N 15 119.454 0.10 . 1 . . . . . . . . 5996 1 247 . 1 1 127 127 SER H H 1 8.195 0.01 . 1 . . . . . . . . 5996 1 248 . 1 1 127 127 SER N N 15 114.483 0.10 . 1 . . . . . . . . 5996 1 249 . 1 1 128 128 SER H H 1 8.980 0.01 . 1 . . . . . . . . 5996 1 250 . 1 1 128 128 SER N N 15 118.054 0.10 . 1 . . . . . . . . 5996 1 251 . 1 1 129 129 ASP H H 1 8.506 0.01 . 1 . . . . . . . . 5996 1 252 . 1 1 129 129 ASP N N 15 120.888 0.10 . 1 . . . . . . . . 5996 1 253 . 1 1 130 130 ILE H H 1 7.406 0.01 . 1 . . . . . . . . 5996 1 254 . 1 1 130 130 ILE N N 15 121.650 0.10 . 1 . . . . . . . . 5996 1 255 . 1 1 131 131 LYS H H 1 7.619 0.01 . 1 . . . . . . . . 5996 1 256 . 1 1 131 131 LYS N N 15 119.254 0.10 . 1 . . . . . . . . 5996 1 257 . 1 1 132 132 GLU H H 1 8.238 0.01 . 1 . . . . . . . . 5996 1 258 . 1 1 132 132 GLU N N 15 121.143 0.10 . 1 . . . . . . . . 5996 1 259 . 1 1 133 133 ARG H H 1 7.842 0.01 . 1 . . . . . . . . 5996 1 260 . 1 1 133 133 ARG N N 15 120.706 0.10 . 1 . . . . . . . . 5996 1 261 . 1 1 134 134 PHE H H 1 8.421 0.01 . 1 . . . . . . . . 5996 1 262 . 1 1 134 134 PHE N N 15 120.340 0.10 . 1 . . . . . . . . 5996 1 263 . 1 1 135 135 ALA H H 1 8.342 0.01 . 1 . . . . . . . . 5996 1 264 . 1 1 135 135 ALA N N 15 124.617 0.10 . 1 . . . . . . . . 5996 1 265 . 1 1 136 136 GLN H H 1 8.088 0.01 . 1 . . . . . . . . 5996 1 266 . 1 1 136 136 GLN N N 15 116.119 0.10 . 1 . . . . . . . . 5996 1 267 . 1 1 137 137 LEU H H 1 7.545 0.01 . 1 . . . . . . . . 5996 1 268 . 1 1 137 137 LEU N N 15 123.140 0.10 . 1 . . . . . . . . 5996 1 269 . 1 1 138 138 CYS H H 1 8.022 0.01 . 1 . . . . . . . . 5996 1 270 . 1 1 138 138 CYS N N 15 118.786 0.10 . 1 . . . . . . . . 5996 1 271 . 1 1 139 139 GLU H H 1 7.987 0.01 . 1 . . . . . . . . 5996 1 272 . 1 1 139 139 GLU N N 15 120.609 0.10 . 1 . . . . . . . . 5996 1 273 . 1 1 140 140 LYS H H 1 7.739 0.01 . 1 . . . . . . . . 5996 1 274 . 1 1 140 140 LYS N N 15 120.700 0.10 . 1 . . . . . . . . 5996 1 275 . 1 1 141 141 HIS H H 1 7.453 0.01 . 1 . . . . . . . . 5996 1 276 . 1 1 141 141 HIS N N 15 115.962 0.10 . 1 . . . . . . . . 5996 1 277 . 1 1 142 142 GLY H H 1 7.775 0.01 . 1 . . . . . . . . 5996 1 278 . 1 1 142 142 GLY N N 15 106.807 0.10 . 1 . . . . . . . . 5996 1 279 . 1 1 143 143 ILE H H 1 7.839 0.01 . 1 . . . . . . . . 5996 1 280 . 1 1 143 143 ILE N N 15 122.924 0.10 . 1 . . . . . . . . 5996 1 281 . 1 1 144 144 LEU H H 1 8.019 0.01 . 1 . . . . . . . . 5996 1 282 . 1 1 144 144 LEU N N 15 125.106 0.10 . 1 . . . . . . . . 5996 1 283 . 1 1 145 145 ARG H H 1 8.667 0.01 . 1 . . . . . . . . 5996 1 284 . 1 1 145 145 ARG N N 15 119.781 0.10 . 1 . . . . . . . . 5996 1 285 . 1 1 146 146 GLU H H 1 8.810 0.01 . 1 . . . . . . . . 5996 1 286 . 1 1 146 146 GLU N N 15 116.749 0.10 . 1 . . . . . . . . 5996 1 287 . 1 1 147 147 ASN H H 1 8.214 0.01 . 1 . . . . . . . . 5996 1 288 . 1 1 147 147 ASN N N 15 120.859 0.10 . 1 . . . . . . . . 5996 1 289 . 1 1 148 148 ILE H H 1 7.110 0.01 . 1 . . . . . . . . 5996 1 290 . 1 1 148 148 ILE N N 15 118.491 0.10 . 1 . . . . . . . . 5996 1 291 . 1 1 149 149 ILE H H 1 9.367 0.01 . 1 . . . . . . . . 5996 1 292 . 1 1 149 149 ILE N N 15 128.783 0.10 . 1 . . . . . . . . 5996 1 293 . 1 1 150 150 ASP H H 1 8.703 0.01 . 1 . . . . . . . . 5996 1 294 . 1 1 150 150 ASP N N 15 127.365 0.10 . 1 . . . . . . . . 5996 1 295 . 1 1 151 151 LEU H H 1 9.019 0.01 . 1 . . . . . . . . 5996 1 296 . 1 1 151 151 LEU N N 15 130.437 0.10 . 1 . . . . . . . . 5996 1 297 . 1 1 152 152 SER H H 1 9.046 0.01 . 1 . . . . . . . . 5996 1 298 . 1 1 152 152 SER N N 15 118.980 0.10 . 1 . . . . . . . . 5996 1 299 . 1 1 153 153 ASN H H 1 8.399 0.01 . 1 . . . . . . . . 5996 1 300 . 1 1 153 153 ASN N N 15 117.700 0.10 . 1 . . . . . . . . 5996 1 301 . 1 1 154 154 ALA H H 1 7.830 0.01 . 1 . . . . . . . . 5996 1 302 . 1 1 154 154 ALA N N 15 122.605 0.10 . 1 . . . . . . . . 5996 1 303 . 1 1 155 155 ASN H H 1 7.986 0.01 . 1 . . . . . . . . 5996 1 304 . 1 1 155 155 ASN N N 15 117.043 0.10 . 1 . . . . . . . . 5996 1 305 . 1 1 156 156 ARG H H 1 7.916 0.01 . 1 . . . . . . . . 5996 1 306 . 1 1 156 156 ARG N N 15 122.170 0.10 . 1 . . . . . . . . 5996 1 307 . 1 1 157 157 CYS H H 1 8.319 0.01 . 1 . . . . . . . . 5996 1 308 . 1 1 157 157 CYS N N 15 118.221 0.10 . 1 . . . . . . . . 5996 1 309 . 1 1 158 158 LEU H H 1 8.103 0.01 . 1 . . . . . . . . 5996 1 310 . 1 1 158 158 LEU N N 15 122.760 0.10 . 1 . . . . . . . . 5996 1 311 . 1 1 159 159 GLN H H 1 8.316 0.01 . 1 . . . . . . . . 5996 1 312 . 1 1 159 159 GLN N N 15 120.951 0.10 . 1 . . . . . . . . 5996 1 313 . 1 1 160 160 ALA H H 1 8.235 0.01 . 1 . . . . . . . . 5996 1 314 . 1 1 160 160 ALA N N 15 125.851 0.10 . 1 . . . . . . . . 5996 1 315 . 1 1 161 161 ARG H H 1 8.229 0.01 . 1 . . . . . . . . 5996 1 316 . 1 1 161 161 ARG N N 15 121.126 0.10 . 1 . . . . . . . . 5996 1 317 . 1 1 162 162 GLU H H 1 7.996 0.01 . 1 . . . . . . . . 5996 1 318 . 1 1 162 162 GLU N N 15 127.051 0.10 . 1 . . . . . . . . 5996 1 stop_ save_ ############################## # Heteronuclear NOE values # ############################## save_283_600_bound_noe _Heteronucl_NOE_list.Sf_category heteronucl_NOEs _Heteronucl_NOE_list.Sf_framecode 283_600_bound_noe _Heteronucl_NOE_list.Entry_ID 5996 _Heteronucl_NOE_list.ID 1 _Heteronucl_NOE_list.Sample_condition_list_ID 1 _Heteronucl_NOE_list.Sample_condition_list_label $283K _Heteronucl_NOE_list.Spectrometer_frequency_1H 600 _Heteronucl_NOE_list.Heteronuclear_NOE_val_type 'relative intensities' _Heteronucl_NOE_list.NOE_ref_val . _Heteronucl_NOE_list.NOE_ref_description . _Heteronucl_NOE_list.Details . _Heteronucl_NOE_list.Text_data_format . _Heteronucl_NOE_list.Text_data . loop_ _Heteronucl_NOE_experiment.Experiment_ID _Heteronucl_NOE_experiment.Experiment_name _Heteronucl_NOE_experiment.Sample_ID _Heteronucl_NOE_experiment.Sample_label _Heteronucl_NOE_experiment.Sample_state _Heteronucl_NOE_experiment.Entry_ID _Heteronucl_NOE_experiment.Heteronucl_NOE_list_ID 3 '{1H}-15N NOE' 1 $sample_1 . 5996 1 stop_ loop_ _Heteronucl_NOE.ID _Heteronucl_NOE.Assembly_atom_ID_1 _Heteronucl_NOE.Entity_assembly_ID_1 _Heteronucl_NOE.Entity_ID_1 _Heteronucl_NOE.Comp_index_ID_1 _Heteronucl_NOE.Seq_ID_1 _Heteronucl_NOE.Comp_ID_1 _Heteronucl_NOE.Atom_ID_1 _Heteronucl_NOE.Atom_type_1 _Heteronucl_NOE.Atom_isotope_number_1 _Heteronucl_NOE.Assembly_atom_ID_2 _Heteronucl_NOE.Entity_assembly_ID_2 _Heteronucl_NOE.Entity_ID_2 _Heteronucl_NOE.Comp_index_ID_2 _Heteronucl_NOE.Seq_ID_2 _Heteronucl_NOE.Comp_ID_2 _Heteronucl_NOE.Atom_ID_2 _Heteronucl_NOE.Atom_type_2 _Heteronucl_NOE.Atom_isotope_number_2 _Heteronucl_NOE.Val _Heteronucl_NOE.Val_err _Heteronucl_NOE.Resonance_ID_1 _Heteronucl_NOE.Resonance_ID_2 _Heteronucl_NOE.Auth_entity_assembly_ID_1 _Heteronucl_NOE.Auth_seq_ID_1 _Heteronucl_NOE.Auth_comp_ID_1 _Heteronucl_NOE.Auth_atom_ID_1 _Heteronucl_NOE.Auth_entity_assembly_ID_2 _Heteronucl_NOE.Auth_seq_ID_2 _Heteronucl_NOE.Auth_comp_ID_2 _Heteronucl_NOE.Auth_atom_ID_2 _Heteronucl_NOE.Entry_ID _Heteronucl_NOE.Heteronucl_NOE_list_ID 1 . 1 1 3 3 ALA N N 15 . 1 1 3 3 ALA H H 1 0.67 0.01 . . . . . . . . . . 5996 1 2 . 1 1 4 4 SER N N 15 . 1 1 4 4 SER H H 1 0.73 0.01 . . . . . . . . . . 5996 1 3 . 1 1 5 5 SER N N 15 . 1 1 5 5 SER H H 1 0.80 0.03 . . . . . . . . . . 5996 1 4 . 1 1 6 6 THR N N 15 . 1 1 6 6 THR H H 1 0.78 0.01 . . . . . . . . . . 5996 1 5 . 1 1 7 7 GLY N N 15 . 1 1 7 7 GLY H H 1 0.71 0.01 . . . . . . . . . . 5996 1 6 . 1 1 10 10 PHE N N 15 . 1 1 10 10 PHE H H 1 0.49 0.01 . . . . . . . . . . 5996 1 7 . 1 1 11 11 ASN N N 15 . 1 1 11 11 ASN H H 1 0.79 0.03 . . . . . . . . . . 5996 1 8 . 1 1 12 12 VAL N N 15 . 1 1 12 12 VAL H H 1 0.79 0.01 . . . . . . . . . . 5996 1 9 . 1 1 13 13 GLU N N 15 . 1 1 13 13 GLU H H 1 0.76 0.01 . . . . . . . . . . 5996 1 10 . 1 1 15 15 ILE N N 15 . 1 1 15 15 ILE H H 1 0.78 0.01 . . . . . . . . . . 5996 1 11 . 1 1 16 16 ASN N N 15 . 1 1 16 16 ASN H H 1 0.83 0.01 . . . . . . . . . . 5996 1 12 . 1 1 17 17 GLY N N 15 . 1 1 17 17 GLY H H 1 0.85 0.01 . . . . . . . . . . 5996 1 13 . 1 1 18 18 GLU N N 15 . 1 1 18 18 GLU H H 1 0.13 0.05 . . . . . . . . . . 5996 1 14 . 1 1 22 22 ILE N N 15 . 1 1 22 22 ILE H H 1 0.82 0.02 . . . . . . . . . . 5996 1 15 . 1 1 23 23 ILE N N 15 . 1 1 23 23 ILE H H 1 0.83 0.01 . . . . . . . . . . 5996 1 16 . 1 1 26 26 SER N N 15 . 1 1 26 26 SER H H 1 0.81 0.01 . . . . . . . . . . 5996 1 17 . 1 1 27 27 ASP N N 15 . 1 1 27 27 ASP H H 1 0.66 0.01 . . . . . . . . . . 5996 1 18 . 1 1 29 29 ARG N N 15 . 1 1 29 29 ARG H H 1 0.80 0.01 . . . . . . . . . . 5996 1 19 . 1 1 30 30 GLU N N 15 . 1 1 30 30 GLU H H 1 0.78 0.01 . . . . . . . . . . 5996 1 20 . 1 1 31 31 LYS N N 15 . 1 1 31 31 LYS H H 1 0.84 0.01 . . . . . . . . . . 5996 1 21 . 1 1 32 32 ILE N N 15 . 1 1 32 32 ILE H H 1 0.85 0.01 . . . . . . . . . . 5996 1 22 . 1 1 33 33 GLU N N 15 . 1 1 33 33 GLU H H 1 0.82 0.02 . . . . . . . . . . 5996 1 23 . 1 1 36 36 GLY N N 15 . 1 1 36 36 GLY H H 1 0.82 0.02 . . . . . . . . . . 5996 1 24 . 1 1 37 37 ASN N N 15 . 1 1 37 37 ASN H H 1 0.77 0.01 . . . . . . . . . . 5996 1 25 . 1 1 38 38 PHE N N 15 . 1 1 38 38 PHE H H 1 0.84 0.02 . . . . . . . . . . 5996 1 26 . 1 1 46 46 HIS N N 15 . 1 1 46 46 HIS H H 1 0.80 0.02 . . . . . . . . . . 5996 1 27 . 1 1 48 48 LEU N N 15 . 1 1 48 48 LEU H H 1 0.81 0.01 . . . . . . . . . . 5996 1 28 . 1 1 50 50 ASN N N 15 . 1 1 50 50 ASN H H 1 0.67 0.01 . . . . . . . . . . 5996 1 29 . 1 1 51 51 SER N N 15 . 1 1 51 51 SER H H 1 0.71 0.01 . . . . . . . . . . 5996 1 30 . 1 1 52 52 LEU N N 15 . 1 1 52 52 LEU H H 1 0.78 0.01 . . . . . . . . . . 5996 1 31 . 1 1 54 54 LEU N N 15 . 1 1 54 54 LEU H H 1 0.81 0.01 . . . . . . . . . . 5996 1 32 . 1 1 55 55 LYS N N 15 . 1 1 55 55 LYS H H 1 0.76 0.01 . . . . . . . . . . 5996 1 33 . 1 1 61 61 ASP N N 15 . 1 1 61 61 ASP H H 1 0.69 0.01 . . . . . . . . . . 5996 1 34 . 1 1 66 66 GLU N N 15 . 1 1 66 66 GLU H H 1 0.79 0.01 . . . . . . . . . . 5996 1 35 . 1 1 67 67 LEU N N 15 . 1 1 67 67 LEU H H 1 0.76 0.01 . . . . . . . . . . 5996 1 36 . 1 1 68 68 SER N N 15 . 1 1 68 68 SER H H 1 0.75 0.01 . . . . . . . . . . 5996 1 37 . 1 1 70 70 VAL N N 15 . 1 1 70 70 VAL H H 1 0.80 0.01 . . . . . . . . . . 5996 1 38 . 1 1 71 71 ALA N N 15 . 1 1 71 71 ALA H H 1 0.79 0.01 . . . . . . . . . . 5996 1 39 . 1 1 72 72 ASP N N 15 . 1 1 72 72 ASP H H 1 0.82 0.01 . . . . . . . . . . 5996 1 40 . 1 1 74 74 THR N N 15 . 1 1 74 74 THR H H 1 0.70 0.01 . . . . . . . . . . 5996 1 41 . 1 1 75 75 GLU N N 15 . 1 1 75 75 GLU H H 1 0.67 0.01 . . . . . . . . . . 5996 1 42 . 1 1 76 76 LYS N N 15 . 1 1 76 76 LYS H H 1 0.79 0.01 . . . . . . . . . . 5996 1 43 . 1 1 78 78 GLY N N 15 . 1 1 78 78 GLY H H 1 0.64 0.01 . . . . . . . . . . 5996 1 44 . 1 1 79 79 GLU N N 15 . 1 1 79 79 GLU H H 1 0.82 0.01 . . . . . . . . . . 5996 1 45 . 1 1 80 80 TYR N N 15 . 1 1 80 80 TYR H H 1 0.80 0.01 . . . . . . . . . . 5996 1 46 . 1 1 81 81 SER N N 15 . 1 1 81 81 SER H H 1 0.84 0.01 . . . . . . . . . . 5996 1 47 . 1 1 82 82 VAL N N 15 . 1 1 82 82 VAL H H 1 0.81 0.01 . . . . . . . . . . 5996 1 48 . 1 1 84 84 TYR N N 15 . 1 1 84 84 TYR H H 1 0.81 0.01 . . . . . . . . . . 5996 1 49 . 1 1 85 85 ASP N N 15 . 1 1 85 85 ASP H H 1 0.82 0.01 . . . . . . . . . . 5996 1 50 . 1 1 86 86 GLY N N 15 . 1 1 86 86 GLY H H 1 0.81 0.01 . . . . . . . . . . 5996 1 51 . 1 1 89 89 THR N N 15 . 1 1 89 89 THR H H 1 0.82 0.01 . . . . . . . . . . 5996 1 52 . 1 1 90 90 PHE N N 15 . 1 1 90 90 PHE H H 1 0.82 0.01 . . . . . . . . . . 5996 1 53 . 1 1 91 91 THR N N 15 . 1 1 91 91 THR H H 1 0.80 0.01 . . . . . . . . . . 5996 1 54 . 1 1 92 92 ILE N N 15 . 1 1 92 92 ILE H H 1 0.77 0.01 . . . . . . . . . . 5996 1 55 . 1 1 94 94 LYS N N 15 . 1 1 94 94 LYS H H 1 0.83 0.01 . . . . . . . . . . 5996 1 56 . 1 1 96 96 ASP N N 15 . 1 1 96 96 ASP H H 1 0.83 0.01 . . . . . . . . . . 5996 1 57 . 1 1 98 98 ASP N N 15 . 1 1 98 98 ASP H H 1 0.86 0.02 . . . . . . . . . . 5996 1 58 . 1 1 100 100 PHE N N 15 . 1 1 100 100 PHE H H 1 0.81 0.01 . . . . . . . . . . 5996 1 59 . 1 1 101 101 LEU N N 15 . 1 1 101 101 LEU H H 1 0.85 0.01 . . . . . . . . . . 5996 1 60 . 1 1 103 103 ALA N N 15 . 1 1 103 103 ALA H H 1 0.78 0.04 . . . . . . . . . . 5996 1 61 . 1 1 104 104 HIS N N 15 . 1 1 104 104 HIS H H 1 0.73 0.01 . . . . . . . . . . 5996 1 62 . 1 1 105 105 LEU N N 15 . 1 1 105 105 LEU H H 1 0.85 0.01 . . . . . . . . . . 5996 1 63 . 1 1 107 107 ASN N N 15 . 1 1 107 107 ASN H H 1 0.83 0.02 . . . . . . . . . . 5996 1 64 . 1 1 108 108 GLU N N 15 . 1 1 108 108 GLU H H 1 0.81 0.01 . . . . . . . . . . 5996 1 65 . 1 1 109 109 LYS N N 15 . 1 1 109 109 LYS H H 1 0.79 0.01 . . . . . . . . . . 5996 1 66 . 1 1 110 110 ASP N N 15 . 1 1 110 110 ASP H H 1 0.74 0.01 . . . . . . . . . . 5996 1 67 . 1 1 111 111 GLY N N 15 . 1 1 111 111 GLY H H 1 0.70 0.01 . . . . . . . . . . 5996 1 68 . 1 1 113 113 THR N N 15 . 1 1 113 113 THR H H 1 0.73 0.01 . . . . . . . . . . 5996 1 69 . 1 1 114 114 PHE N N 15 . 1 1 114 114 PHE H H 1 0.74 0.01 . . . . . . . . . . 5996 1 70 . 1 1 115 115 GLN N N 15 . 1 1 115 115 GLN H H 1 0.81 0.01 . . . . . . . . . . 5996 1 71 . 1 1 116 116 LEU N N 15 . 1 1 116 116 LEU H H 1 0.83 0.01 . . . . . . . . . . 5996 1 72 . 1 1 117 117 MET N N 15 . 1 1 117 117 MET H H 1 0.85 0.02 . . . . . . . . . . 5996 1 73 . 1 1 118 118 GLY N N 15 . 1 1 118 118 GLY H H 1 0.82 0.01 . . . . . . . . . . 5996 1 74 . 1 1 119 119 LEU N N 15 . 1 1 119 119 LEU H H 1 0.82 0.02 . . . . . . . . . . 5996 1 75 . 1 1 121 121 GLY N N 15 . 1 1 121 121 GLY H H 1 0.82 0.02 . . . . . . . . . . 5996 1 76 . 1 1 123 123 GLU N N 15 . 1 1 123 123 GLU H H 1 0.77 0.01 . . . . . . . . . . 5996 1 77 . 1 1 125 125 ASP N N 15 . 1 1 125 125 ASP H H 1 0.80 0.01 . . . . . . . . . . 5996 1 78 . 1 1 126 126 LEU N N 15 . 1 1 126 126 LEU H H 1 0.75 0.01 . . . . . . . . . . 5996 1 79 . 1 1 127 127 SER N N 15 . 1 1 127 127 SER H H 1 0.79 0.01 . . . . . . . . . . 5996 1 80 . 1 1 129 129 ASP N N 15 . 1 1 129 129 ASP H H 1 0.79 0.01 . . . . . . . . . . 5996 1 81 . 1 1 130 130 ILE N N 15 . 1 1 130 130 ILE H H 1 0.82 0.01 . . . . . . . . . . 5996 1 82 . 1 1 131 131 LYS N N 15 . 1 1 131 131 LYS H H 1 0.83 0.01 . . . . . . . . . . 5996 1 83 . 1 1 133 133 ARG N N 15 . 1 1 133 133 ARG H H 1 0.83 0.01 . . . . . . . . . . 5996 1 84 . 1 1 135 135 ALA N N 15 . 1 1 135 135 ALA H H 1 0.84 0.01 . . . . . . . . . . 5996 1 85 . 1 1 136 136 GLN N N 15 . 1 1 136 136 GLN H H 1 0.81 0.01 . . . . . . . . . . 5996 1 86 . 1 1 137 137 LEU N N 15 . 1 1 137 137 LEU H H 1 0.84 0.01 . . . . . . . . . . 5996 1 87 . 1 1 138 138 CYS N N 15 . 1 1 138 138 CYS H H 1 0.81 0.01 . . . . . . . . . . 5996 1 88 . 1 1 140 140 LYS N N 15 . 1 1 140 140 LYS H H 1 0.81 0.01 . . . . . . . . . . 5996 1 89 . 1 1 141 141 HIS N N 15 . 1 1 141 141 HIS H H 1 0.77 0.01 . . . . . . . . . . 5996 1 90 . 1 1 142 142 GLY N N 15 . 1 1 142 142 GLY H H 1 0.78 0.01 . . . . . . . . . . 5996 1 91 . 1 1 144 144 LEU N N 15 . 1 1 144 144 LEU H H 1 0.66 0.01 . . . . . . . . . . 5996 1 92 . 1 1 145 145 ARG N N 15 . 1 1 145 145 ARG H H 1 0.27 0.01 . . . . . . . . . . 5996 1 93 . 1 1 150 150 ASP N N 15 . 1 1 150 150 ASP H H 1 0.80 0.01 . . . . . . . . . . 5996 1 94 . 1 1 151 151 LEU N N 15 . 1 1 151 151 LEU H H 1 0.79 0.04 . . . . . . . . . . 5996 1 95 . 1 1 152 152 SER N N 15 . 1 1 152 152 SER H H 1 0.80 0.01 . . . . . . . . . . 5996 1 96 . 1 1 162 162 GLU N N 15 . 1 1 162 162 GLU H H 1 -0.31 0.01 . . . . . . . . . . 5996 1 stop_ save_ save_288_600_bound_noe _Heteronucl_NOE_list.Sf_category heteronucl_NOEs _Heteronucl_NOE_list.Sf_framecode 288_600_bound_noe _Heteronucl_NOE_list.Entry_ID 5996 _Heteronucl_NOE_list.ID 2 _Heteronucl_NOE_list.Sample_condition_list_ID 2 _Heteronucl_NOE_list.Sample_condition_list_label $288K _Heteronucl_NOE_list.Spectrometer_frequency_1H 600 _Heteronucl_NOE_list.Heteronuclear_NOE_val_type 'relative intensities' _Heteronucl_NOE_list.NOE_ref_val . _Heteronucl_NOE_list.NOE_ref_description . _Heteronucl_NOE_list.Details . _Heteronucl_NOE_list.Text_data_format . _Heteronucl_NOE_list.Text_data . loop_ _Heteronucl_NOE_experiment.Experiment_ID _Heteronucl_NOE_experiment.Experiment_name _Heteronucl_NOE_experiment.Sample_ID _Heteronucl_NOE_experiment.Sample_label _Heteronucl_NOE_experiment.Sample_state _Heteronucl_NOE_experiment.Entry_ID _Heteronucl_NOE_experiment.Heteronucl_NOE_list_ID 3 '{1H}-15N NOE' 1 $sample_1 . 5996 2 stop_ loop_ _Heteronucl_NOE.ID _Heteronucl_NOE.Assembly_atom_ID_1 _Heteronucl_NOE.Entity_assembly_ID_1 _Heteronucl_NOE.Entity_ID_1 _Heteronucl_NOE.Comp_index_ID_1 _Heteronucl_NOE.Seq_ID_1 _Heteronucl_NOE.Comp_ID_1 _Heteronucl_NOE.Atom_ID_1 _Heteronucl_NOE.Atom_type_1 _Heteronucl_NOE.Atom_isotope_number_1 _Heteronucl_NOE.Assembly_atom_ID_2 _Heteronucl_NOE.Entity_assembly_ID_2 _Heteronucl_NOE.Entity_ID_2 _Heteronucl_NOE.Comp_index_ID_2 _Heteronucl_NOE.Seq_ID_2 _Heteronucl_NOE.Comp_ID_2 _Heteronucl_NOE.Atom_ID_2 _Heteronucl_NOE.Atom_type_2 _Heteronucl_NOE.Atom_isotope_number_2 _Heteronucl_NOE.Val _Heteronucl_NOE.Val_err _Heteronucl_NOE.Resonance_ID_1 _Heteronucl_NOE.Resonance_ID_2 _Heteronucl_NOE.Auth_entity_assembly_ID_1 _Heteronucl_NOE.Auth_seq_ID_1 _Heteronucl_NOE.Auth_comp_ID_1 _Heteronucl_NOE.Auth_atom_ID_1 _Heteronucl_NOE.Auth_entity_assembly_ID_2 _Heteronucl_NOE.Auth_seq_ID_2 _Heteronucl_NOE.Auth_comp_ID_2 _Heteronucl_NOE.Auth_atom_ID_2 _Heteronucl_NOE.Entry_ID _Heteronucl_NOE.Heteronucl_NOE_list_ID 1 . 1 1 3 3 ALA N N 15 . 1 1 3 3 ALA H H 1 0.69 0.02 . . . . . . . . . . 5996 2 2 . 1 1 4 4 SER N N 15 . 1 1 4 4 SER H H 1 0.75 0.02 . . . . . . . . . . 5996 2 3 . 1 1 5 5 SER N N 15 . 1 1 5 5 SER H H 1 0.83 0.02 . . . . . . . . . . 5996 2 4 . 1 1 6 6 THR N N 15 . 1 1 6 6 THR H H 1 0.78 0.02 . . . . . . . . . . 5996 2 5 . 1 1 7 7 GLY N N 15 . 1 1 7 7 GLY H H 1 0.70 0.02 . . . . . . . . . . 5996 2 6 . 1 1 10 10 PHE N N 15 . 1 1 10 10 PHE H H 1 0.52 0.02 . . . . . . . . . . 5996 2 7 . 1 1 12 12 VAL N N 15 . 1 1 12 12 VAL H H 1 0.81 0.02 . . . . . . . . . . 5996 2 8 . 1 1 13 13 GLU N N 15 . 1 1 13 13 GLU H H 1 0.78 0.02 . . . . . . . . . . 5996 2 9 . 1 1 15 15 ILE N N 15 . 1 1 15 15 ILE H H 1 0.77 0.02 . . . . . . . . . . 5996 2 10 . 1 1 16 16 ASN N N 15 . 1 1 16 16 ASN H H 1 0.82 0.02 . . . . . . . . . . 5996 2 11 . 1 1 17 17 GLY N N 15 . 1 1 17 17 GLY H H 1 0.80 0.02 . . . . . . . . . . 5996 2 12 . 1 1 18 18 GLU N N 15 . 1 1 18 18 GLU H H 1 0.79 0.02 . . . . . . . . . . 5996 2 13 . 1 1 19 19 TRP N N 15 . 1 1 19 19 TRP H H 1 0.82 0.02 . . . . . . . . . . 5996 2 14 . 1 1 20 20 HIS N N 15 . 1 1 20 20 HIS H H 1 0.79 0.02 . . . . . . . . . . 5996 2 15 . 1 1 21 21 THR N N 15 . 1 1 21 21 THR H H 1 0.86 0.04 . . . . . . . . . . 5996 2 16 . 1 1 22 22 ILE N N 15 . 1 1 22 22 ILE H H 1 0.82 0.02 . . . . . . . . . . 5996 2 17 . 1 1 23 23 ILE N N 15 . 1 1 23 23 ILE H H 1 0.79 0.02 . . . . . . . . . . 5996 2 18 . 1 1 26 26 SER N N 15 . 1 1 26 26 SER H H 1 0.83 0.02 . . . . . . . . . . 5996 2 19 . 1 1 27 27 ASP N N 15 . 1 1 27 27 ASP H H 1 0.80 0.02 . . . . . . . . . . 5996 2 20 . 1 1 29 29 ARG N N 15 . 1 1 29 29 ARG H H 1 0.82 0.02 . . . . . . . . . . 5996 2 21 . 1 1 30 30 GLU N N 15 . 1 1 30 30 GLU H H 1 0.78 0.02 . . . . . . . . . . 5996 2 22 . 1 1 31 31 LYS N N 15 . 1 1 31 31 LYS H H 1 0.81 0.02 . . . . . . . . . . 5996 2 23 . 1 1 32 32 ILE N N 15 . 1 1 32 32 ILE H H 1 0.83 0.02 . . . . . . . . . . 5996 2 24 . 1 1 33 33 GLU N N 15 . 1 1 33 33 GLU H H 1 0.82 0.02 . . . . . . . . . . 5996 2 25 . 1 1 35 35 ASN N N 15 . 1 1 35 35 ASN H H 1 0.80 0.01 . . . . . . . . . . 5996 2 26 . 1 1 36 36 GLY N N 15 . 1 1 36 36 GLY H H 1 0.84 0.02 . . . . . . . . . . 5996 2 27 . 1 1 37 37 ASN N N 15 . 1 1 37 37 ASN H H 1 0.78 0.01 . . . . . . . . . . 5996 2 28 . 1 1 38 38 PHE N N 15 . 1 1 38 38 PHE H H 1 0.82 0.02 . . . . . . . . . . 5996 2 29 . 1 1 39 39 ARG N N 15 . 1 1 39 39 ARG H H 1 0.82 0.02 . . . . . . . . . . 5996 2 30 . 1 1 40 40 LEU N N 15 . 1 1 40 40 LEU H H 1 0.82 0.02 . . . . . . . . . . 5996 2 31 . 1 1 42 42 LEU N N 15 . 1 1 42 42 LEU H H 1 0.86 0.04 . . . . . . . . . . 5996 2 32 . 1 1 45 45 ILE N N 15 . 1 1 45 45 ILE H H 1 0.77 0.02 . . . . . . . . . . 5996 2 33 . 1 1 46 46 HIS N N 15 . 1 1 46 46 HIS H H 1 0.81 0.02 . . . . . . . . . . 5996 2 34 . 1 1 48 48 LEU N N 15 . 1 1 48 48 LEU H H 1 0.80 0.02 . . . . . . . . . . 5996 2 35 . 1 1 50 50 ASN N N 15 . 1 1 50 50 ASN H H 1 0.68 0.02 . . . . . . . . . . 5996 2 36 . 1 1 51 51 SER N N 15 . 1 1 51 51 SER H H 1 0.72 0.02 . . . . . . . . . . 5996 2 37 . 1 1 52 52 LEU N N 15 . 1 1 52 52 LEU H H 1 0.79 0.02 . . . . . . . . . . 5996 2 38 . 1 1 53 53 VAL N N 15 . 1 1 53 53 VAL H H 1 0.78 0.01 . . . . . . . . . . 5996 2 39 . 1 1 54 54 LEU N N 15 . 1 1 54 54 LEU H H 1 0.83 0.02 . . . . . . . . . . 5996 2 40 . 1 1 55 55 LYS N N 15 . 1 1 55 55 LYS H H 1 0.75 0.02 . . . . . . . . . . 5996 2 41 . 1 1 57 57 HIS N N 15 . 1 1 57 57 HIS H H 1 0.82 0.02 . . . . . . . . . . 5996 2 42 . 1 1 60 60 ARG N N 15 . 1 1 60 60 ARG H H 1 0.68 0.02 . . . . . . . . . . 5996 2 43 . 1 1 61 61 ASP N N 15 . 1 1 61 61 ASP H H 1 0.70 0.02 . . . . . . . . . . 5996 2 44 . 1 1 62 62 GLU N N 15 . 1 1 62 62 GLU H H 1 0.67 0.01 . . . . . . . . . . 5996 2 45 . 1 1 64 64 CYS N N 15 . 1 1 64 64 CYS H H 1 0.68 0.01 . . . . . . . . . . 5996 2 46 . 1 1 66 66 GLU N N 15 . 1 1 66 66 GLU H H 1 0.70 0.02 . . . . . . . . . . 5996 2 47 . 1 1 67 67 LEU N N 15 . 1 1 67 67 LEU H H 1 0.79 0.01 . . . . . . . . . . 5996 2 48 . 1 1 68 68 SER N N 15 . 1 1 68 68 SER H H 1 0.75 0.02 . . . . . . . . . . 5996 2 49 . 1 1 69 69 MET N N 15 . 1 1 69 69 MET H H 1 0.79 0.01 . . . . . . . . . . 5996 2 50 . 1 1 71 71 ALA N N 15 . 1 1 71 71 ALA H H 1 0.78 0.01 . . . . . . . . . . 5996 2 51 . 1 1 72 72 ASP N N 15 . 1 1 72 72 ASP H H 1 0.78 0.02 . . . . . . . . . . 5996 2 52 . 1 1 74 74 THR N N 15 . 1 1 74 74 THR H H 1 0.70 0.02 . . . . . . . . . . 5996 2 53 . 1 1 75 75 GLU N N 15 . 1 1 75 75 GLU H H 1 0.67 0.02 . . . . . . . . . . 5996 2 54 . 1 1 77 77 ALA N N 15 . 1 1 77 77 ALA H H 1 0.70 0.01 . . . . . . . . . . 5996 2 55 . 1 1 78 78 GLY N N 15 . 1 1 78 78 GLY H H 1 0.66 0.02 . . . . . . . . . . 5996 2 56 . 1 1 79 79 GLU N N 15 . 1 1 79 79 GLU H H 1 0.80 0.02 . . . . . . . . . . 5996 2 57 . 1 1 80 80 TYR N N 15 . 1 1 80 80 TYR H H 1 0.79 0.02 . . . . . . . . . . 5996 2 58 . 1 1 81 81 SER N N 15 . 1 1 81 81 SER H H 1 0.82 0.02 . . . . . . . . . . 5996 2 59 . 1 1 82 82 VAL N N 15 . 1 1 82 82 VAL H H 1 0.82 0.02 . . . . . . . . . . 5996 2 60 . 1 1 84 84 TYR N N 15 . 1 1 84 84 TYR H H 1 0.82 0.01 . . . . . . . . . . 5996 2 61 . 1 1 85 85 ASP N N 15 . 1 1 85 85 ASP H H 1 0.81 0.02 . . . . . . . . . . 5996 2 62 . 1 1 86 86 GLY N N 15 . 1 1 86 86 GLY H H 1 0.82 0.01 . . . . . . . . . . 5996 2 63 . 1 1 87 87 PHE N N 15 . 1 1 87 87 PHE H H 1 0.82 0.02 . . . . . . . . . . 5996 2 64 . 1 1 88 88 ASN N N 15 . 1 1 88 88 ASN H H 1 0.80 0.01 . . . . . . . . . . 5996 2 65 . 1 1 89 89 THR N N 15 . 1 1 89 89 THR H H 1 0.82 0.02 . . . . . . . . . . 5996 2 66 . 1 1 90 90 PHE N N 15 . 1 1 90 90 PHE H H 1 0.82 0.02 . . . . . . . . . . 5996 2 67 . 1 1 91 91 THR N N 15 . 1 1 91 91 THR H H 1 0.80 0.02 . . . . . . . . . . 5996 2 68 . 1 1 92 92 ILE N N 15 . 1 1 92 92 ILE H H 1 0.81 0.02 . . . . . . . . . . 5996 2 69 . 1 1 94 94 LYS N N 15 . 1 1 94 94 LYS H H 1 0.83 0.02 . . . . . . . . . . 5996 2 70 . 1 1 95 95 THR N N 15 . 1 1 95 95 THR H H 1 0.81 0.02 . . . . . . . . . . 5996 2 71 . 1 1 96 96 ASP N N 15 . 1 1 96 96 ASP H H 1 0.83 0.02 . . . . . . . . . . 5996 2 72 . 1 1 97 97 TYR N N 15 . 1 1 97 97 TYR H H 1 0.79 0.02 . . . . . . . . . . 5996 2 73 . 1 1 98 98 ASP N N 15 . 1 1 98 98 ASP H H 1 0.83 0.01 . . . . . . . . . . 5996 2 74 . 1 1 100 100 PHE N N 15 . 1 1 100 100 PHE H H 1 0.83 0.02 . . . . . . . . . . 5996 2 75 . 1 1 101 101 LEU N N 15 . 1 1 101 101 LEU H H 1 0.90 0.02 . . . . . . . . . . 5996 2 76 . 1 1 102 102 MET N N 15 . 1 1 102 102 MET H H 1 0.81 0.01 . . . . . . . . . . 5996 2 77 . 1 1 103 103 ALA N N 15 . 1 1 103 103 ALA H H 1 0.82 0.02 . . . . . . . . . . 5996 2 78 . 1 1 104 104 HIS N N 15 . 1 1 104 104 HIS H H 1 0.74 0.02 . . . . . . . . . . 5996 2 79 . 1 1 105 105 LEU N N 15 . 1 1 105 105 LEU H H 1 0.85 0.02 . . . . . . . . . . 5996 2 80 . 1 1 107 107 ASN N N 15 . 1 1 107 107 ASN H H 1 0.84 0.02 . . . . . . . . . . 5996 2 81 . 1 1 108 108 GLU N N 15 . 1 1 108 108 GLU H H 1 0.81 0.02 . . . . . . . . . . 5996 2 82 . 1 1 109 109 LYS N N 15 . 1 1 109 109 LYS H H 1 0.76 0.02 . . . . . . . . . . 5996 2 83 . 1 1 110 110 ASP N N 15 . 1 1 110 110 ASP H H 1 0.75 0.02 . . . . . . . . . . 5996 2 84 . 1 1 111 111 GLY N N 15 . 1 1 111 111 GLY H H 1 0.72 0.02 . . . . . . . . . . 5996 2 85 . 1 1 113 113 THR N N 15 . 1 1 113 113 THR H H 1 0.76 0.02 . . . . . . . . . . 5996 2 86 . 1 1 114 114 PHE N N 15 . 1 1 114 114 PHE H H 1 0.75 0.01 . . . . . . . . . . 5996 2 87 . 1 1 115 115 GLN N N 15 . 1 1 115 115 GLN H H 1 0.82 0.02 . . . . . . . . . . 5996 2 88 . 1 1 116 116 LEU N N 15 . 1 1 116 116 LEU H H 1 0.79 0.02 . . . . . . . . . . 5996 2 89 . 1 1 117 117 MET N N 15 . 1 1 117 117 MET H H 1 0.83 0.02 . . . . . . . . . . 5996 2 90 . 1 1 118 118 GLY N N 15 . 1 1 118 118 GLY H H 1 0.78 0.02 . . . . . . . . . . 5996 2 91 . 1 1 121 121 GLY N N 15 . 1 1 121 121 GLY H H 1 0.80 0.02 . . . . . . . . . . 5996 2 92 . 1 1 123 123 GLU N N 15 . 1 1 123 123 GLU H H 1 0.76 0.01 . . . . . . . . . . 5996 2 93 . 1 1 125 125 ASP N N 15 . 1 1 125 125 ASP H H 1 0.79 0.02 . . . . . . . . . . 5996 2 94 . 1 1 126 126 LEU N N 15 . 1 1 126 126 LEU H H 1 0.23 0.02 . . . . . . . . . . 5996 2 95 . 1 1 127 127 SER N N 15 . 1 1 127 127 SER H H 1 0.79 0.02 . . . . . . . . . . 5996 2 96 . 1 1 128 128 SER N N 15 . 1 1 128 128 SER H H 1 0.79 0.02 . . . . . . . . . . 5996 2 97 . 1 1 130 130 ILE N N 15 . 1 1 130 130 ILE H H 1 0.81 0.02 . . . . . . . . . . 5996 2 98 . 1 1 131 131 LYS N N 15 . 1 1 131 131 LYS H H 1 0.83 0.01 . . . . . . . . . . 5996 2 99 . 1 1 134 134 PHE N N 15 . 1 1 134 134 PHE H H 1 0.80 0.01 . . . . . . . . . . 5996 2 100 . 1 1 135 135 ALA N N 15 . 1 1 135 135 ALA H H 1 0.82 0.02 . . . . . . . . . . 5996 2 101 . 1 1 136 136 GLN N N 15 . 1 1 136 136 GLN H H 1 0.81 0.02 . . . . . . . . . . 5996 2 102 . 1 1 137 137 LEU N N 15 . 1 1 137 137 LEU H H 1 0.81 0.02 . . . . . . . . . . 5996 2 103 . 1 1 138 138 CYS N N 15 . 1 1 138 138 CYS H H 1 0.82 0.02 . . . . . . . . . . 5996 2 104 . 1 1 140 140 LYS N N 15 . 1 1 140 140 LYS H H 1 0.81 0.01 . . . . . . . . . . 5996 2 105 . 1 1 141 141 HIS N N 15 . 1 1 141 141 HIS H H 1 0.78 0.02 . . . . . . . . . . 5996 2 106 . 1 1 142 142 GLY N N 15 . 1 1 142 142 GLY H H 1 0.76 0.01 . . . . . . . . . . 5996 2 107 . 1 1 145 145 ARG N N 15 . 1 1 145 145 ARG H H 1 0.72 0.02 . . . . . . . . . . 5996 2 108 . 1 1 146 146 GLU N N 15 . 1 1 146 146 GLU H H 1 0.78 0.02 . . . . . . . . . . 5996 2 109 . 1 1 148 148 ILE N N 15 . 1 1 148 148 ILE H H 1 0.79 0.02 . . . . . . . . . . 5996 2 110 . 1 1 151 151 LEU N N 15 . 1 1 151 151 LEU H H 1 0.80 0.02 . . . . . . . . . . 5996 2 111 . 1 1 152 152 SER N N 15 . 1 1 152 152 SER H H 1 0.81 0.02 . . . . . . . . . . 5996 2 112 . 1 1 153 153 ASN N N 15 . 1 1 153 153 ASN H H 1 0.75 0.02 . . . . . . . . . . 5996 2 113 . 1 1 160 160 ALA N N 15 . 1 1 160 160 ALA H H 1 0.18 0.02 . . . . . . . . . . 5996 2 stop_ save_ save_293_600_bound_noe _Heteronucl_NOE_list.Sf_category heteronucl_NOEs _Heteronucl_NOE_list.Sf_framecode 293_600_bound_noe _Heteronucl_NOE_list.Entry_ID 5996 _Heteronucl_NOE_list.ID 3 _Heteronucl_NOE_list.Sample_condition_list_ID 3 _Heteronucl_NOE_list.Sample_condition_list_label $293K _Heteronucl_NOE_list.Spectrometer_frequency_1H 600 _Heteronucl_NOE_list.Heteronuclear_NOE_val_type 'relative intensities' _Heteronucl_NOE_list.NOE_ref_val . _Heteronucl_NOE_list.NOE_ref_description . _Heteronucl_NOE_list.Details . _Heteronucl_NOE_list.Text_data_format . _Heteronucl_NOE_list.Text_data . loop_ _Heteronucl_NOE_experiment.Experiment_ID _Heteronucl_NOE_experiment.Experiment_name _Heteronucl_NOE_experiment.Sample_ID _Heteronucl_NOE_experiment.Sample_label _Heteronucl_NOE_experiment.Sample_state _Heteronucl_NOE_experiment.Entry_ID _Heteronucl_NOE_experiment.Heteronucl_NOE_list_ID 3 '{1H}-15N NOE' 1 $sample_1 . 5996 3 stop_ loop_ _Heteronucl_NOE.ID _Heteronucl_NOE.Assembly_atom_ID_1 _Heteronucl_NOE.Entity_assembly_ID_1 _Heteronucl_NOE.Entity_ID_1 _Heteronucl_NOE.Comp_index_ID_1 _Heteronucl_NOE.Seq_ID_1 _Heteronucl_NOE.Comp_ID_1 _Heteronucl_NOE.Atom_ID_1 _Heteronucl_NOE.Atom_type_1 _Heteronucl_NOE.Atom_isotope_number_1 _Heteronucl_NOE.Assembly_atom_ID_2 _Heteronucl_NOE.Entity_assembly_ID_2 _Heteronucl_NOE.Entity_ID_2 _Heteronucl_NOE.Comp_index_ID_2 _Heteronucl_NOE.Seq_ID_2 _Heteronucl_NOE.Comp_ID_2 _Heteronucl_NOE.Atom_ID_2 _Heteronucl_NOE.Atom_type_2 _Heteronucl_NOE.Atom_isotope_number_2 _Heteronucl_NOE.Val _Heteronucl_NOE.Val_err _Heteronucl_NOE.Resonance_ID_1 _Heteronucl_NOE.Resonance_ID_2 _Heteronucl_NOE.Auth_entity_assembly_ID_1 _Heteronucl_NOE.Auth_seq_ID_1 _Heteronucl_NOE.Auth_comp_ID_1 _Heteronucl_NOE.Auth_atom_ID_1 _Heteronucl_NOE.Auth_entity_assembly_ID_2 _Heteronucl_NOE.Auth_seq_ID_2 _Heteronucl_NOE.Auth_comp_ID_2 _Heteronucl_NOE.Auth_atom_ID_2 _Heteronucl_NOE.Entry_ID _Heteronucl_NOE.Heteronucl_NOE_list_ID 1 . 1 1 3 3 ALA N N 15 . 1 1 3 3 ALA H H 1 0.68 0.02 . . . . . . . . . . 5996 3 2 . 1 1 5 5 SER N N 15 . 1 1 5 5 SER H H 1 0.81 0.02 . . . . . . . . . . 5996 3 3 . 1 1 6 6 THR N N 15 . 1 1 6 6 THR H H 1 0.80 0.02 . . . . . . . . . . 5996 3 4 . 1 1 7 7 GLY N N 15 . 1 1 7 7 GLY H H 1 0.63 0.02 . . . . . . . . . . 5996 3 5 . 1 1 10 10 PHE N N 15 . 1 1 10 10 PHE H H 1 0.54 0.02 . . . . . . . . . . 5996 3 6 . 1 1 11 11 ASN N N 15 . 1 1 11 11 ASN H H 1 0.80 0.02 . . . . . . . . . . 5996 3 7 . 1 1 12 12 VAL N N 15 . 1 1 12 12 VAL H H 1 0.81 0.02 . . . . . . . . . . 5996 3 8 . 1 1 13 13 GLU N N 15 . 1 1 13 13 GLU H H 1 0.78 0.02 . . . . . . . . . . 5996 3 9 . 1 1 15 15 ILE N N 15 . 1 1 15 15 ILE H H 1 0.78 0.02 . . . . . . . . . . 5996 3 10 . 1 1 16 16 ASN N N 15 . 1 1 16 16 ASN H H 1 0.83 0.02 . . . . . . . . . . 5996 3 11 . 1 1 18 18 GLU N N 15 . 1 1 18 18 GLU H H 1 0.79 0.02 . . . . . . . . . . 5996 3 12 . 1 1 19 19 TRP N N 15 . 1 1 19 19 TRP H H 1 0.83 0.02 . . . . . . . . . . 5996 3 13 . 1 1 20 20 HIS N N 15 . 1 1 20 20 HIS H H 1 0.82 0.02 . . . . . . . . . . 5996 3 14 . 1 1 22 22 ILE N N 15 . 1 1 22 22 ILE H H 1 0.79 0.02 . . . . . . . . . . 5996 3 15 . 1 1 23 23 ILE N N 15 . 1 1 23 23 ILE H H 1 0.82 0.04 . . . . . . . . . . 5996 3 16 . 1 1 26 26 SER N N 15 . 1 1 26 26 SER H H 1 0.81 0.02 . . . . . . . . . . 5996 3 17 . 1 1 27 27 ASP N N 15 . 1 1 27 27 ASP H H 1 0.77 0.02 . . . . . . . . . . 5996 3 18 . 1 1 29 29 ARG N N 15 . 1 1 29 29 ARG H H 1 0.80 0.02 . . . . . . . . . . 5996 3 19 . 1 1 30 30 GLU N N 15 . 1 1 30 30 GLU H H 1 0.78 0.02 . . . . . . . . . . 5996 3 20 . 1 1 31 31 LYS N N 15 . 1 1 31 31 LYS H H 1 0.81 0.02 . . . . . . . . . . 5996 3 21 . 1 1 32 32 ILE N N 15 . 1 1 32 32 ILE H H 1 0.84 0.02 . . . . . . . . . . 5996 3 22 . 1 1 33 33 GLU N N 15 . 1 1 33 33 GLU H H 1 0.81 0.02 . . . . . . . . . . 5996 3 23 . 1 1 36 36 GLY N N 15 . 1 1 36 36 GLY H H 1 0.82 0.02 . . . . . . . . . . 5996 3 24 . 1 1 37 37 ASN N N 15 . 1 1 37 37 ASN H H 1 0.80 0.02 . . . . . . . . . . 5996 3 25 . 1 1 39 39 ARG N N 15 . 1 1 39 39 ARG H H 1 0.80 0.01 . . . . . . . . . . 5996 3 26 . 1 1 40 40 LEU N N 15 . 1 1 40 40 LEU H H 1 0.83 0.02 . . . . . . . . . . 5996 3 27 . 1 1 43 43 GLU N N 15 . 1 1 43 43 GLU H H 1 0.81 0.01 . . . . . . . . . . 5996 3 28 . 1 1 45 45 ILE N N 15 . 1 1 45 45 ILE H H 1 0.81 0.02 . . . . . . . . . . 5996 3 29 . 1 1 46 46 HIS N N 15 . 1 1 46 46 HIS H H 1 0.80 0.02 . . . . . . . . . . 5996 3 30 . 1 1 47 47 VAL N N 15 . 1 1 47 47 VAL H H 1 0.76 0.02 . . . . . . . . . . 5996 3 31 . 1 1 48 48 LEU N N 15 . 1 1 48 48 LEU H H 1 0.80 0.04 . . . . . . . . . . 5996 3 32 . 1 1 50 50 ASN N N 15 . 1 1 50 50 ASN H H 1 0.67 0.02 . . . . . . . . . . 5996 3 33 . 1 1 51 51 SER N N 15 . 1 1 51 51 SER H H 1 0.73 0.02 . . . . . . . . . . 5996 3 34 . 1 1 52 52 LEU N N 15 . 1 1 52 52 LEU H H 1 0.80 0.02 . . . . . . . . . . 5996 3 35 . 1 1 53 53 VAL N N 15 . 1 1 53 53 VAL H H 1 0.80 0.02 . . . . . . . . . . 5996 3 36 . 1 1 54 54 LEU N N 15 . 1 1 54 54 LEU H H 1 0.80 0.02 . . . . . . . . . . 5996 3 37 . 1 1 55 55 LYS N N 15 . 1 1 55 55 LYS H H 1 0.74 0.02 . . . . . . . . . . 5996 3 38 . 1 1 57 57 HIS N N 15 . 1 1 57 57 HIS H H 1 0.81 0.01 . . . . . . . . . . 5996 3 39 . 1 1 60 60 ARG N N 15 . 1 1 60 60 ARG H H 1 0.69 0.02 . . . . . . . . . . 5996 3 40 . 1 1 61 61 ASP N N 15 . 1 1 61 61 ASP H H 1 0.72 0.02 . . . . . . . . . . 5996 3 41 . 1 1 62 62 GLU N N 15 . 1 1 62 62 GLU H H 1 0.68 0.02 . . . . . . . . . . 5996 3 42 . 1 1 64 64 CYS N N 15 . 1 1 64 64 CYS H H 1 0.70 0.02 . . . . . . . . . . 5996 3 43 . 1 1 66 66 GLU N N 15 . 1 1 66 66 GLU H H 1 0.70 0.02 . . . . . . . . . . 5996 3 44 . 1 1 67 67 LEU N N 15 . 1 1 67 67 LEU H H 1 0.76 0.01 . . . . . . . . . . 5996 3 45 . 1 1 68 68 SER N N 15 . 1 1 68 68 SER H H 1 0.76 0.01 . . . . . . . . . . 5996 3 46 . 1 1 69 69 MET N N 15 . 1 1 69 69 MET H H 1 0.79 0.02 . . . . . . . . . . 5996 3 47 . 1 1 71 71 ALA N N 15 . 1 1 71 71 ALA H H 1 0.79 0.01 . . . . . . . . . . 5996 3 48 . 1 1 72 72 ASP N N 15 . 1 1 72 72 ASP H H 1 0.78 0.02 . . . . . . . . . . 5996 3 49 . 1 1 74 74 THR N N 15 . 1 1 74 74 THR H H 1 0.73 0.01 . . . . . . . . . . 5996 3 50 . 1 1 75 75 GLU N N 15 . 1 1 75 75 GLU H H 1 0.67 0.01 . . . . . . . . . . 5996 3 51 . 1 1 76 76 LYS N N 15 . 1 1 76 76 LYS H H 1 0.81 0.02 . . . . . . . . . . 5996 3 52 . 1 1 77 77 ALA N N 15 . 1 1 77 77 ALA H H 1 0.70 0.02 . . . . . . . . . . 5996 3 53 . 1 1 78 78 GLY N N 15 . 1 1 78 78 GLY H H 1 0.68 0.02 . . . . . . . . . . 5996 3 54 . 1 1 79 79 GLU N N 15 . 1 1 79 79 GLU H H 1 0.80 0.01 . . . . . . . . . . 5996 3 55 . 1 1 80 80 TYR N N 15 . 1 1 80 80 TYR H H 1 0.81 0.02 . . . . . . . . . . 5996 3 56 . 1 1 81 81 SER N N 15 . 1 1 81 81 SER H H 1 0.80 0.02 . . . . . . . . . . 5996 3 57 . 1 1 82 82 VAL N N 15 . 1 1 82 82 VAL H H 1 0.82 0.02 . . . . . . . . . . 5996 3 58 . 1 1 83 83 THR N N 15 . 1 1 83 83 THR H H 1 0.79 0.02 . . . . . . . . . . 5996 3 59 . 1 1 84 84 TYR N N 15 . 1 1 84 84 TYR H H 1 0.80 0.02 . . . . . . . . . . 5996 3 60 . 1 1 86 86 GLY N N 15 . 1 1 86 86 GLY H H 1 0.82 0.01 . . . . . . . . . . 5996 3 61 . 1 1 87 87 PHE N N 15 . 1 1 87 87 PHE H H 1 0.80 0.02 . . . . . . . . . . 5996 3 62 . 1 1 88 88 ASN N N 15 . 1 1 88 88 ASN H H 1 0.82 0.01 . . . . . . . . . . 5996 3 63 . 1 1 89 89 THR N N 15 . 1 1 89 89 THR H H 1 0.81 0.02 . . . . . . . . . . 5996 3 64 . 1 1 90 90 PHE N N 15 . 1 1 90 90 PHE H H 1 0.81 0.01 . . . . . . . . . . 5996 3 65 . 1 1 91 91 THR N N 15 . 1 1 91 91 THR H H 1 0.78 0.02 . . . . . . . . . . 5996 3 66 . 1 1 92 92 ILE N N 15 . 1 1 92 92 ILE H H 1 0.79 0.02 . . . . . . . . . . 5996 3 67 . 1 1 94 94 LYS N N 15 . 1 1 94 94 LYS H H 1 0.81 0.02 . . . . . . . . . . 5996 3 68 . 1 1 95 95 THR N N 15 . 1 1 95 95 THR H H 1 0.81 0.02 . . . . . . . . . . 5996 3 69 . 1 1 96 96 ASP N N 15 . 1 1 96 96 ASP H H 1 0.82 0.02 . . . . . . . . . . 5996 3 70 . 1 1 97 97 TYR N N 15 . 1 1 97 97 TYR H H 1 0.79 0.02 . . . . . . . . . . 5996 3 71 . 1 1 98 98 ASP N N 15 . 1 1 98 98 ASP H H 1 0.83 0.02 . . . . . . . . . . 5996 3 72 . 1 1 101 101 LEU N N 15 . 1 1 101 101 LEU H H 1 0.83 0.02 . . . . . . . . . . 5996 3 73 . 1 1 102 102 MET N N 15 . 1 1 102 102 MET H H 1 0.84 0.01 . . . . . . . . . . 5996 3 74 . 1 1 103 103 ALA N N 15 . 1 1 103 103 ALA H H 1 0.82 0.02 . . . . . . . . . . 5996 3 75 . 1 1 104 104 HIS N N 15 . 1 1 104 104 HIS H H 1 0.74 0.02 . . . . . . . . . . 5996 3 76 . 1 1 105 105 LEU N N 15 . 1 1 105 105 LEU H H 1 0.85 0.01 . . . . . . . . . . 5996 3 77 . 1 1 108 108 GLU N N 15 . 1 1 108 108 GLU H H 1 0.80 0.02 . . . . . . . . . . 5996 3 78 . 1 1 109 109 LYS N N 15 . 1 1 109 109 LYS H H 1 0.76 0.02 . . . . . . . . . . 5996 3 79 . 1 1 110 110 ASP N N 15 . 1 1 110 110 ASP H H 1 0.77 0.02 . . . . . . . . . . 5996 3 80 . 1 1 111 111 GLY N N 15 . 1 1 111 111 GLY H H 1 0.72 0.02 . . . . . . . . . . 5996 3 81 . 1 1 115 115 GLN N N 15 . 1 1 115 115 GLN H H 1 0.81 0.02 . . . . . . . . . . 5996 3 82 . 1 1 116 116 LEU N N 15 . 1 1 116 116 LEU H H 1 0.78 0.02 . . . . . . . . . . 5996 3 83 . 1 1 117 117 MET N N 15 . 1 1 117 117 MET H H 1 0.80 0.02 . . . . . . . . . . 5996 3 84 . 1 1 118 118 GLY N N 15 . 1 1 118 118 GLY H H 1 0.81 0.02 . . . . . . . . . . 5996 3 85 . 1 1 119 119 LEU N N 15 . 1 1 119 119 LEU H H 1 0.81 0.02 . . . . . . . . . . 5996 3 86 . 1 1 120 120 TYR N N 15 . 1 1 120 120 TYR H H 1 0.84 0.01 . . . . . . . . . . 5996 3 87 . 1 1 121 121 GLY N N 15 . 1 1 121 121 GLY H H 1 0.82 0.02 . . . . . . . . . . 5996 3 88 . 1 1 123 123 GLU N N 15 . 1 1 123 123 GLU H H 1 0.78 0.02 . . . . . . . . . . 5996 3 89 . 1 1 125 125 ASP N N 15 . 1 1 125 125 ASP H H 1 0.79 0.02 . . . . . . . . . . 5996 3 90 . 1 1 128 128 SER N N 15 . 1 1 128 128 SER H H 1 0.82 0.02 . . . . . . . . . . 5996 3 91 . 1 1 129 129 ASP N N 15 . 1 1 129 129 ASP H H 1 0.83 0.02 . . . . . . . . . . 5996 3 92 . 1 1 130 130 ILE N N 15 . 1 1 130 130 ILE H H 1 0.79 0.01 . . . . . . . . . . 5996 3 93 . 1 1 131 131 LYS N N 15 . 1 1 131 131 LYS H H 1 0.82 0.02 . . . . . . . . . . 5996 3 94 . 1 1 134 134 PHE N N 15 . 1 1 134 134 PHE H H 1 0.78 0.02 . . . . . . . . . . 5996 3 95 . 1 1 135 135 ALA N N 15 . 1 1 135 135 ALA H H 1 0.80 0.02 . . . . . . . . . . 5996 3 96 . 1 1 136 136 GLN N N 15 . 1 1 136 136 GLN H H 1 0.82 0.02 . . . . . . . . . . 5996 3 97 . 1 1 137 137 LEU N N 15 . 1 1 137 137 LEU H H 1 0.82 0.02 . . . . . . . . . . 5996 3 98 . 1 1 138 138 CYS N N 15 . 1 1 138 138 CYS H H 1 0.82 0.01 . . . . . . . . . . 5996 3 99 . 1 1 141 141 HIS N N 15 . 1 1 141 141 HIS H H 1 0.78 0.01 . . . . . . . . . . 5996 3 100 . 1 1 142 142 GLY N N 15 . 1 1 142 142 GLY H H 1 0.76 0.02 . . . . . . . . . . 5996 3 101 . 1 1 143 143 ILE N N 15 . 1 1 143 143 ILE H H 1 0.81 0.02 . . . . . . . . . . 5996 3 102 . 1 1 144 144 LEU N N 15 . 1 1 144 144 LEU H H 1 0.67 0.02 . . . . . . . . . . 5996 3 103 . 1 1 145 145 ARG N N 15 . 1 1 145 145 ARG H H 1 0.70 0.02 . . . . . . . . . . 5996 3 104 . 1 1 148 148 ILE N N 15 . 1 1 148 148 ILE H H 1 0.78 0.01 . . . . . . . . . . 5996 3 105 . 1 1 151 151 LEU N N 15 . 1 1 151 151 LEU H H 1 0.78 0.02 . . . . . . . . . . 5996 3 106 . 1 1 156 156 ARG N N 15 . 1 1 156 156 ARG H H 1 0.72 0.01 . . . . . . . . . . 5996 3 107 . 1 1 160 160 ALA N N 15 . 1 1 160 160 ALA H H 1 0.09 0.02 . . . . . . . . . . 5996 3 108 . 1 1 162 162 GLU N N 15 . 1 1 162 162 GLU H H 1 -0.49 0.02 . . . . . . . . . . 5996 3 stop_ save_ save_298_600_bound_noe _Heteronucl_NOE_list.Sf_category heteronucl_NOEs _Heteronucl_NOE_list.Sf_framecode 298_600_bound_noe _Heteronucl_NOE_list.Entry_ID 5996 _Heteronucl_NOE_list.ID 4 _Heteronucl_NOE_list.Sample_condition_list_ID 4 _Heteronucl_NOE_list.Sample_condition_list_label $298K _Heteronucl_NOE_list.Spectrometer_frequency_1H 600 _Heteronucl_NOE_list.Heteronuclear_NOE_val_type 'relative intensities' _Heteronucl_NOE_list.NOE_ref_val . _Heteronucl_NOE_list.NOE_ref_description . _Heteronucl_NOE_list.Details . _Heteronucl_NOE_list.Text_data_format . _Heteronucl_NOE_list.Text_data . loop_ _Heteronucl_NOE_experiment.Experiment_ID _Heteronucl_NOE_experiment.Experiment_name _Heteronucl_NOE_experiment.Sample_ID _Heteronucl_NOE_experiment.Sample_label _Heteronucl_NOE_experiment.Sample_state _Heteronucl_NOE_experiment.Entry_ID _Heteronucl_NOE_experiment.Heteronucl_NOE_list_ID 3 '{1H}-15N NOE' 1 $sample_1 . 5996 4 stop_ loop_ _Heteronucl_NOE.ID _Heteronucl_NOE.Assembly_atom_ID_1 _Heteronucl_NOE.Entity_assembly_ID_1 _Heteronucl_NOE.Entity_ID_1 _Heteronucl_NOE.Comp_index_ID_1 _Heteronucl_NOE.Seq_ID_1 _Heteronucl_NOE.Comp_ID_1 _Heteronucl_NOE.Atom_ID_1 _Heteronucl_NOE.Atom_type_1 _Heteronucl_NOE.Atom_isotope_number_1 _Heteronucl_NOE.Assembly_atom_ID_2 _Heteronucl_NOE.Entity_assembly_ID_2 _Heteronucl_NOE.Entity_ID_2 _Heteronucl_NOE.Comp_index_ID_2 _Heteronucl_NOE.Seq_ID_2 _Heteronucl_NOE.Comp_ID_2 _Heteronucl_NOE.Atom_ID_2 _Heteronucl_NOE.Atom_type_2 _Heteronucl_NOE.Atom_isotope_number_2 _Heteronucl_NOE.Val _Heteronucl_NOE.Val_err _Heteronucl_NOE.Resonance_ID_1 _Heteronucl_NOE.Resonance_ID_2 _Heteronucl_NOE.Auth_entity_assembly_ID_1 _Heteronucl_NOE.Auth_seq_ID_1 _Heteronucl_NOE.Auth_comp_ID_1 _Heteronucl_NOE.Auth_atom_ID_1 _Heteronucl_NOE.Auth_entity_assembly_ID_2 _Heteronucl_NOE.Auth_seq_ID_2 _Heteronucl_NOE.Auth_comp_ID_2 _Heteronucl_NOE.Auth_atom_ID_2 _Heteronucl_NOE.Entry_ID _Heteronucl_NOE.Heteronucl_NOE_list_ID 1 . 1 1 3 3 ALA N N 15 . 1 1 3 3 ALA H H 1 0.66 0.01 . . . . . . . . . . 5996 4 2 . 1 1 4 4 SER N N 15 . 1 1 4 4 SER H H 1 0.74 0.01 . . . . . . . . . . 5996 4 3 . 1 1 5 5 SER N N 15 . 1 1 5 5 SER H H 1 0.79 0.01 . . . . . . . . . . 5996 4 4 . 1 1 6 6 THR N N 15 . 1 1 6 6 THR H H 1 0.80 0.01 . . . . . . . . . . 5996 4 5 . 1 1 7 7 GLY N N 15 . 1 1 7 7 GLY H H 1 0.60 0.01 . . . . . . . . . . 5996 4 6 . 1 1 10 10 PHE N N 15 . 1 1 10 10 PHE H H 1 0.56 0.01 . . . . . . . . . . 5996 4 7 . 1 1 11 11 ASN N N 15 . 1 1 11 11 ASN H H 1 0.79 0.01 . . . . . . . . . . 5996 4 8 . 1 1 12 12 VAL N N 15 . 1 1 12 12 VAL H H 1 0.80 0.01 . . . . . . . . . . 5996 4 9 . 1 1 13 13 GLU N N 15 . 1 1 13 13 GLU H H 1 0.78 0.01 . . . . . . . . . . 5996 4 10 . 1 1 15 15 ILE N N 15 . 1 1 15 15 ILE H H 1 0.81 0.01 . . . . . . . . . . 5996 4 11 . 1 1 16 16 ASN N N 15 . 1 1 16 16 ASN H H 1 0.81 0.01 . . . . . . . . . . 5996 4 12 . 1 1 17 17 GLY N N 15 . 1 1 17 17 GLY H H 1 0.82 0.01 . . . . . . . . . . 5996 4 13 . 1 1 18 18 GLU N N 15 . 1 1 18 18 GLU H H 1 0.72 0.01 . . . . . . . . . . 5996 4 14 . 1 1 19 19 TRP N N 15 . 1 1 19 19 TRP H H 1 0.80 0.01 . . . . . . . . . . 5996 4 15 . 1 1 20 20 HIS N N 15 . 1 1 20 20 HIS H H 1 0.78 0.01 . . . . . . . . . . 5996 4 16 . 1 1 21 21 THR N N 15 . 1 1 21 21 THR H H 1 0.79 0.01 . . . . . . . . . . 5996 4 17 . 1 1 22 22 ILE N N 15 . 1 1 22 22 ILE H H 1 0.82 0.01 . . . . . . . . . . 5996 4 18 . 1 1 23 23 ILE N N 15 . 1 1 23 23 ILE H H 1 0.81 0.01 . . . . . . . . . . 5996 4 19 . 1 1 26 26 SER N N 15 . 1 1 26 26 SER H H 1 0.80 0.01 . . . . . . . . . . 5996 4 20 . 1 1 27 27 ASP N N 15 . 1 1 27 27 ASP H H 1 0.80 0.01 . . . . . . . . . . 5996 4 21 . 1 1 29 29 ARG N N 15 . 1 1 29 29 ARG H H 1 0.78 0.01 . . . . . . . . . . 5996 4 22 . 1 1 30 30 GLU N N 15 . 1 1 30 30 GLU H H 1 0.79 0.01 . . . . . . . . . . 5996 4 23 . 1 1 31 31 LYS N N 15 . 1 1 31 31 LYS H H 1 0.81 0.01 . . . . . . . . . . 5996 4 24 . 1 1 32 32 ILE N N 15 . 1 1 32 32 ILE H H 1 0.81 0.01 . . . . . . . . . . 5996 4 25 . 1 1 33 33 GLU N N 15 . 1 1 33 33 GLU H H 1 0.80 0.01 . . . . . . . . . . 5996 4 26 . 1 1 35 35 ASN N N 15 . 1 1 35 35 ASN H H 1 0.68 0.01 . . . . . . . . . . 5996 4 27 . 1 1 36 36 GLY N N 15 . 1 1 36 36 GLY H H 1 0.79 0.01 . . . . . . . . . . 5996 4 28 . 1 1 37 37 ASN N N 15 . 1 1 37 37 ASN H H 1 0.80 0.01 . . . . . . . . . . 5996 4 29 . 1 1 39 39 ARG N N 15 . 1 1 39 39 ARG H H 1 0.83 0.01 . . . . . . . . . . 5996 4 30 . 1 1 40 40 LEU N N 15 . 1 1 40 40 LEU H H 1 0.78 0.01 . . . . . . . . . . 5996 4 31 . 1 1 42 42 LEU N N 15 . 1 1 42 42 LEU H H 1 0.75 0.01 . . . . . . . . . . 5996 4 32 . 1 1 43 43 GLU N N 15 . 1 1 43 43 GLU H H 1 0.77 0.01 . . . . . . . . . . 5996 4 33 . 1 1 45 45 ILE N N 15 . 1 1 45 45 ILE H H 1 0.80 0.01 . . . . . . . . . . 5996 4 34 . 1 1 46 46 HIS N N 15 . 1 1 46 46 HIS H H 1 0.80 0.01 . . . . . . . . . . 5996 4 35 . 1 1 47 47 VAL N N 15 . 1 1 47 47 VAL H H 1 0.79 0.01 . . . . . . . . . . 5996 4 36 . 1 1 48 48 LEU N N 15 . 1 1 48 48 LEU H H 1 0.79 0.01 . . . . . . . . . . 5996 4 37 . 1 1 50 50 ASN N N 15 . 1 1 50 50 ASN H H 1 0.69 0.01 . . . . . . . . . . 5996 4 38 . 1 1 51 51 SER N N 15 . 1 1 51 51 SER H H 1 0.72 0.01 . . . . . . . . . . 5996 4 39 . 1 1 52 52 LEU N N 15 . 1 1 52 52 LEU H H 1 0.78 0.01 . . . . . . . . . . 5996 4 40 . 1 1 53 53 VAL N N 15 . 1 1 53 53 VAL H H 1 0.78 0.01 . . . . . . . . . . 5996 4 41 . 1 1 54 54 LEU N N 15 . 1 1 54 54 LEU H H 1 0.82 0.01 . . . . . . . . . . 5996 4 42 . 1 1 55 55 LYS N N 15 . 1 1 55 55 LYS H H 1 0.72 0.01 . . . . . . . . . . 5996 4 43 . 1 1 57 57 HIS N N 15 . 1 1 57 57 HIS H H 1 0.80 0.01 . . . . . . . . . . 5996 4 44 . 1 1 58 58 THR N N 15 . 1 1 58 58 THR H H 1 0.83 0.01 . . . . . . . . . . 5996 4 45 . 1 1 60 60 ARG N N 15 . 1 1 60 60 ARG H H 1 0.70 0.01 . . . . . . . . . . 5996 4 46 . 1 1 61 61 ASP N N 15 . 1 1 61 61 ASP H H 1 0.70 0.01 . . . . . . . . . . 5996 4 47 . 1 1 62 62 GLU N N 15 . 1 1 62 62 GLU H H 1 0.70 0.01 . . . . . . . . . . 5996 4 48 . 1 1 64 64 CYS N N 15 . 1 1 64 64 CYS H H 1 0.68 0.01 . . . . . . . . . . 5996 4 49 . 1 1 65 65 SER N N 15 . 1 1 65 65 SER H H 1 0.72 0.01 . . . . . . . . . . 5996 4 50 . 1 1 66 66 GLU N N 15 . 1 1 66 66 GLU H H 1 0.71 0.01 . . . . . . . . . . 5996 4 51 . 1 1 67 67 LEU N N 15 . 1 1 67 67 LEU H H 1 0.76 0.01 . . . . . . . . . . 5996 4 52 . 1 1 68 68 SER N N 15 . 1 1 68 68 SER H H 1 0.73 0.01 . . . . . . . . . . 5996 4 53 . 1 1 69 69 MET N N 15 . 1 1 69 69 MET H H 1 0.79 0.01 . . . . . . . . . . 5996 4 54 . 1 1 71 71 ALA N N 15 . 1 1 71 71 ALA H H 1 0.81 0.01 . . . . . . . . . . 5996 4 55 . 1 1 72 72 ASP N N 15 . 1 1 72 72 ASP H H 1 0.78 0.01 . . . . . . . . . . 5996 4 56 . 1 1 74 74 THR N N 15 . 1 1 74 74 THR H H 1 0.73 0.01 . . . . . . . . . . 5996 4 57 . 1 1 75 75 GLU N N 15 . 1 1 75 75 GLU H H 1 0.66 0.01 . . . . . . . . . . 5996 4 58 . 1 1 76 76 LYS N N 15 . 1 1 76 76 LYS H H 1 0.77 0.01 . . . . . . . . . . 5996 4 59 . 1 1 77 77 ALA N N 15 . 1 1 77 77 ALA H H 1 0.67 0.01 . . . . . . . . . . 5996 4 60 . 1 1 78 78 GLY N N 15 . 1 1 78 78 GLY H H 1 0.70 0.01 . . . . . . . . . . 5996 4 61 . 1 1 79 79 GLU N N 15 . 1 1 79 79 GLU H H 1 0.78 0.01 . . . . . . . . . . 5996 4 62 . 1 1 80 80 TYR N N 15 . 1 1 80 80 TYR H H 1 0.81 0.01 . . . . . . . . . . 5996 4 63 . 1 1 81 81 SER N N 15 . 1 1 81 81 SER H H 1 0.80 0.01 . . . . . . . . . . 5996 4 64 . 1 1 82 82 VAL N N 15 . 1 1 82 82 VAL H H 1 0.79 0.01 . . . . . . . . . . 5996 4 65 . 1 1 83 83 THR N N 15 . 1 1 83 83 THR H H 1 0.77 0.01 . . . . . . . . . . 5996 4 66 . 1 1 84 84 TYR N N 15 . 1 1 84 84 TYR H H 1 0.81 0.01 . . . . . . . . . . 5996 4 67 . 1 1 85 85 ASP N N 15 . 1 1 85 85 ASP H H 1 0.79 0.01 . . . . . . . . . . 5996 4 68 . 1 1 86 86 GLY N N 15 . 1 1 86 86 GLY H H 1 0.81 0.04 . . . . . . . . . . 5996 4 69 . 1 1 87 87 PHE N N 15 . 1 1 87 87 PHE H H 1 0.82 0.01 . . . . . . . . . . 5996 4 70 . 1 1 88 88 ASN N N 15 . 1 1 88 88 ASN H H 1 0.79 0.01 . . . . . . . . . . 5996 4 71 . 1 1 89 89 THR N N 15 . 1 1 89 89 THR H H 1 0.81 0.01 . . . . . . . . . . 5996 4 72 . 1 1 90 90 PHE N N 15 . 1 1 90 90 PHE H H 1 0.79 0.01 . . . . . . . . . . 5996 4 73 . 1 1 91 91 THR N N 15 . 1 1 91 91 THR H H 1 0.82 0.01 . . . . . . . . . . 5996 4 74 . 1 1 92 92 ILE N N 15 . 1 1 92 92 ILE H H 1 0.81 0.01 . . . . . . . . . . 5996 4 75 . 1 1 94 94 LYS N N 15 . 1 1 94 94 LYS H H 1 0.81 0.01 . . . . . . . . . . 5996 4 76 . 1 1 95 95 THR N N 15 . 1 1 95 95 THR H H 1 0.80 0.01 . . . . . . . . . . 5996 4 77 . 1 1 96 96 ASP N N 15 . 1 1 96 96 ASP H H 1 0.82 0.01 . . . . . . . . . . 5996 4 78 . 1 1 97 97 TYR N N 15 . 1 1 97 97 TYR H H 1 0.83 0.01 . . . . . . . . . . 5996 4 79 . 1 1 99 99 ASN N N 15 . 1 1 99 99 ASN H H 1 0.82 0.01 . . . . . . . . . . 5996 4 80 . 1 1 100 100 PHE N N 15 . 1 1 100 100 PHE H H 1 0.82 0.01 . . . . . . . . . . 5996 4 81 . 1 1 101 101 LEU N N 15 . 1 1 101 101 LEU H H 1 0.81 0.04 . . . . . . . . . . 5996 4 82 . 1 1 103 103 ALA N N 15 . 1 1 103 103 ALA H H 1 0.83 0.01 . . . . . . . . . . 5996 4 83 . 1 1 104 104 HIS N N 15 . 1 1 104 104 HIS H H 1 0.72 0.01 . . . . . . . . . . 5996 4 84 . 1 1 105 105 LEU N N 15 . 1 1 105 105 LEU H H 1 0.83 0.01 . . . . . . . . . . 5996 4 85 . 1 1 107 107 ASN N N 15 . 1 1 107 107 ASN H H 1 0.81 0.01 . . . . . . . . . . 5996 4 86 . 1 1 108 108 GLU N N 15 . 1 1 108 108 GLU H H 1 0.82 0.01 . . . . . . . . . . 5996 4 87 . 1 1 109 109 LYS N N 15 . 1 1 109 109 LYS H H 1 0.77 0.01 . . . . . . . . . . 5996 4 88 . 1 1 110 110 ASP N N 15 . 1 1 110 110 ASP H H 1 0.75 0.01 . . . . . . . . . . 5996 4 89 . 1 1 111 111 GLY N N 15 . 1 1 111 111 GLY H H 1 0.71 0.01 . . . . . . . . . . 5996 4 90 . 1 1 113 113 THR N N 15 . 1 1 113 113 THR H H 1 0.74 0.01 . . . . . . . . . . 5996 4 91 . 1 1 114 114 PHE N N 15 . 1 1 114 114 PHE H H 1 0.79 0.01 . . . . . . . . . . 5996 4 92 . 1 1 115 115 GLN N N 15 . 1 1 115 115 GLN H H 1 0.81 0.01 . . . . . . . . . . 5996 4 93 . 1 1 116 116 LEU N N 15 . 1 1 116 116 LEU H H 1 0.81 0.02 . . . . . . . . . . 5996 4 94 . 1 1 117 117 MET N N 15 . 1 1 117 117 MET H H 1 0.83 0.01 . . . . . . . . . . 5996 4 95 . 1 1 118 118 GLY N N 15 . 1 1 118 118 GLY H H 1 0.80 0.01 . . . . . . . . . . 5996 4 96 . 1 1 119 119 LEU N N 15 . 1 1 119 119 LEU H H 1 0.82 0.01 . . . . . . . . . . 5996 4 97 . 1 1 121 121 GLY N N 15 . 1 1 121 121 GLY H H 1 0.81 0.01 . . . . . . . . . . 5996 4 98 . 1 1 123 123 GLU N N 15 . 1 1 123 123 GLU H H 1 0.79 0.01 . . . . . . . . . . 5996 4 99 . 1 1 125 125 ASP N N 15 . 1 1 125 125 ASP H H 1 0.78 0.01 . . . . . . . . . . 5996 4 100 . 1 1 126 126 LEU N N 15 . 1 1 126 126 LEU H H 1 0.79 0.01 . . . . . . . . . . 5996 4 101 . 1 1 127 127 SER N N 15 . 1 1 127 127 SER H H 1 0.77 0.01 . . . . . . . . . . 5996 4 102 . 1 1 128 128 SER N N 15 . 1 1 128 128 SER H H 1 0.80 0.01 . . . . . . . . . . 5996 4 103 . 1 1 130 130 ILE N N 15 . 1 1 130 130 ILE H H 1 0.78 0.01 . . . . . . . . . . 5996 4 104 . 1 1 131 131 LYS N N 15 . 1 1 131 131 LYS H H 1 0.80 0.01 . . . . . . . . . . 5996 4 105 . 1 1 133 133 ARG N N 15 . 1 1 133 133 ARG H H 1 0.82 0.01 . . . . . . . . . . 5996 4 106 . 1 1 134 134 PHE N N 15 . 1 1 134 134 PHE H H 1 0.78 0.01 . . . . . . . . . . 5996 4 107 . 1 1 135 135 ALA N N 15 . 1 1 135 135 ALA H H 1 0.81 0.01 . . . . . . . . . . 5996 4 108 . 1 1 136 136 GLN N N 15 . 1 1 136 136 GLN H H 1 0.80 0.01 . . . . . . . . . . 5996 4 109 . 1 1 137 137 LEU N N 15 . 1 1 137 137 LEU H H 1 0.79 0.01 . . . . . . . . . . 5996 4 110 . 1 1 138 138 CYS N N 15 . 1 1 138 138 CYS H H 1 0.81 0.02 . . . . . . . . . . 5996 4 111 . 1 1 141 141 HIS N N 15 . 1 1 141 141 HIS H H 1 0.78 0.01 . . . . . . . . . . 5996 4 112 . 1 1 142 142 GLY N N 15 . 1 1 142 142 GLY H H 1 0.79 0.03 . . . . . . . . . . 5996 4 113 . 1 1 143 143 ILE N N 15 . 1 1 143 143 ILE H H 1 0.77 0.01 . . . . . . . . . . 5996 4 114 . 1 1 144 144 LEU N N 15 . 1 1 144 144 LEU H H 1 0.67 0.01 . . . . . . . . . . 5996 4 115 . 1 1 145 145 ARG N N 15 . 1 1 145 145 ARG H H 1 0.72 0.01 . . . . . . . . . . 5996 4 116 . 1 1 146 146 GLU N N 15 . 1 1 146 146 GLU H H 1 0.77 0.01 . . . . . . . . . . 5996 4 117 . 1 1 148 148 ILE N N 15 . 1 1 148 148 ILE H H 1 0.81 0.01 . . . . . . . . . . 5996 4 118 . 1 1 149 149 ILE N N 15 . 1 1 149 149 ILE H H 1 0.79 0.01 . . . . . . . . . . 5996 4 119 . 1 1 150 150 ASP N N 15 . 1 1 150 150 ASP H H 1 0.79 0.01 . . . . . . . . . . 5996 4 120 . 1 1 151 151 LEU N N 15 . 1 1 151 151 LEU H H 1 0.79 0.01 . . . . . . . . . . 5996 4 121 . 1 1 152 152 SER N N 15 . 1 1 152 152 SER H H 1 0.81 0.01 . . . . . . . . . . 5996 4 122 . 1 1 153 153 ASN N N 15 . 1 1 153 153 ASN H H 1 0.78 0.01 . . . . . . . . . . 5996 4 123 . 1 1 160 160 ALA N N 15 . 1 1 160 160 ALA H H 1 0.08 0.01 . . . . . . . . . . 5996 4 124 . 1 1 162 162 GLU N N 15 . 1 1 162 162 GLU H H 1 -0.52 0.01 . . . . . . . . . . 5996 4 stop_ save_ save_303_600_bound_noe _Heteronucl_NOE_list.Sf_category heteronucl_NOEs _Heteronucl_NOE_list.Sf_framecode 303_600_bound_noe _Heteronucl_NOE_list.Entry_ID 5996 _Heteronucl_NOE_list.ID 5 _Heteronucl_NOE_list.Sample_condition_list_ID 5 _Heteronucl_NOE_list.Sample_condition_list_label $303K _Heteronucl_NOE_list.Spectrometer_frequency_1H 600 _Heteronucl_NOE_list.Heteronuclear_NOE_val_type 'relative intensities' _Heteronucl_NOE_list.NOE_ref_val . _Heteronucl_NOE_list.NOE_ref_description . _Heteronucl_NOE_list.Details . _Heteronucl_NOE_list.Text_data_format . _Heteronucl_NOE_list.Text_data . loop_ _Heteronucl_NOE_experiment.Experiment_ID _Heteronucl_NOE_experiment.Experiment_name _Heteronucl_NOE_experiment.Sample_ID _Heteronucl_NOE_experiment.Sample_label _Heteronucl_NOE_experiment.Sample_state _Heteronucl_NOE_experiment.Entry_ID _Heteronucl_NOE_experiment.Heteronucl_NOE_list_ID 3 '{1H}-15N NOE' 1 $sample_1 . 5996 5 stop_ loop_ _Heteronucl_NOE.ID _Heteronucl_NOE.Assembly_atom_ID_1 _Heteronucl_NOE.Entity_assembly_ID_1 _Heteronucl_NOE.Entity_ID_1 _Heteronucl_NOE.Comp_index_ID_1 _Heteronucl_NOE.Seq_ID_1 _Heteronucl_NOE.Comp_ID_1 _Heteronucl_NOE.Atom_ID_1 _Heteronucl_NOE.Atom_type_1 _Heteronucl_NOE.Atom_isotope_number_1 _Heteronucl_NOE.Assembly_atom_ID_2 _Heteronucl_NOE.Entity_assembly_ID_2 _Heteronucl_NOE.Entity_ID_2 _Heteronucl_NOE.Comp_index_ID_2 _Heteronucl_NOE.Seq_ID_2 _Heteronucl_NOE.Comp_ID_2 _Heteronucl_NOE.Atom_ID_2 _Heteronucl_NOE.Atom_type_2 _Heteronucl_NOE.Atom_isotope_number_2 _Heteronucl_NOE.Val _Heteronucl_NOE.Val_err _Heteronucl_NOE.Resonance_ID_1 _Heteronucl_NOE.Resonance_ID_2 _Heteronucl_NOE.Auth_entity_assembly_ID_1 _Heteronucl_NOE.Auth_seq_ID_1 _Heteronucl_NOE.Auth_comp_ID_1 _Heteronucl_NOE.Auth_atom_ID_1 _Heteronucl_NOE.Auth_entity_assembly_ID_2 _Heteronucl_NOE.Auth_seq_ID_2 _Heteronucl_NOE.Auth_comp_ID_2 _Heteronucl_NOE.Auth_atom_ID_2 _Heteronucl_NOE.Entry_ID _Heteronucl_NOE.Heteronucl_NOE_list_ID 1 . 1 1 3 3 ALA N N 15 . 1 1 3 3 ALA H H 1 0.63 0.01 . . . . . . . . . . 5996 5 2 . 1 1 4 4 SER N N 15 . 1 1 4 4 SER H H 1 0.71 0.01 . . . . . . . . . . 5996 5 3 . 1 1 5 5 SER N N 15 . 1 1 5 5 SER H H 1 0.79 0.01 . . . . . . . . . . 5996 5 4 . 1 1 6 6 THR N N 15 . 1 1 6 6 THR H H 1 0.80 0.01 . . . . . . . . . . 5996 5 5 . 1 1 7 7 GLY N N 15 . 1 1 7 7 GLY H H 1 0.68 0.01 . . . . . . . . . . 5996 5 6 . 1 1 10 10 PHE N N 15 . 1 1 10 10 PHE H H 1 0.57 0.01 . . . . . . . . . . 5996 5 7 . 1 1 11 11 ASN N N 15 . 1 1 11 11 ASN H H 1 0.84 0.01 . . . . . . . . . . 5996 5 8 . 1 1 12 12 VAL N N 15 . 1 1 12 12 VAL H H 1 0.75 0.01 . . . . . . . . . . 5996 5 9 . 1 1 13 13 GLU N N 15 . 1 1 13 13 GLU H H 1 0.79 0.01 . . . . . . . . . . 5996 5 10 . 1 1 15 15 ILE N N 15 . 1 1 15 15 ILE H H 1 0.80 0.01 . . . . . . . . . . 5996 5 11 . 1 1 16 16 ASN N N 15 . 1 1 16 16 ASN H H 1 0.81 0.01 . . . . . . . . . . 5996 5 12 . 1 1 17 17 GLY N N 15 . 1 1 17 17 GLY H H 1 0.82 0.01 . . . . . . . . . . 5996 5 13 . 1 1 18 18 GLU N N 15 . 1 1 18 18 GLU H H 1 0.77 0.01 . . . . . . . . . . 5996 5 14 . 1 1 20 20 HIS N N 15 . 1 1 20 20 HIS H H 1 0.85 0.01 . . . . . . . . . . 5996 5 15 . 1 1 21 21 THR N N 15 . 1 1 21 21 THR H H 1 0.82 0.01 . . . . . . . . . . 5996 5 16 . 1 1 22 22 ILE N N 15 . 1 1 22 22 ILE H H 1 0.81 0.01 . . . . . . . . . . 5996 5 17 . 1 1 23 23 ILE N N 15 . 1 1 23 23 ILE H H 1 0.79 0.01 . . . . . . . . . . 5996 5 18 . 1 1 27 27 ASP N N 15 . 1 1 27 27 ASP H H 1 0.77 0.01 . . . . . . . . . . 5996 5 19 . 1 1 29 29 ARG N N 15 . 1 1 29 29 ARG H H 1 0.76 0.01 . . . . . . . . . . 5996 5 20 . 1 1 31 31 LYS N N 15 . 1 1 31 31 LYS H H 1 0.81 0.01 . . . . . . . . . . 5996 5 21 . 1 1 32 32 ILE N N 15 . 1 1 32 32 ILE H H 1 0.81 0.01 . . . . . . . . . . 5996 5 22 . 1 1 33 33 GLU N N 15 . 1 1 33 33 GLU H H 1 0.80 0.01 . . . . . . . . . . 5996 5 23 . 1 1 35 35 ASN N N 15 . 1 1 35 35 ASN H H 1 0.68 0.01 . . . . . . . . . . 5996 5 24 . 1 1 36 36 GLY N N 15 . 1 1 36 36 GLY H H 1 0.80 0.01 . . . . . . . . . . 5996 5 25 . 1 1 37 37 ASN N N 15 . 1 1 37 37 ASN H H 1 0.79 0.01 . . . . . . . . . . 5996 5 26 . 1 1 39 39 ARG N N 15 . 1 1 39 39 ARG H H 1 0.83 0.01 . . . . . . . . . . 5996 5 27 . 1 1 40 40 LEU N N 15 . 1 1 40 40 LEU H H 1 0.77 0.01 . . . . . . . . . . 5996 5 28 . 1 1 42 42 LEU N N 15 . 1 1 42 42 LEU H H 1 0.72 0.01 . . . . . . . . . . 5996 5 29 . 1 1 43 43 GLU N N 15 . 1 1 43 43 GLU H H 1 0.73 0.01 . . . . . . . . . . 5996 5 30 . 1 1 45 45 ILE N N 15 . 1 1 45 45 ILE H H 1 0.77 0.01 . . . . . . . . . . 5996 5 31 . 1 1 46 46 HIS N N 15 . 1 1 46 46 HIS H H 1 0.80 0.01 . . . . . . . . . . 5996 5 32 . 1 1 47 47 VAL N N 15 . 1 1 47 47 VAL H H 1 0.78 0.01 . . . . . . . . . . 5996 5 33 . 1 1 48 48 LEU N N 15 . 1 1 48 48 LEU H H 1 0.76 0.01 . . . . . . . . . . 5996 5 34 . 1 1 50 50 ASN N N 15 . 1 1 50 50 ASN H H 1 0.69 0.01 . . . . . . . . . . 5996 5 35 . 1 1 51 51 SER N N 15 . 1 1 51 51 SER H H 1 0.71 0.01 . . . . . . . . . . 5996 5 36 . 1 1 52 52 LEU N N 15 . 1 1 52 52 LEU H H 1 0.78 0.01 . . . . . . . . . . 5996 5 37 . 1 1 53 53 VAL N N 15 . 1 1 53 53 VAL H H 1 0.79 0.01 . . . . . . . . . . 5996 5 38 . 1 1 54 54 LEU N N 15 . 1 1 54 54 LEU H H 1 0.79 0.01 . . . . . . . . . . 5996 5 39 . 1 1 55 55 LYS N N 15 . 1 1 55 55 LYS H H 1 0.77 0.01 . . . . . . . . . . 5996 5 40 . 1 1 57 57 HIS N N 15 . 1 1 57 57 HIS H H 1 0.77 0.01 . . . . . . . . . . 5996 5 41 . 1 1 58 58 THR N N 15 . 1 1 58 58 THR H H 1 0.72 0.01 . . . . . . . . . . 5996 5 42 . 1 1 60 60 ARG N N 15 . 1 1 60 60 ARG H H 1 0.67 0.01 . . . . . . . . . . 5996 5 43 . 1 1 61 61 ASP N N 15 . 1 1 61 61 ASP H H 1 0.71 0.01 . . . . . . . . . . 5996 5 44 . 1 1 62 62 GLU N N 15 . 1 1 62 62 GLU H H 1 0.71 0.01 . . . . . . . . . . 5996 5 45 . 1 1 64 64 CYS N N 15 . 1 1 64 64 CYS H H 1 0.67 0.01 . . . . . . . . . . 5996 5 46 . 1 1 65 65 SER N N 15 . 1 1 65 65 SER H H 1 0.68 0.01 . . . . . . . . . . 5996 5 47 . 1 1 66 66 GLU N N 15 . 1 1 66 66 GLU H H 1 0.73 0.01 . . . . . . . . . . 5996 5 48 . 1 1 67 67 LEU N N 15 . 1 1 67 67 LEU H H 1 0.72 0.01 . . . . . . . . . . 5996 5 49 . 1 1 68 68 SER N N 15 . 1 1 68 68 SER H H 1 0.72 0.01 . . . . . . . . . . 5996 5 50 . 1 1 69 69 MET N N 15 . 1 1 69 69 MET H H 1 0.77 0.01 . . . . . . . . . . 5996 5 51 . 1 1 71 71 ALA N N 15 . 1 1 71 71 ALA H H 1 0.80 0.01 . . . . . . . . . . 5996 5 52 . 1 1 72 72 ASP N N 15 . 1 1 72 72 ASP H H 1 0.73 0.01 . . . . . . . . . . 5996 5 53 . 1 1 74 74 THR N N 15 . 1 1 74 74 THR H H 1 0.72 0.01 . . . . . . . . . . 5996 5 54 . 1 1 75 75 GLU N N 15 . 1 1 75 75 GLU H H 1 0.70 0.01 . . . . . . . . . . 5996 5 55 . 1 1 76 76 LYS N N 15 . 1 1 76 76 LYS H H 1 0.74 0.01 . . . . . . . . . . 5996 5 56 . 1 1 77 77 ALA N N 15 . 1 1 77 77 ALA H H 1 0.68 0.01 . . . . . . . . . . 5996 5 57 . 1 1 78 78 GLY N N 15 . 1 1 78 78 GLY H H 1 0.70 0.01 . . . . . . . . . . 5996 5 58 . 1 1 79 79 GLU N N 15 . 1 1 79 79 GLU H H 1 0.76 0.01 . . . . . . . . . . 5996 5 59 . 1 1 81 81 SER N N 15 . 1 1 81 81 SER H H 1 0.80 0.01 . . . . . . . . . . 5996 5 60 . 1 1 82 82 VAL N N 15 . 1 1 82 82 VAL H H 1 0.78 0.01 . . . . . . . . . . 5996 5 61 . 1 1 83 83 THR N N 15 . 1 1 83 83 THR H H 1 0.77 0.01 . . . . . . . . . . 5996 5 62 . 1 1 84 84 TYR N N 15 . 1 1 84 84 TYR H H 1 0.81 0.01 . . . . . . . . . . 5996 5 63 . 1 1 85 85 ASP N N 15 . 1 1 85 85 ASP H H 1 0.78 0.01 . . . . . . . . . . 5996 5 64 . 1 1 86 86 GLY N N 15 . 1 1 86 86 GLY H H 1 0.78 0.01 . . . . . . . . . . 5996 5 65 . 1 1 87 87 PHE N N 15 . 1 1 87 87 PHE H H 1 0.79 0.01 . . . . . . . . . . 5996 5 66 . 1 1 89 89 THR N N 15 . 1 1 89 89 THR H H 1 0.81 0.01 . . . . . . . . . . 5996 5 67 . 1 1 90 90 PHE N N 15 . 1 1 90 90 PHE H H 1 0.79 0.01 . . . . . . . . . . 5996 5 68 . 1 1 91 91 THR N N 15 . 1 1 91 91 THR H H 1 0.79 0.01 . . . . . . . . . . 5996 5 69 . 1 1 92 92 ILE N N 15 . 1 1 92 92 ILE H H 1 0.81 0.01 . . . . . . . . . . 5996 5 70 . 1 1 94 94 LYS N N 15 . 1 1 94 94 LYS H H 1 0.80 0.01 . . . . . . . . . . 5996 5 71 . 1 1 95 95 THR N N 15 . 1 1 95 95 THR H H 1 0.80 0.01 . . . . . . . . . . 5996 5 72 . 1 1 96 96 ASP N N 15 . 1 1 96 96 ASP H H 1 0.77 0.01 . . . . . . . . . . 5996 5 73 . 1 1 97 97 TYR N N 15 . 1 1 97 97 TYR H H 1 0.78 0.01 . . . . . . . . . . 5996 5 74 . 1 1 98 98 ASP N N 15 . 1 1 98 98 ASP H H 1 0.82 0.01 . . . . . . . . . . 5996 5 75 . 1 1 99 99 ASN N N 15 . 1 1 99 99 ASN H H 1 0.80 0.01 . . . . . . . . . . 5996 5 76 . 1 1 100 100 PHE N N 15 . 1 1 100 100 PHE H H 1 0.81 0.01 . . . . . . . . . . 5996 5 77 . 1 1 102 102 MET N N 15 . 1 1 102 102 MET H H 1 0.81 0.01 . . . . . . . . . . 5996 5 78 . 1 1 103 103 ALA N N 15 . 1 1 103 103 ALA H H 1 0.79 0.01 . . . . . . . . . . 5996 5 79 . 1 1 104 104 HIS N N 15 . 1 1 104 104 HIS H H 1 0.72 0.01 . . . . . . . . . . 5996 5 80 . 1 1 105 105 LEU N N 15 . 1 1 105 105 LEU H H 1 0.82 0.01 . . . . . . . . . . 5996 5 81 . 1 1 107 107 ASN N N 15 . 1 1 107 107 ASN H H 1 0.81 0.01 . . . . . . . . . . 5996 5 82 . 1 1 108 108 GLU N N 15 . 1 1 108 108 GLU H H 1 0.77 0.01 . . . . . . . . . . 5996 5 83 . 1 1 109 109 LYS N N 15 . 1 1 109 109 LYS H H 1 0.80 0.01 . . . . . . . . . . 5996 5 84 . 1 1 110 110 ASP N N 15 . 1 1 110 110 ASP H H 1 0.72 0.01 . . . . . . . . . . 5996 5 85 . 1 1 111 111 GLY N N 15 . 1 1 111 111 GLY H H 1 0.71 0.01 . . . . . . . . . . 5996 5 86 . 1 1 113 113 THR N N 15 . 1 1 113 113 THR H H 1 0.76 0.01 . . . . . . . . . . 5996 5 87 . 1 1 114 114 PHE N N 15 . 1 1 114 114 PHE H H 1 0.78 0.01 . . . . . . . . . . 5996 5 88 . 1 1 115 115 GLN N N 15 . 1 1 115 115 GLN H H 1 0.80 0.01 . . . . . . . . . . 5996 5 89 . 1 1 116 116 LEU N N 15 . 1 1 116 116 LEU H H 1 0.80 0.01 . . . . . . . . . . 5996 5 90 . 1 1 117 117 MET N N 15 . 1 1 117 117 MET H H 1 0.79 0.01 . . . . . . . . . . 5996 5 91 . 1 1 121 121 GLY N N 15 . 1 1 121 121 GLY H H 1 0.79 0.01 . . . . . . . . . . 5996 5 92 . 1 1 123 123 GLU N N 15 . 1 1 123 123 GLU H H 1 0.76 0.01 . . . . . . . . . . 5996 5 93 . 1 1 125 125 ASP N N 15 . 1 1 125 125 ASP H H 1 0.76 0.01 . . . . . . . . . . 5996 5 94 . 1 1 126 126 LEU N N 15 . 1 1 126 126 LEU H H 1 0.78 0.01 . . . . . . . . . . 5996 5 95 . 1 1 127 127 SER N N 15 . 1 1 127 127 SER H H 1 0.78 0.01 . . . . . . . . . . 5996 5 96 . 1 1 128 128 SER N N 15 . 1 1 128 128 SER H H 1 0.76 0.01 . . . . . . . . . . 5996 5 97 . 1 1 129 129 ASP N N 15 . 1 1 129 129 ASP H H 1 0.79 0.01 . . . . . . . . . . 5996 5 98 . 1 1 131 131 LYS N N 15 . 1 1 131 131 LYS H H 1 0.79 0.01 . . . . . . . . . . 5996 5 99 . 1 1 133 133 ARG N N 15 . 1 1 133 133 ARG H H 1 0.81 0.01 . . . . . . . . . . 5996 5 100 . 1 1 134 134 PHE N N 15 . 1 1 134 134 PHE H H 1 0.76 0.01 . . . . . . . . . . 5996 5 101 . 1 1 135 135 ALA N N 15 . 1 1 135 135 ALA H H 1 0.79 0.01 . . . . . . . . . . 5996 5 102 . 1 1 136 136 GLN N N 15 . 1 1 136 136 GLN H H 1 0.81 0.01 . . . . . . . . . . 5996 5 103 . 1 1 138 138 CYS N N 15 . 1 1 138 138 CYS H H 1 0.78 0.01 . . . . . . . . . . 5996 5 104 . 1 1 141 141 HIS N N 15 . 1 1 141 141 HIS H H 1 0.78 0.01 . . . . . . . . . . 5996 5 105 . 1 1 142 142 GLY N N 15 . 1 1 142 142 GLY H H 1 0.77 0.01 . . . . . . . . . . 5996 5 106 . 1 1 143 143 ILE N N 15 . 1 1 143 143 ILE H H 1 0.77 0.01 . . . . . . . . . . 5996 5 107 . 1 1 144 144 LEU N N 15 . 1 1 144 144 LEU H H 1 0.70 0.01 . . . . . . . . . . 5996 5 108 . 1 1 145 145 ARG N N 15 . 1 1 145 145 ARG H H 1 0.73 0.01 . . . . . . . . . . 5996 5 109 . 1 1 146 146 GLU N N 15 . 1 1 146 146 GLU H H 1 0.77 0.01 . . . . . . . . . . 5996 5 110 . 1 1 148 148 ILE N N 15 . 1 1 148 148 ILE H H 1 0.79 0.01 . . . . . . . . . . 5996 5 111 . 1 1 149 149 ILE N N 15 . 1 1 149 149 ILE H H 1 0.78 0.01 . . . . . . . . . . 5996 5 112 . 1 1 150 150 ASP N N 15 . 1 1 150 150 ASP H H 1 0.79 0.01 . . . . . . . . . . 5996 5 113 . 1 1 151 151 LEU N N 15 . 1 1 151 151 LEU H H 1 0.80 0.01 . . . . . . . . . . 5996 5 114 . 1 1 152 152 SER N N 15 . 1 1 152 152 SER H H 1 0.79 0.01 . . . . . . . . . . 5996 5 115 . 1 1 153 153 ASN N N 15 . 1 1 153 153 ASN H H 1 0.75 0.01 . . . . . . . . . . 5996 5 116 . 1 1 155 155 ASN N N 15 . 1 1 155 155 ASN H H 1 0.74 0.01 . . . . . . . . . . 5996 5 117 . 1 1 156 156 ARG N N 15 . 1 1 156 156 ARG H H 1 0.64 0.03 . . . . . . . . . . 5996 5 118 . 1 1 160 160 ALA N N 15 . 1 1 160 160 ALA H H 1 0.02 0.01 . . . . . . . . . . 5996 5 119 . 1 1 162 162 GLU N N 15 . 1 1 162 162 GLU H H 1 -0.57 0.01 . . . . . . . . . . 5996 5 stop_ save_ save_308_600_bound_noe _Heteronucl_NOE_list.Sf_category heteronucl_NOEs _Heteronucl_NOE_list.Sf_framecode 308_600_bound_noe _Heteronucl_NOE_list.Entry_ID 5996 _Heteronucl_NOE_list.ID 6 _Heteronucl_NOE_list.Sample_condition_list_ID 6 _Heteronucl_NOE_list.Sample_condition_list_label $308K _Heteronucl_NOE_list.Spectrometer_frequency_1H 600 _Heteronucl_NOE_list.Heteronuclear_NOE_val_type 'relative intensities' _Heteronucl_NOE_list.NOE_ref_val . _Heteronucl_NOE_list.NOE_ref_description . _Heteronucl_NOE_list.Details . _Heteronucl_NOE_list.Text_data_format . _Heteronucl_NOE_list.Text_data . loop_ _Heteronucl_NOE_experiment.Experiment_ID _Heteronucl_NOE_experiment.Experiment_name _Heteronucl_NOE_experiment.Sample_ID _Heteronucl_NOE_experiment.Sample_label _Heteronucl_NOE_experiment.Sample_state _Heteronucl_NOE_experiment.Entry_ID _Heteronucl_NOE_experiment.Heteronucl_NOE_list_ID 3 '{1H}-15N NOE' 1 $sample_1 . 5996 6 stop_ loop_ _Heteronucl_NOE.ID _Heteronucl_NOE.Assembly_atom_ID_1 _Heteronucl_NOE.Entity_assembly_ID_1 _Heteronucl_NOE.Entity_ID_1 _Heteronucl_NOE.Comp_index_ID_1 _Heteronucl_NOE.Seq_ID_1 _Heteronucl_NOE.Comp_ID_1 _Heteronucl_NOE.Atom_ID_1 _Heteronucl_NOE.Atom_type_1 _Heteronucl_NOE.Atom_isotope_number_1 _Heteronucl_NOE.Assembly_atom_ID_2 _Heteronucl_NOE.Entity_assembly_ID_2 _Heteronucl_NOE.Entity_ID_2 _Heteronucl_NOE.Comp_index_ID_2 _Heteronucl_NOE.Seq_ID_2 _Heteronucl_NOE.Comp_ID_2 _Heteronucl_NOE.Atom_ID_2 _Heteronucl_NOE.Atom_type_2 _Heteronucl_NOE.Atom_isotope_number_2 _Heteronucl_NOE.Val _Heteronucl_NOE.Val_err _Heteronucl_NOE.Resonance_ID_1 _Heteronucl_NOE.Resonance_ID_2 _Heteronucl_NOE.Auth_entity_assembly_ID_1 _Heteronucl_NOE.Auth_seq_ID_1 _Heteronucl_NOE.Auth_comp_ID_1 _Heteronucl_NOE.Auth_atom_ID_1 _Heteronucl_NOE.Auth_entity_assembly_ID_2 _Heteronucl_NOE.Auth_seq_ID_2 _Heteronucl_NOE.Auth_comp_ID_2 _Heteronucl_NOE.Auth_atom_ID_2 _Heteronucl_NOE.Entry_ID _Heteronucl_NOE.Heteronucl_NOE_list_ID 1 . 1 1 3 3 ALA N N 15 . 1 1 3 3 ALA H H 1 0.66 0.01 . . . . . . . . . . 5996 6 2 . 1 1 4 4 SER N N 15 . 1 1 4 4 SER H H 1 0.72 0.01 . . . . . . . . . . 5996 6 3 . 1 1 6 6 THR N N 15 . 1 1 6 6 THR H H 1 0.82 0.01 . . . . . . . . . . 5996 6 4 . 1 1 10 10 PHE N N 15 . 1 1 10 10 PHE H H 1 0.58 0.01 . . . . . . . . . . 5996 6 5 . 1 1 11 11 ASN N N 15 . 1 1 11 11 ASN H H 1 0.81 0.01 . . . . . . . . . . 5996 6 6 . 1 1 12 12 VAL N N 15 . 1 1 12 12 VAL H H 1 0.79 0.01 . . . . . . . . . . 5996 6 7 . 1 1 13 13 GLU N N 15 . 1 1 13 13 GLU H H 1 0.78 0.02 . . . . . . . . . . 5996 6 8 . 1 1 16 16 ASN N N 15 . 1 1 16 16 ASN H H 1 0.83 0.01 . . . . . . . . . . 5996 6 9 . 1 1 17 17 GLY N N 15 . 1 1 17 17 GLY H H 1 0.82 0.01 . . . . . . . . . . 5996 6 10 . 1 1 18 18 GLU N N 15 . 1 1 18 18 GLU H H 1 0.81 0.02 . . . . . . . . . . 5996 6 11 . 1 1 19 19 TRP N N 15 . 1 1 19 19 TRP H H 1 0.81 0.01 . . . . . . . . . . 5996 6 12 . 1 1 21 21 THR N N 15 . 1 1 21 21 THR H H 1 0.79 0.02 . . . . . . . . . . 5996 6 13 . 1 1 22 22 ILE N N 15 . 1 1 22 22 ILE H H 1 0.83 0.02 . . . . . . . . . . 5996 6 14 . 1 1 23 23 ILE N N 15 . 1 1 23 23 ILE H H 1 0.81 0.01 . . . . . . . . . . 5996 6 15 . 1 1 26 26 SER N N 15 . 1 1 26 26 SER H H 1 0.81 0.00 . . . . . . . . . . 5996 6 16 . 1 1 27 27 ASP N N 15 . 1 1 27 27 ASP H H 1 0.81 0.01 . . . . . . . . . . 5996 6 17 . 1 1 29 29 ARG N N 15 . 1 1 29 29 ARG H H 1 0.77 0.01 . . . . . . . . . . 5996 6 18 . 1 1 30 30 GLU N N 15 . 1 1 30 30 GLU H H 1 0.82 0.01 . . . . . . . . . . 5996 6 19 . 1 1 31 31 LYS N N 15 . 1 1 31 31 LYS H H 1 0.80 0.01 . . . . . . . . . . 5996 6 20 . 1 1 32 32 ILE N N 15 . 1 1 32 32 ILE H H 1 0.83 0.01 . . . . . . . . . . 5996 6 21 . 1 1 33 33 GLU N N 15 . 1 1 33 33 GLU H H 1 0.80 0.00 . . . . . . . . . . 5996 6 22 . 1 1 35 35 ASN N N 15 . 1 1 35 35 ASN H H 1 0.71 0.01 . . . . . . . . . . 5996 6 23 . 1 1 36 36 GLY N N 15 . 1 1 36 36 GLY H H 1 0.83 0.01 . . . . . . . . . . 5996 6 24 . 1 1 38 38 PHE N N 15 . 1 1 38 38 PHE H H 1 0.80 0.01 . . . . . . . . . . 5996 6 25 . 1 1 39 39 ARG N N 15 . 1 1 39 39 ARG H H 1 0.81 0.01 . . . . . . . . . . 5996 6 26 . 1 1 40 40 LEU N N 15 . 1 1 40 40 LEU H H 1 0.81 0.01 . . . . . . . . . . 5996 6 27 . 1 1 42 42 LEU N N 15 . 1 1 42 42 LEU H H 1 0.78 0.04 . . . . . . . . . . 5996 6 28 . 1 1 43 43 GLU N N 15 . 1 1 43 43 GLU H H 1 0.84 0.01 . . . . . . . . . . 5996 6 29 . 1 1 45 45 ILE N N 15 . 1 1 45 45 ILE H H 1 0.81 0.01 . . . . . . . . . . 5996 6 30 . 1 1 46 46 HIS N N 15 . 1 1 46 46 HIS H H 1 0.81 0.01 . . . . . . . . . . 5996 6 31 . 1 1 47 47 VAL N N 15 . 1 1 47 47 VAL H H 1 0.78 0.01 . . . . . . . . . . 5996 6 32 . 1 1 48 48 LEU N N 15 . 1 1 48 48 LEU H H 1 0.79 0.01 . . . . . . . . . . 5996 6 33 . 1 1 50 50 ASN N N 15 . 1 1 50 50 ASN H H 1 0.70 0.01 . . . . . . . . . . 5996 6 34 . 1 1 51 51 SER N N 15 . 1 1 51 51 SER H H 1 0.70 0.01 . . . . . . . . . . 5996 6 35 . 1 1 52 52 LEU N N 15 . 1 1 52 52 LEU H H 1 0.77 0.01 . . . . . . . . . . 5996 6 36 . 1 1 53 53 VAL N N 15 . 1 1 53 53 VAL H H 1 0.80 0.01 . . . . . . . . . . 5996 6 37 . 1 1 54 54 LEU N N 15 . 1 1 54 54 LEU H H 1 0.82 0.01 . . . . . . . . . . 5996 6 38 . 1 1 57 57 HIS N N 15 . 1 1 57 57 HIS H H 1 0.81 0.01 . . . . . . . . . . 5996 6 39 . 1 1 60 60 ARG N N 15 . 1 1 60 60 ARG H H 1 0.71 0.01 . . . . . . . . . . 5996 6 40 . 1 1 61 61 ASP N N 15 . 1 1 61 61 ASP H H 1 0.70 0.01 . . . . . . . . . . 5996 6 41 . 1 1 62 62 GLU N N 15 . 1 1 62 62 GLU H H 1 0.71 0.02 . . . . . . . . . . 5996 6 42 . 1 1 64 64 CYS N N 15 . 1 1 64 64 CYS H H 1 0.68 0.01 . . . . . . . . . . 5996 6 43 . 1 1 65 65 SER N N 15 . 1 1 65 65 SER H H 1 0.71 0.01 . . . . . . . . . . 5996 6 44 . 1 1 66 66 GLU N N 15 . 1 1 66 66 GLU H H 1 0.75 0.01 . . . . . . . . . . 5996 6 45 . 1 1 67 67 LEU N N 15 . 1 1 67 67 LEU H H 1 0.75 0.01 . . . . . . . . . . 5996 6 46 . 1 1 68 68 SER N N 15 . 1 1 68 68 SER H H 1 0.74 0.01 . . . . . . . . . . 5996 6 47 . 1 1 69 69 MET N N 15 . 1 1 69 69 MET H H 1 0.79 0.01 . . . . . . . . . . 5996 6 48 . 1 1 71 71 ALA N N 15 . 1 1 71 71 ALA H H 1 0.78 0.01 . . . . . . . . . . 5996 6 49 . 1 1 72 72 ASP N N 15 . 1 1 72 72 ASP H H 1 0.77 0.01 . . . . . . . . . . 5996 6 50 . 1 1 74 74 THR N N 15 . 1 1 74 74 THR H H 1 0.70 0.01 . . . . . . . . . . 5996 6 51 . 1 1 75 75 GLU N N 15 . 1 1 75 75 GLU H H 1 0.70 0.01 . . . . . . . . . . 5996 6 52 . 1 1 77 77 ALA N N 15 . 1 1 77 77 ALA H H 1 0.71 0.02 . . . . . . . . . . 5996 6 53 . 1 1 78 78 GLY N N 15 . 1 1 78 78 GLY H H 1 0.70 0.04 . . . . . . . . . . 5996 6 54 . 1 1 79 79 GLU N N 15 . 1 1 79 79 GLU H H 1 0.77 0.01 . . . . . . . . . . 5996 6 55 . 1 1 80 80 TYR N N 15 . 1 1 80 80 TYR H H 1 0.81 0.01 . . . . . . . . . . 5996 6 56 . 1 1 81 81 SER N N 15 . 1 1 81 81 SER H H 1 0.80 0.01 . . . . . . . . . . 5996 6 57 . 1 1 82 82 VAL N N 15 . 1 1 82 82 VAL H H 1 0.80 0.01 . . . . . . . . . . 5996 6 58 . 1 1 84 84 TYR N N 15 . 1 1 84 84 TYR H H 1 0.81 0.01 . . . . . . . . . . 5996 6 59 . 1 1 85 85 ASP N N 15 . 1 1 85 85 ASP H H 1 0.80 0.01 . . . . . . . . . . 5996 6 60 . 1 1 86 86 GLY N N 15 . 1 1 86 86 GLY H H 1 0.81 0.01 . . . . . . . . . . 5996 6 61 . 1 1 87 87 PHE N N 15 . 1 1 87 87 PHE H H 1 0.81 0.01 . . . . . . . . . . 5996 6 62 . 1 1 88 88 ASN N N 15 . 1 1 88 88 ASN H H 1 0.79 0.01 . . . . . . . . . . 5996 6 63 . 1 1 89 89 THR N N 15 . 1 1 89 89 THR H H 1 0.82 0.01 . . . . . . . . . . 5996 6 64 . 1 1 90 90 PHE N N 15 . 1 1 90 90 PHE H H 1 0.81 0.01 . . . . . . . . . . 5996 6 65 . 1 1 91 91 THR N N 15 . 1 1 91 91 THR H H 1 0.78 0.01 . . . . . . . . . . 5996 6 66 . 1 1 92 92 ILE N N 15 . 1 1 92 92 ILE H H 1 0.80 0.01 . . . . . . . . . . 5996 6 67 . 1 1 94 94 LYS N N 15 . 1 1 94 94 LYS H H 1 0.80 0.01 . . . . . . . . . . 5996 6 68 . 1 1 95 95 THR N N 15 . 1 1 95 95 THR H H 1 0.81 0.01 . . . . . . . . . . 5996 6 69 . 1 1 96 96 ASP N N 15 . 1 1 96 96 ASP H H 1 0.82 0.01 . . . . . . . . . . 5996 6 70 . 1 1 97 97 TYR N N 15 . 1 1 97 97 TYR H H 1 0.83 0.01 . . . . . . . . . . 5996 6 71 . 1 1 98 98 ASP N N 15 . 1 1 98 98 ASP H H 1 0.83 0.01 . . . . . . . . . . 5996 6 72 . 1 1 99 99 ASN N N 15 . 1 1 99 99 ASN H H 1 0.78 0.01 . . . . . . . . . . 5996 6 73 . 1 1 100 100 PHE N N 15 . 1 1 100 100 PHE H H 1 0.82 0.01 . . . . . . . . . . 5996 6 74 . 1 1 103 103 ALA N N 15 . 1 1 103 103 ALA H H 1 0.80 0.01 . . . . . . . . . . 5996 6 75 . 1 1 104 104 HIS N N 15 . 1 1 104 104 HIS H H 1 0.73 0.01 . . . . . . . . . . 5996 6 76 . 1 1 105 105 LEU N N 15 . 1 1 105 105 LEU H H 1 0.81 0.01 . . . . . . . . . . 5996 6 77 . 1 1 107 107 ASN N N 15 . 1 1 107 107 ASN H H 1 0.81 0.01 . . . . . . . . . . 5996 6 78 . 1 1 108 108 GLU N N 15 . 1 1 108 108 GLU H H 1 0.79 0.01 . . . . . . . . . . 5996 6 79 . 1 1 109 109 LYS N N 15 . 1 1 109 109 LYS H H 1 0.80 0.01 . . . . . . . . . . 5996 6 80 . 1 1 111 111 GLY N N 15 . 1 1 111 111 GLY H H 1 0.72 0.01 . . . . . . . . . . 5996 6 81 . 1 1 114 114 PHE N N 15 . 1 1 114 114 PHE H H 1 0.81 0.01 . . . . . . . . . . 5996 6 82 . 1 1 115 115 GLN N N 15 . 1 1 115 115 GLN H H 1 0.79 0.01 . . . . . . . . . . 5996 6 83 . 1 1 116 116 LEU N N 15 . 1 1 116 116 LEU H H 1 0.80 0.01 . . . . . . . . . . 5996 6 84 . 1 1 117 117 MET N N 15 . 1 1 117 117 MET H H 1 0.80 0.01 . . . . . . . . . . 5996 6 85 . 1 1 118 118 GLY N N 15 . 1 1 118 118 GLY H H 1 0.80 0.03 . . . . . . . . . . 5996 6 86 . 1 1 121 121 GLY N N 15 . 1 1 121 121 GLY H H 1 0.81 0.01 . . . . . . . . . . 5996 6 87 . 1 1 123 123 GLU N N 15 . 1 1 123 123 GLU H H 1 0.78 0.01 . . . . . . . . . . 5996 6 88 . 1 1 125 125 ASP N N 15 . 1 1 125 125 ASP H H 1 0.77 0.01 . . . . . . . . . . 5996 6 89 . 1 1 126 126 LEU N N 15 . 1 1 126 126 LEU H H 1 0.76 0.01 . . . . . . . . . . 5996 6 90 . 1 1 127 127 SER N N 15 . 1 1 127 127 SER H H 1 0.78 0.01 . . . . . . . . . . 5996 6 91 . 1 1 129 129 ASP N N 15 . 1 1 129 129 ASP H H 1 0.81 0.01 . . . . . . . . . . 5996 6 92 . 1 1 130 130 ILE N N 15 . 1 1 130 130 ILE H H 1 0.80 0.01 . . . . . . . . . . 5996 6 93 . 1 1 131 131 LYS N N 15 . 1 1 131 131 LYS H H 1 0.82 0.01 . . . . . . . . . . 5996 6 94 . 1 1 133 133 ARG N N 15 . 1 1 133 133 ARG H H 1 0.82 0.01 . . . . . . . . . . 5996 6 95 . 1 1 136 136 GLN N N 15 . 1 1 136 136 GLN H H 1 0.83 0.01 . . . . . . . . . . 5996 6 96 . 1 1 137 137 LEU N N 15 . 1 1 137 137 LEU H H 1 0.81 0.01 . . . . . . . . . . 5996 6 97 . 1 1 138 138 CYS N N 15 . 1 1 138 138 CYS H H 1 0.83 0.01 . . . . . . . . . . 5996 6 98 . 1 1 140 140 LYS N N 15 . 1 1 140 140 LYS H H 1 0.82 0.01 . . . . . . . . . . 5996 6 99 . 1 1 142 142 GLY N N 15 . 1 1 142 142 GLY H H 1 0.78 0.01 . . . . . . . . . . 5996 6 100 . 1 1 143 143 ILE N N 15 . 1 1 143 143 ILE H H 1 0.74 0.02 . . . . . . . . . . 5996 6 101 . 1 1 144 144 LEU N N 15 . 1 1 144 144 LEU H H 1 0.72 0.01 . . . . . . . . . . 5996 6 102 . 1 1 145 145 ARG N N 15 . 1 1 145 145 ARG H H 1 0.74 0.01 . . . . . . . . . . 5996 6 103 . 1 1 146 146 GLU N N 15 . 1 1 146 146 GLU H H 1 0.78 0.01 . . . . . . . . . . 5996 6 104 . 1 1 148 148 ILE N N 15 . 1 1 148 148 ILE H H 1 0.80 0.01 . . . . . . . . . . 5996 6 105 . 1 1 150 150 ASP N N 15 . 1 1 150 150 ASP H H 1 0.81 0.01 . . . . . . . . . . 5996 6 106 . 1 1 151 151 LEU N N 15 . 1 1 151 151 LEU H H 1 0.81 0.01 . . . . . . . . . . 5996 6 107 . 1 1 152 152 SER N N 15 . 1 1 152 152 SER H H 1 0.82 0.01 . . . . . . . . . . 5996 6 108 . 1 1 153 153 ASN N N 15 . 1 1 153 153 ASN H H 1 0.80 0.01 . . . . . . . . . . 5996 6 109 . 1 1 155 155 ASN N N 15 . 1 1 155 155 ASN H H 1 0.76 0.01 . . . . . . . . . . 5996 6 110 . 1 1 160 160 ALA N N 15 . 1 1 160 160 ALA H H 1 0.04 0.01 . . . . . . . . . . 5996 6 111 . 1 1 162 162 GLU N N 15 . 1 1 162 162 GLU H H 1 -0.59 0.01 . . . . . . . . . . 5996 6 stop_ save_ save_291_500_bound_noe _Heteronucl_NOE_list.Sf_category heteronucl_NOEs _Heteronucl_NOE_list.Sf_framecode 291_500_bound_noe _Heteronucl_NOE_list.Entry_ID 5996 _Heteronucl_NOE_list.ID 7 _Heteronucl_NOE_list.Sample_condition_list_ID 7 _Heteronucl_NOE_list.Sample_condition_list_label $291K _Heteronucl_NOE_list.Spectrometer_frequency_1H 500 _Heteronucl_NOE_list.Heteronuclear_NOE_val_type 'relative intensities' _Heteronucl_NOE_list.NOE_ref_val . _Heteronucl_NOE_list.NOE_ref_description . _Heteronucl_NOE_list.Details . _Heteronucl_NOE_list.Text_data_format . _Heteronucl_NOE_list.Text_data . loop_ _Heteronucl_NOE_experiment.Experiment_ID _Heteronucl_NOE_experiment.Experiment_name _Heteronucl_NOE_experiment.Sample_ID _Heteronucl_NOE_experiment.Sample_label _Heteronucl_NOE_experiment.Sample_state _Heteronucl_NOE_experiment.Entry_ID _Heteronucl_NOE_experiment.Heteronucl_NOE_list_ID 3 '{1H}-15N NOE' 1 $sample_1 . 5996 7 stop_ loop_ _Heteronucl_NOE.ID _Heteronucl_NOE.Assembly_atom_ID_1 _Heteronucl_NOE.Entity_assembly_ID_1 _Heteronucl_NOE.Entity_ID_1 _Heteronucl_NOE.Comp_index_ID_1 _Heteronucl_NOE.Seq_ID_1 _Heteronucl_NOE.Comp_ID_1 _Heteronucl_NOE.Atom_ID_1 _Heteronucl_NOE.Atom_type_1 _Heteronucl_NOE.Atom_isotope_number_1 _Heteronucl_NOE.Assembly_atom_ID_2 _Heteronucl_NOE.Entity_assembly_ID_2 _Heteronucl_NOE.Entity_ID_2 _Heteronucl_NOE.Comp_index_ID_2 _Heteronucl_NOE.Seq_ID_2 _Heteronucl_NOE.Comp_ID_2 _Heteronucl_NOE.Atom_ID_2 _Heteronucl_NOE.Atom_type_2 _Heteronucl_NOE.Atom_isotope_number_2 _Heteronucl_NOE.Val _Heteronucl_NOE.Val_err _Heteronucl_NOE.Resonance_ID_1 _Heteronucl_NOE.Resonance_ID_2 _Heteronucl_NOE.Auth_entity_assembly_ID_1 _Heteronucl_NOE.Auth_seq_ID_1 _Heteronucl_NOE.Auth_comp_ID_1 _Heteronucl_NOE.Auth_atom_ID_1 _Heteronucl_NOE.Auth_entity_assembly_ID_2 _Heteronucl_NOE.Auth_seq_ID_2 _Heteronucl_NOE.Auth_comp_ID_2 _Heteronucl_NOE.Auth_atom_ID_2 _Heteronucl_NOE.Entry_ID _Heteronucl_NOE.Heteronucl_NOE_list_ID 1 . 1 1 3 3 ALA N N 15 . 1 1 3 3 ALA H H 1 0.61 0.03 . . . . . . . . . . 5996 7 2 . 1 1 4 4 SER N N 15 . 1 1 4 4 SER H H 1 0.69 0.03 . . . . . . . . . . 5996 7 3 . 1 1 5 5 SER N N 15 . 1 1 5 5 SER H H 1 0.74 0.03 . . . . . . . . . . 5996 7 4 . 1 1 6 6 THR N N 15 . 1 1 6 6 THR H H 1 0.68 0.04 . . . . . . . . . . 5996 7 5 . 1 1 7 7 GLY N N 15 . 1 1 7 7 GLY H H 1 0.62 0.04 . . . . . . . . . . 5996 7 6 . 1 1 11 11 ASN N N 15 . 1 1 11 11 ASN H H 1 0.73 0.04 . . . . . . . . . . 5996 7 7 . 1 1 13 13 GLU N N 15 . 1 1 13 13 GLU H H 1 0.77 0.05 . . . . . . . . . . 5996 7 8 . 1 1 15 15 ILE N N 15 . 1 1 15 15 ILE H H 1 0.75 0.05 . . . . . . . . . . 5996 7 9 . 1 1 16 16 ASN N N 15 . 1 1 16 16 ASN H H 1 0.74 0.03 . . . . . . . . . . 5996 7 10 . 1 1 17 17 GLY N N 15 . 1 1 17 17 GLY H H 1 0.75 0.03 . . . . . . . . . . 5996 7 11 . 1 1 18 18 GLU N N 15 . 1 1 18 18 GLU H H 1 0.73 0.03 . . . . . . . . . . 5996 7 12 . 1 1 19 19 TRP N N 15 . 1 1 19 19 TRP H H 1 0.73 0.05 . . . . . . . . . . 5996 7 13 . 1 1 20 20 HIS N N 15 . 1 1 20 20 HIS H H 1 0.70 0.04 . . . . . . . . . . 5996 7 14 . 1 1 22 22 ILE N N 15 . 1 1 22 22 ILE H H 1 0.74 0.03 . . . . . . . . . . 5996 7 15 . 1 1 23 23 ILE N N 15 . 1 1 23 23 ILE H H 1 0.76 0.04 . . . . . . . . . . 5996 7 16 . 1 1 26 26 SER N N 15 . 1 1 26 26 SER H H 1 0.76 0.02 . . . . . . . . . . 5996 7 17 . 1 1 27 27 ASP N N 15 . 1 1 27 27 ASP H H 1 0.73 0.04 . . . . . . . . . . 5996 7 18 . 1 1 29 29 ARG N N 15 . 1 1 29 29 ARG H H 1 0.73 0.03 . . . . . . . . . . 5996 7 19 . 1 1 30 30 GLU N N 15 . 1 1 30 30 GLU H H 1 0.74 0.03 . . . . . . . . . . 5996 7 20 . 1 1 31 31 LYS N N 15 . 1 1 31 31 LYS H H 1 0.61 0.04 . . . . . . . . . . 5996 7 21 . 1 1 32 32 ILE N N 15 . 1 1 32 32 ILE H H 1 0.73 0.04 . . . . . . . . . . 5996 7 22 . 1 1 33 33 GLU N N 15 . 1 1 33 33 GLU H H 1 0.78 0.03 . . . . . . . . . . 5996 7 23 . 1 1 36 36 GLY N N 15 . 1 1 36 36 GLY H H 1 0.72 0.04 . . . . . . . . . . 5996 7 24 . 1 1 37 37 ASN N N 15 . 1 1 37 37 ASN H H 1 0.74 0.03 . . . . . . . . . . 5996 7 25 . 1 1 39 39 ARG N N 15 . 1 1 39 39 ARG H H 1 0.82 0.10 . . . . . . . . . . 5996 7 26 . 1 1 40 40 LEU N N 15 . 1 1 40 40 LEU H H 1 0.77 0.03 . . . . . . . . . . 5996 7 27 . 1 1 45 45 ILE N N 15 . 1 1 45 45 ILE H H 1 0.69 0.03 . . . . . . . . . . 5996 7 28 . 1 1 46 46 HIS N N 15 . 1 1 46 46 HIS H H 1 0.72 0.04 . . . . . . . . . . 5996 7 29 . 1 1 47 47 VAL N N 15 . 1 1 47 47 VAL H H 1 0.73 0.04 . . . . . . . . . . 5996 7 30 . 1 1 48 48 LEU N N 15 . 1 1 48 48 LEU H H 1 0.75 0.04 . . . . . . . . . . 5996 7 31 . 1 1 50 50 ASN N N 15 . 1 1 50 50 ASN H H 1 0.64 0.01 . . . . . . . . . . 5996 7 32 . 1 1 51 51 SER N N 15 . 1 1 51 51 SER H H 1 0.64 0.03 . . . . . . . . . . 5996 7 33 . 1 1 52 52 LEU N N 15 . 1 1 52 52 LEU H H 1 0.78 0.04 . . . . . . . . . . 5996 7 34 . 1 1 54 54 LEU N N 15 . 1 1 54 54 LEU H H 1 0.80 0.06 . . . . . . . . . . 5996 7 35 . 1 1 58 58 THR N N 15 . 1 1 58 58 THR H H 1 0.79 0.06 . . . . . . . . . . 5996 7 36 . 1 1 60 60 ARG N N 15 . 1 1 60 60 ARG H H 1 0.66 0.00 . . . . . . . . . . 5996 7 37 . 1 1 61 61 ASP N N 15 . 1 1 61 61 ASP H H 1 0.69 0.05 . . . . . . . . . . 5996 7 38 . 1 1 62 62 GLU N N 15 . 1 1 62 62 GLU H H 1 0.62 0.03 . . . . . . . . . . 5996 7 39 . 1 1 64 64 CYS N N 15 . 1 1 64 64 CYS H H 1 0.63 0.03 . . . . . . . . . . 5996 7 40 . 1 1 66 66 GLU N N 15 . 1 1 66 66 GLU H H 1 0.63 0.04 . . . . . . . . . . 5996 7 41 . 1 1 67 67 LEU N N 15 . 1 1 67 67 LEU H H 1 0.75 0.03 . . . . . . . . . . 5996 7 42 . 1 1 68 68 SER N N 15 . 1 1 68 68 SER H H 1 0.69 0.03 . . . . . . . . . . 5996 7 43 . 1 1 69 69 MET N N 15 . 1 1 69 69 MET H H 1 0.73 0.05 . . . . . . . . . . 5996 7 44 . 1 1 71 71 ALA N N 15 . 1 1 71 71 ALA H H 1 0.77 0.04 . . . . . . . . . . 5996 7 45 . 1 1 72 72 ASP N N 15 . 1 1 72 72 ASP H H 1 0.72 0.03 . . . . . . . . . . 5996 7 46 . 1 1 74 74 THR N N 15 . 1 1 74 74 THR H H 1 0.72 0.06 . . . . . . . . . . 5996 7 47 . 1 1 75 75 GLU N N 15 . 1 1 75 75 GLU H H 1 0.62 0.03 . . . . . . . . . . 5996 7 48 . 1 1 77 77 ALA N N 15 . 1 1 77 77 ALA H H 1 0.65 0.04 . . . . . . . . . . 5996 7 49 . 1 1 78 78 GLY N N 15 . 1 1 78 78 GLY H H 1 0.60 0.03 . . . . . . . . . . 5996 7 50 . 1 1 79 79 GLU N N 15 . 1 1 79 79 GLU H H 1 0.71 0.04 . . . . . . . . . . 5996 7 51 . 1 1 80 80 TYR N N 15 . 1 1 80 80 TYR H H 1 0.75 0.03 . . . . . . . . . . 5996 7 52 . 1 1 81 81 SER N N 15 . 1 1 81 81 SER H H 1 0.76 0.03 . . . . . . . . . . 5996 7 53 . 1 1 82 82 VAL N N 15 . 1 1 82 82 VAL H H 1 0.75 0.04 . . . . . . . . . . 5996 7 54 . 1 1 84 84 TYR N N 15 . 1 1 84 84 TYR H H 1 0.76 0.04 . . . . . . . . . . 5996 7 55 . 1 1 85 85 ASP N N 15 . 1 1 85 85 ASP H H 1 0.73 0.04 . . . . . . . . . . 5996 7 56 . 1 1 86 86 GLY N N 15 . 1 1 86 86 GLY H H 1 0.73 0.03 . . . . . . . . . . 5996 7 57 . 1 1 87 87 PHE N N 15 . 1 1 87 87 PHE H H 1 0.74 0.02 . . . . . . . . . . 5996 7 58 . 1 1 89 89 THR N N 15 . 1 1 89 89 THR H H 1 0.79 0.03 . . . . . . . . . . 5996 7 59 . 1 1 90 90 PHE N N 15 . 1 1 90 90 PHE H H 1 0.78 0.07 . . . . . . . . . . 5996 7 60 . 1 1 91 91 THR N N 15 . 1 1 91 91 THR H H 1 0.71 0.03 . . . . . . . . . . 5996 7 61 . 1 1 94 94 LYS N N 15 . 1 1 94 94 LYS H H 1 0.70 0.03 . . . . . . . . . . 5996 7 62 . 1 1 95 95 THR N N 15 . 1 1 95 95 THR H H 1 0.69 0.04 . . . . . . . . . . 5996 7 63 . 1 1 96 96 ASP N N 15 . 1 1 96 96 ASP H H 1 0.78 0.04 . . . . . . . . . . 5996 7 64 . 1 1 98 98 ASP N N 15 . 1 1 98 98 ASP H H 1 0.78 0.02 . . . . . . . . . . 5996 7 65 . 1 1 100 100 PHE N N 15 . 1 1 100 100 PHE H H 1 0.76 0.04 . . . . . . . . . . 5996 7 66 . 1 1 103 103 ALA N N 15 . 1 1 103 103 ALA H H 1 0.74 0.03 . . . . . . . . . . 5996 7 67 . 1 1 105 105 LEU N N 15 . 1 1 105 105 LEU H H 1 0.86 0.04 . . . . . . . . . . 5996 7 68 . 1 1 107 107 ASN N N 15 . 1 1 107 107 ASN H H 1 0.79 0.05 . . . . . . . . . . 5996 7 69 . 1 1 108 108 GLU N N 15 . 1 1 108 108 GLU H H 1 0.78 0.03 . . . . . . . . . . 5996 7 70 . 1 1 109 109 LYS N N 15 . 1 1 109 109 LYS H H 1 0.72 0.03 . . . . . . . . . . 5996 7 71 . 1 1 110 110 ASP N N 15 . 1 1 110 110 ASP H H 1 0.67 0.04 . . . . . . . . . . 5996 7 72 . 1 1 111 111 GLY N N 15 . 1 1 111 111 GLY H H 1 0.68 0.03 . . . . . . . . . . 5996 7 73 . 1 1 115 115 GLN N N 15 . 1 1 115 115 GLN H H 1 0.76 0.04 . . . . . . . . . . 5996 7 74 . 1 1 117 117 MET N N 15 . 1 1 117 117 MET H H 1 0.77 0.05 . . . . . . . . . . 5996 7 75 . 1 1 118 118 GLY N N 15 . 1 1 118 118 GLY H H 1 0.76 0.05 . . . . . . . . . . 5996 7 76 . 1 1 121 121 GLY N N 15 . 1 1 121 121 GLY H H 1 0.78 0.03 . . . . . . . . . . 5996 7 77 . 1 1 123 123 GLU N N 15 . 1 1 123 123 GLU H H 1 0.68 0.05 . . . . . . . . . . 5996 7 78 . 1 1 125 125 ASP N N 15 . 1 1 125 125 ASP H H 1 0.71 0.03 . . . . . . . . . . 5996 7 79 . 1 1 126 126 LEU N N 15 . 1 1 126 126 LEU H H 1 0.22 0.04 . . . . . . . . . . 5996 7 80 . 1 1 127 127 SER N N 15 . 1 1 127 127 SER H H 1 0.74 0.04 . . . . . . . . . . 5996 7 81 . 1 1 128 128 SER N N 15 . 1 1 128 128 SER H H 1 0.72 0.05 . . . . . . . . . . 5996 7 82 . 1 1 130 130 ILE N N 15 . 1 1 130 130 ILE H H 1 0.74 0.04 . . . . . . . . . . 5996 7 83 . 1 1 131 131 LYS N N 15 . 1 1 131 131 LYS H H 1 0.75 0.05 . . . . . . . . . . 5996 7 84 . 1 1 133 133 ARG N N 15 . 1 1 133 133 ARG H H 1 0.77 0.05 . . . . . . . . . . 5996 7 85 . 1 1 136 136 GLN N N 15 . 1 1 136 136 GLN H H 1 0.78 0.04 . . . . . . . . . . 5996 7 86 . 1 1 137 137 LEU N N 15 . 1 1 137 137 LEU H H 1 0.74 0.03 . . . . . . . . . . 5996 7 87 . 1 1 138 138 CYS N N 15 . 1 1 138 138 CYS H H 1 0.77 0.04 . . . . . . . . . . 5996 7 88 . 1 1 140 140 LYS N N 15 . 1 1 140 140 LYS H H 1 0.78 0.04 . . . . . . . . . . 5996 7 89 . 1 1 141 141 HIS N N 15 . 1 1 141 141 HIS H H 1 0.69 0.04 . . . . . . . . . . 5996 7 90 . 1 1 142 142 GLY N N 15 . 1 1 142 142 GLY H H 1 0.72 0.03 . . . . . . . . . . 5996 7 91 . 1 1 144 144 LEU N N 15 . 1 1 144 144 LEU H H 1 0.67 0.05 . . . . . . . . . . 5996 7 92 . 1 1 145 145 ARG N N 15 . 1 1 145 145 ARG H H 1 0.66 0.05 . . . . . . . . . . 5996 7 93 . 1 1 146 146 GLU N N 15 . 1 1 146 146 GLU H H 1 0.71 0.03 . . . . . . . . . . 5996 7 94 . 1 1 148 148 ILE N N 15 . 1 1 148 148 ILE H H 1 0.73 0.03 . . . . . . . . . . 5996 7 95 . 1 1 150 150 ASP N N 15 . 1 1 150 150 ASP H H 1 0.74 0.04 . . . . . . . . . . 5996 7 96 . 1 1 151 151 LEU N N 15 . 1 1 151 151 LEU H H 1 0.74 0.04 . . . . . . . . . . 5996 7 97 . 1 1 152 152 SER N N 15 . 1 1 152 152 SER H H 1 0.78 0.03 . . . . . . . . . . 5996 7 98 . 1 1 153 153 ASN N N 15 . 1 1 153 153 ASN H H 1 0.70 0.03 . . . . . . . . . . 5996 7 99 . 1 1 155 155 ASN N N 15 . 1 1 155 155 ASN H H 1 0.53 0.03 . . . . . . . . . . 5996 7 100 . 1 1 160 160 ALA N N 15 . 1 1 160 160 ALA H H 1 -0.07 0.04 . . . . . . . . . . 5996 7 101 . 1 1 162 162 GLU N N 15 . 1 1 162 162 GLU H H 1 -0.54 0.03 . . . . . . . . . . 5996 7 stop_ save_ save_297_500_bound_noe _Heteronucl_NOE_list.Sf_category heteronucl_NOEs _Heteronucl_NOE_list.Sf_framecode 297_500_bound_noe _Heteronucl_NOE_list.Entry_ID 5996 _Heteronucl_NOE_list.ID 8 _Heteronucl_NOE_list.Sample_condition_list_ID 8 _Heteronucl_NOE_list.Sample_condition_list_label $297K _Heteronucl_NOE_list.Spectrometer_frequency_1H 500 _Heteronucl_NOE_list.Heteronuclear_NOE_val_type 'relative intensities' _Heteronucl_NOE_list.NOE_ref_val . _Heteronucl_NOE_list.NOE_ref_description . _Heteronucl_NOE_list.Details . _Heteronucl_NOE_list.Text_data_format . _Heteronucl_NOE_list.Text_data . loop_ _Heteronucl_NOE_experiment.Experiment_ID _Heteronucl_NOE_experiment.Experiment_name _Heteronucl_NOE_experiment.Sample_ID _Heteronucl_NOE_experiment.Sample_label _Heteronucl_NOE_experiment.Sample_state _Heteronucl_NOE_experiment.Entry_ID _Heteronucl_NOE_experiment.Heteronucl_NOE_list_ID 3 '{1H}-15N NOE' 1 $sample_1 . 5996 8 stop_ loop_ _Heteronucl_NOE.ID _Heteronucl_NOE.Assembly_atom_ID_1 _Heteronucl_NOE.Entity_assembly_ID_1 _Heteronucl_NOE.Entity_ID_1 _Heteronucl_NOE.Comp_index_ID_1 _Heteronucl_NOE.Seq_ID_1 _Heteronucl_NOE.Comp_ID_1 _Heteronucl_NOE.Atom_ID_1 _Heteronucl_NOE.Atom_type_1 _Heteronucl_NOE.Atom_isotope_number_1 _Heteronucl_NOE.Assembly_atom_ID_2 _Heteronucl_NOE.Entity_assembly_ID_2 _Heteronucl_NOE.Entity_ID_2 _Heteronucl_NOE.Comp_index_ID_2 _Heteronucl_NOE.Seq_ID_2 _Heteronucl_NOE.Comp_ID_2 _Heteronucl_NOE.Atom_ID_2 _Heteronucl_NOE.Atom_type_2 _Heteronucl_NOE.Atom_isotope_number_2 _Heteronucl_NOE.Val _Heteronucl_NOE.Val_err _Heteronucl_NOE.Resonance_ID_1 _Heteronucl_NOE.Resonance_ID_2 _Heteronucl_NOE.Auth_entity_assembly_ID_1 _Heteronucl_NOE.Auth_seq_ID_1 _Heteronucl_NOE.Auth_comp_ID_1 _Heteronucl_NOE.Auth_atom_ID_1 _Heteronucl_NOE.Auth_entity_assembly_ID_2 _Heteronucl_NOE.Auth_seq_ID_2 _Heteronucl_NOE.Auth_comp_ID_2 _Heteronucl_NOE.Auth_atom_ID_2 _Heteronucl_NOE.Entry_ID _Heteronucl_NOE.Heteronucl_NOE_list_ID 1 . 1 1 3 3 ALA N N 15 . 1 1 3 3 ALA H H 1 0.63 0.02 . . . . . . . . . . 5996 8 2 . 1 1 4 4 SER N N 15 . 1 1 4 4 SER H H 1 0.68 0.01 . . . . . . . . . . 5996 8 3 . 1 1 5 5 SER N N 15 . 1 1 5 5 SER H H 1 0.76 0.02 . . . . . . . . . . 5996 8 4 . 1 1 6 6 THR N N 15 . 1 1 6 6 THR H H 1 0.72 0.01 . . . . . . . . . . 5996 8 5 . 1 1 7 7 GLY N N 15 . 1 1 7 7 GLY H H 1 0.62 0.01 . . . . . . . . . . 5996 8 6 . 1 1 10 10 PHE N N 15 . 1 1 10 10 PHE H H 1 0.51 0.00 . . . . . . . . . . 5996 8 7 . 1 1 11 11 ASN N N 15 . 1 1 11 11 ASN H H 1 0.73 0.01 . . . . . . . . . . 5996 8 8 . 1 1 12 12 VAL N N 15 . 1 1 12 12 VAL H H 1 0.74 0.02 . . . . . . . . . . 5996 8 9 . 1 1 13 13 GLU N N 15 . 1 1 13 13 GLU H H 1 0.71 0.01 . . . . . . . . . . 5996 8 10 . 1 1 15 15 ILE N N 15 . 1 1 15 15 ILE H H 1 0.76 0.03 . . . . . . . . . . 5996 8 11 . 1 1 16 16 ASN N N 15 . 1 1 16 16 ASN H H 1 0.78 0.01 . . . . . . . . . . 5996 8 12 . 1 1 17 17 GLY N N 15 . 1 1 17 17 GLY H H 1 0.76 0.02 . . . . . . . . . . 5996 8 13 . 1 1 18 18 GLU N N 15 . 1 1 18 18 GLU H H 1 0.61 0.01 . . . . . . . . . . 5996 8 14 . 1 1 19 19 TRP N N 15 . 1 1 19 19 TRP H H 1 0.74 0.03 . . . . . . . . . . 5996 8 15 . 1 1 20 20 HIS N N 15 . 1 1 20 20 HIS H H 1 0.72 0.02 . . . . . . . . . . 5996 8 16 . 1 1 21 21 THR N N 15 . 1 1 21 21 THR H H 1 0.75 0.01 . . . . . . . . . . 5996 8 17 . 1 1 22 22 ILE N N 15 . 1 1 22 22 ILE H H 1 0.70 0.00 . . . . . . . . . . 5996 8 18 . 1 1 23 23 ILE N N 15 . 1 1 23 23 ILE H H 1 0.74 0.01 . . . . . . . . . . 5996 8 19 . 1 1 26 26 SER N N 15 . 1 1 26 26 SER H H 1 0.75 0.00 . . . . . . . . . . 5996 8 20 . 1 1 27 27 ASP N N 15 . 1 1 27 27 ASP H H 1 0.73 0.01 . . . . . . . . . . 5996 8 21 . 1 1 29 29 ARG N N 15 . 1 1 29 29 ARG H H 1 0.75 0.02 . . . . . . . . . . 5996 8 22 . 1 1 30 30 GLU N N 15 . 1 1 30 30 GLU H H 1 0.71 0.02 . . . . . . . . . . 5996 8 23 . 1 1 31 31 LYS N N 15 . 1 1 31 31 LYS H H 1 0.69 0.00 . . . . . . . . . . 5996 8 24 . 1 1 32 32 ILE N N 15 . 1 1 32 32 ILE H H 1 0.79 0.00 . . . . . . . . . . 5996 8 25 . 1 1 33 33 GLU N N 15 . 1 1 33 33 GLU H H 1 0.75 0.01 . . . . . . . . . . 5996 8 26 . 1 1 36 36 GLY N N 15 . 1 1 36 36 GLY H H 1 0.73 0.02 . . . . . . . . . . 5996 8 27 . 1 1 37 37 ASN N N 15 . 1 1 37 37 ASN H H 1 0.72 0.01 . . . . . . . . . . 5996 8 28 . 1 1 42 42 LEU N N 15 . 1 1 42 42 LEU H H 1 0.73 0.07 . . . . . . . . . . 5996 8 29 . 1 1 43 43 GLU N N 15 . 1 1 43 43 GLU H H 1 0.74 0.02 . . . . . . . . . . 5996 8 30 . 1 1 45 45 ILE N N 15 . 1 1 45 45 ILE H H 1 0.75 0.01 . . . . . . . . . . 5996 8 31 . 1 1 46 46 HIS N N 15 . 1 1 46 46 HIS H H 1 0.73 0.02 . . . . . . . . . . 5996 8 32 . 1 1 47 47 VAL N N 15 . 1 1 47 47 VAL H H 1 0.72 0.01 . . . . . . . . . . 5996 8 33 . 1 1 48 48 LEU N N 15 . 1 1 48 48 LEU H H 1 0.72 0.03 . . . . . . . . . . 5996 8 34 . 1 1 50 50 ASN N N 15 . 1 1 50 50 ASN H H 1 0.64 0.01 . . . . . . . . . . 5996 8 35 . 1 1 51 51 SER N N 15 . 1 1 51 51 SER H H 1 0.67 0.01 . . . . . . . . . . 5996 8 36 . 1 1 52 52 LEU N N 15 . 1 1 52 52 LEU H H 1 0.72 0.02 . . . . . . . . . . 5996 8 37 . 1 1 54 54 LEU N N 15 . 1 1 54 54 LEU H H 1 0.75 0.04 . . . . . . . . . . 5996 8 38 . 1 1 57 57 HIS N N 15 . 1 1 57 57 HIS H H 1 0.77 0.02 . . . . . . . . . . 5996 8 39 . 1 1 58 58 THR N N 15 . 1 1 58 58 THR H H 1 0.74 0.04 . . . . . . . . . . 5996 8 40 . 1 1 60 60 ARG N N 15 . 1 1 60 60 ARG H H 1 0.65 0.00 . . . . . . . . . . 5996 8 41 . 1 1 62 62 GLU N N 15 . 1 1 62 62 GLU H H 1 0.66 0.03 . . . . . . . . . . 5996 8 42 . 1 1 64 64 CYS N N 15 . 1 1 64 64 CYS H H 1 0.61 0.02 . . . . . . . . . . 5996 8 43 . 1 1 65 65 SER N N 15 . 1 1 65 65 SER H H 1 0.73 0.02 . . . . . . . . . . 5996 8 44 . 1 1 66 66 GLU N N 15 . 1 1 66 66 GLU H H 1 0.66 0.00 . . . . . . . . . . 5996 8 45 . 1 1 67 67 LEU N N 15 . 1 1 67 67 LEU H H 1 0.72 0.02 . . . . . . . . . . 5996 8 46 . 1 1 68 68 SER N N 15 . 1 1 68 68 SER H H 1 0.70 0.00 . . . . . . . . . . 5996 8 47 . 1 1 69 69 MET N N 15 . 1 1 69 69 MET H H 1 0.73 0.03 . . . . . . . . . . 5996 8 48 . 1 1 71 71 ALA N N 15 . 1 1 71 71 ALA H H 1 0.74 0.01 . . . . . . . . . . 5996 8 49 . 1 1 74 74 THR N N 15 . 1 1 74 74 THR H H 1 0.66 0.04 . . . . . . . . . . 5996 8 50 . 1 1 75 75 GLU N N 15 . 1 1 75 75 GLU H H 1 0.65 0.01 . . . . . . . . . . 5996 8 51 . 1 1 77 77 ALA N N 15 . 1 1 77 77 ALA H H 1 0.66 0.00 . . . . . . . . . . 5996 8 52 . 1 1 78 78 GLY N N 15 . 1 1 78 78 GLY H H 1 0.64 0.02 . . . . . . . . . . 5996 8 53 . 1 1 79 79 GLU N N 15 . 1 1 79 79 GLU H H 1 0.78 0.01 . . . . . . . . . . 5996 8 54 . 1 1 80 80 TYR N N 15 . 1 1 80 80 TYR H H 1 0.72 0.02 . . . . . . . . . . 5996 8 55 . 1 1 81 81 SER N N 15 . 1 1 81 81 SER H H 1 0.76 0.02 . . . . . . . . . . 5996 8 56 . 1 1 82 82 VAL N N 15 . 1 1 82 82 VAL H H 1 0.72 0.00 . . . . . . . . . . 5996 8 57 . 1 1 84 84 TYR N N 15 . 1 1 84 84 TYR H H 1 0.73 0.00 . . . . . . . . . . 5996 8 58 . 1 1 85 85 ASP N N 15 . 1 1 85 85 ASP H H 1 0.73 0.02 . . . . . . . . . . 5996 8 59 . 1 1 87 87 PHE N N 15 . 1 1 87 87 PHE H H 1 0.77 0.01 . . . . . . . . . . 5996 8 60 . 1 1 89 89 THR N N 15 . 1 1 89 89 THR H H 1 0.77 0.00 . . . . . . . . . . 5996 8 61 . 1 1 90 90 PHE N N 15 . 1 1 90 90 PHE H H 1 0.73 0.04 . . . . . . . . . . 5996 8 62 . 1 1 91 91 THR N N 15 . 1 1 91 91 THR H H 1 0.71 0.02 . . . . . . . . . . 5996 8 63 . 1 1 92 92 ILE N N 15 . 1 1 92 92 ILE H H 1 0.73 0.02 . . . . . . . . . . 5996 8 64 . 1 1 94 94 LYS N N 15 . 1 1 94 94 LYS H H 1 0.76 0.02 . . . . . . . . . . 5996 8 65 . 1 1 95 95 THR N N 15 . 1 1 95 95 THR H H 1 0.74 0.02 . . . . . . . . . . 5996 8 66 . 1 1 97 97 TYR N N 15 . 1 1 97 97 TYR H H 1 0.74 0.03 . . . . . . . . . . 5996 8 67 . 1 1 98 98 ASP N N 15 . 1 1 98 98 ASP H H 1 0.77 0.01 . . . . . . . . . . 5996 8 68 . 1 1 100 100 PHE N N 15 . 1 1 100 100 PHE H H 1 0.76 0.01 . . . . . . . . . . 5996 8 69 . 1 1 103 103 ALA N N 15 . 1 1 103 103 ALA H H 1 0.77 0.01 . . . . . . . . . . 5996 8 70 . 1 1 104 104 HIS N N 15 . 1 1 104 104 HIS H H 1 0.68 0.01 . . . . . . . . . . 5996 8 71 . 1 1 105 105 LEU N N 15 . 1 1 105 105 LEU H H 1 0.78 0.01 . . . . . . . . . . 5996 8 72 . 1 1 107 107 ASN N N 15 . 1 1 107 107 ASN H H 1 0.78 0.01 . . . . . . . . . . 5996 8 73 . 1 1 108 108 GLU N N 15 . 1 1 108 108 GLU H H 1 0.75 0.02 . . . . . . . . . . 5996 8 74 . 1 1 109 109 LYS N N 15 . 1 1 109 109 LYS H H 1 0.72 0.00 . . . . . . . . . . 5996 8 75 . 1 1 110 110 ASP N N 15 . 1 1 110 110 ASP H H 1 0.70 0.03 . . . . . . . . . . 5996 8 76 . 1 1 111 111 GLY N N 15 . 1 1 111 111 GLY H H 1 0.68 0.01 . . . . . . . . . . 5996 8 77 . 1 1 113 113 THR N N 15 . 1 1 113 113 THR H H 1 0.67 0.00 . . . . . . . . . . 5996 8 78 . 1 1 115 115 GLN N N 15 . 1 1 115 115 GLN H H 1 0.69 0.00 . . . . . . . . . . 5996 8 79 . 1 1 117 117 MET N N 15 . 1 1 117 117 MET H H 1 0.79 0.03 . . . . . . . . . . 5996 8 80 . 1 1 118 118 GLY N N 15 . 1 1 118 118 GLY H H 1 0.84 0.03 . . . . . . . . . . 5996 8 81 . 1 1 121 121 GLY N N 15 . 1 1 121 121 GLY H H 1 0.79 0.02 . . . . . . . . . . 5996 8 82 . 1 1 123 123 GLU N N 15 . 1 1 123 123 GLU H H 1 0.72 0.01 . . . . . . . . . . 5996 8 83 . 1 1 125 125 ASP N N 15 . 1 1 125 125 ASP H H 1 0.73 0.02 . . . . . . . . . . 5996 8 84 . 1 1 126 126 LEU N N 15 . 1 1 126 126 LEU H H 1 0.75 0.01 . . . . . . . . . . 5996 8 85 . 1 1 127 127 SER N N 15 . 1 1 127 127 SER H H 1 0.72 0.01 . . . . . . . . . . 5996 8 86 . 1 1 128 128 SER N N 15 . 1 1 128 128 SER H H 1 0.78 0.01 . . . . . . . . . . 5996 8 87 . 1 1 129 129 ASP N N 15 . 1 1 129 129 ASP H H 1 0.74 0.03 . . . . . . . . . . 5996 8 88 . 1 1 130 130 ILE N N 15 . 1 1 130 130 ILE H H 1 0.76 0.03 . . . . . . . . . . 5996 8 89 . 1 1 131 131 LYS N N 15 . 1 1 131 131 LYS H H 1 0.80 0.00 . . . . . . . . . . 5996 8 90 . 1 1 133 133 ARG N N 15 . 1 1 133 133 ARG H H 1 0.77 0.01 . . . . . . . . . . 5996 8 91 . 1 1 136 136 GLN N N 15 . 1 1 136 136 GLN H H 1 0.76 0.01 . . . . . . . . . . 5996 8 92 . 1 1 137 137 LEU N N 15 . 1 1 137 137 LEU H H 1 0.75 0.02 . . . . . . . . . . 5996 8 93 . 1 1 138 138 CYS N N 15 . 1 1 138 138 CYS H H 1 0.75 0.00 . . . . . . . . . . 5996 8 94 . 1 1 140 140 LYS N N 15 . 1 1 140 140 LYS H H 1 0.78 0.01 . . . . . . . . . . 5996 8 95 . 1 1 141 141 HIS N N 15 . 1 1 141 141 HIS H H 1 0.71 0.00 . . . . . . . . . . 5996 8 96 . 1 1 142 142 GLY N N 15 . 1 1 142 142 GLY H H 1 0.73 0.01 . . . . . . . . . . 5996 8 97 . 1 1 144 144 LEU N N 15 . 1 1 144 144 LEU H H 1 0.67 0.03 . . . . . . . . . . 5996 8 98 . 1 1 145 145 ARG N N 15 . 1 1 145 145 ARG H H 1 0.66 0.01 . . . . . . . . . . 5996 8 99 . 1 1 146 146 GLU N N 15 . 1 1 146 146 GLU H H 1 0.73 0.00 . . . . . . . . . . 5996 8 100 . 1 1 148 148 ILE N N 15 . 1 1 148 148 ILE H H 1 0.73 0.00 . . . . . . . . . . 5996 8 101 . 1 1 150 150 ASP N N 15 . 1 1 150 150 ASP H H 1 0.73 0.01 . . . . . . . . . . 5996 8 102 . 1 1 151 151 LEU N N 15 . 1 1 151 151 LEU H H 1 0.69 0.02 . . . . . . . . . . 5996 8 103 . 1 1 152 152 SER N N 15 . 1 1 152 152 SER H H 1 0.67 0.02 . . . . . . . . . . 5996 8 104 . 1 1 153 153 ASN N N 15 . 1 1 153 153 ASN H H 1 0.66 0.01 . . . . . . . . . . 5996 8 105 . 1 1 155 155 ASN N N 15 . 1 1 155 155 ASN H H 1 0.55 0.02 . . . . . . . . . . 5996 8 106 . 1 1 160 160 ALA N N 15 . 1 1 160 160 ALA H H 1 -0.13 0.01 . . . . . . . . . . 5996 8 107 . 1 1 162 162 GLU N N 15 . 1 1 162 162 GLU H H 1 -0.60 0.01 . . . . . . . . . . 5996 8 stop_ save_ save_302_500_bound_noe _Heteronucl_NOE_list.Sf_category heteronucl_NOEs _Heteronucl_NOE_list.Sf_framecode 302_500_bound_noe _Heteronucl_NOE_list.Entry_ID 5996 _Heteronucl_NOE_list.ID 9 _Heteronucl_NOE_list.Sample_condition_list_ID 9 _Heteronucl_NOE_list.Sample_condition_list_label $302K _Heteronucl_NOE_list.Spectrometer_frequency_1H 500 _Heteronucl_NOE_list.Heteronuclear_NOE_val_type 'relative intensities' _Heteronucl_NOE_list.NOE_ref_val . _Heteronucl_NOE_list.NOE_ref_description . _Heteronucl_NOE_list.Details . _Heteronucl_NOE_list.Text_data_format . _Heteronucl_NOE_list.Text_data . loop_ _Heteronucl_NOE_experiment.Experiment_ID _Heteronucl_NOE_experiment.Experiment_name _Heteronucl_NOE_experiment.Sample_ID _Heteronucl_NOE_experiment.Sample_label _Heteronucl_NOE_experiment.Sample_state _Heteronucl_NOE_experiment.Entry_ID _Heteronucl_NOE_experiment.Heteronucl_NOE_list_ID 3 '{1H}-15N NOE' 1 $sample_1 . 5996 9 stop_ loop_ _Heteronucl_NOE.ID _Heteronucl_NOE.Assembly_atom_ID_1 _Heteronucl_NOE.Entity_assembly_ID_1 _Heteronucl_NOE.Entity_ID_1 _Heteronucl_NOE.Comp_index_ID_1 _Heteronucl_NOE.Seq_ID_1 _Heteronucl_NOE.Comp_ID_1 _Heteronucl_NOE.Atom_ID_1 _Heteronucl_NOE.Atom_type_1 _Heteronucl_NOE.Atom_isotope_number_1 _Heteronucl_NOE.Assembly_atom_ID_2 _Heteronucl_NOE.Entity_assembly_ID_2 _Heteronucl_NOE.Entity_ID_2 _Heteronucl_NOE.Comp_index_ID_2 _Heteronucl_NOE.Seq_ID_2 _Heteronucl_NOE.Comp_ID_2 _Heteronucl_NOE.Atom_ID_2 _Heteronucl_NOE.Atom_type_2 _Heteronucl_NOE.Atom_isotope_number_2 _Heteronucl_NOE.Val _Heteronucl_NOE.Val_err _Heteronucl_NOE.Resonance_ID_1 _Heteronucl_NOE.Resonance_ID_2 _Heteronucl_NOE.Auth_entity_assembly_ID_1 _Heteronucl_NOE.Auth_seq_ID_1 _Heteronucl_NOE.Auth_comp_ID_1 _Heteronucl_NOE.Auth_atom_ID_1 _Heteronucl_NOE.Auth_entity_assembly_ID_2 _Heteronucl_NOE.Auth_seq_ID_2 _Heteronucl_NOE.Auth_comp_ID_2 _Heteronucl_NOE.Auth_atom_ID_2 _Heteronucl_NOE.Entry_ID _Heteronucl_NOE.Heteronucl_NOE_list_ID 1 . 1 1 3 3 ALA N N 15 . 1 1 3 3 ALA H H 1 0.61 0.01 . . . . . . . . . . 5996 9 2 . 1 1 4 4 SER N N 15 . 1 1 4 4 SER H H 1 0.65 0.01 . . . . . . . . . . 5996 9 3 . 1 1 6 6 THR N N 15 . 1 1 6 6 THR H H 1 0.78 0.11 . . . . . . . . . . 5996 9 4 . 1 1 10 10 PHE N N 15 . 1 1 10 10 PHE H H 1 0.55 0.02 . . . . . . . . . . 5996 9 5 . 1 1 11 11 ASN N N 15 . 1 1 11 11 ASN H H 1 0.74 0.03 . . . . . . . . . . 5996 9 6 . 1 1 12 12 VAL N N 15 . 1 1 12 12 VAL H H 1 0.70 0.01 . . . . . . . . . . 5996 9 7 . 1 1 13 13 GLU N N 15 . 1 1 13 13 GLU H H 1 0.76 0.01 . . . . . . . . . . 5996 9 8 . 1 1 16 16 ASN N N 15 . 1 1 16 16 ASN H H 1 0.77 0.05 . . . . . . . . . . 5996 9 9 . 1 1 17 17 GLY N N 15 . 1 1 17 17 GLY H H 1 0.76 0.03 . . . . . . . . . . 5996 9 10 . 1 1 18 18 GLU N N 15 . 1 1 18 18 GLU H H 1 0.72 0.01 . . . . . . . . . . 5996 9 11 . 1 1 19 19 TRP N N 15 . 1 1 19 19 TRP H H 1 0.66 0.11 . . . . . . . . . . 5996 9 12 . 1 1 21 21 THR N N 15 . 1 1 21 21 THR H H 1 0.69 0.18 . . . . . . . . . . 5996 9 13 . 1 1 22 22 ILE N N 15 . 1 1 22 22 ILE H H 1 0.77 0.05 . . . . . . . . . . 5996 9 14 . 1 1 23 23 ILE N N 15 . 1 1 23 23 ILE H H 1 0.73 0.02 . . . . . . . . . . 5996 9 15 . 1 1 26 26 SER N N 15 . 1 1 26 26 SER H H 1 0.73 0.02 . . . . . . . . . . 5996 9 16 . 1 1 27 27 ASP N N 15 . 1 1 27 27 ASP H H 1 0.75 0.02 . . . . . . . . . . 5996 9 17 . 1 1 29 29 ARG N N 15 . 1 1 29 29 ARG H H 1 0.71 0.01 . . . . . . . . . . 5996 9 18 . 1 1 30 30 GLU N N 15 . 1 1 30 30 GLU H H 1 0.71 0.03 . . . . . . . . . . 5996 9 19 . 1 1 31 31 LYS N N 15 . 1 1 31 31 LYS H H 1 0.59 0.02 . . . . . . . . . . 5996 9 20 . 1 1 32 32 ILE N N 15 . 1 1 32 32 ILE H H 1 0.76 0.06 . . . . . . . . . . 5996 9 21 . 1 1 33 33 GLU N N 15 . 1 1 33 33 GLU H H 1 0.71 0.02 . . . . . . . . . . 5996 9 22 . 1 1 35 35 ASN N N 15 . 1 1 35 35 ASN H H 1 0.67 0.03 . . . . . . . . . . 5996 9 23 . 1 1 36 36 GLY N N 15 . 1 1 36 36 GLY H H 1 0.73 0.03 . . . . . . . . . . 5996 9 24 . 1 1 39 39 ARG N N 15 . 1 1 39 39 ARG H H 1 0.81 0.11 . . . . . . . . . . 5996 9 25 . 1 1 40 40 LEU N N 15 . 1 1 40 40 LEU H H 1 0.70 0.04 . . . . . . . . . . 5996 9 26 . 1 1 42 42 LEU N N 15 . 1 1 42 42 LEU H H 1 0.73 0.10 . . . . . . . . . . 5996 9 27 . 1 1 43 43 GLU N N 15 . 1 1 43 43 GLU H H 1 0.73 0.01 . . . . . . . . . . 5996 9 28 . 1 1 46 46 HIS N N 15 . 1 1 46 46 HIS H H 1 0.75 0.01 . . . . . . . . . . 5996 9 29 . 1 1 47 47 VAL N N 15 . 1 1 47 47 VAL H H 1 0.78 0.01 . . . . . . . . . . 5996 9 30 . 1 1 48 48 LEU N N 15 . 1 1 48 48 LEU H H 1 0.72 0.02 . . . . . . . . . . 5996 9 31 . 1 1 50 50 ASN N N 15 . 1 1 50 50 ASN H H 1 0.70 0.03 . . . . . . . . . . 5996 9 32 . 1 1 51 51 SER N N 15 . 1 1 51 51 SER H H 1 0.60 0.01 . . . . . . . . . . 5996 9 33 . 1 1 52 52 LEU N N 15 . 1 1 52 52 LEU H H 1 0.77 0.01 . . . . . . . . . . 5996 9 34 . 1 1 54 54 LEU N N 15 . 1 1 54 54 LEU H H 1 0.76 0.02 . . . . . . . . . . 5996 9 35 . 1 1 60 60 ARG N N 15 . 1 1 60 60 ARG H H 1 0.64 0.01 . . . . . . . . . . 5996 9 36 . 1 1 61 61 ASP N N 15 . 1 1 61 61 ASP H H 1 0.67 0.03 . . . . . . . . . . 5996 9 37 . 1 1 62 62 GLU N N 15 . 1 1 62 62 GLU H H 1 0.62 0.01 . . . . . . . . . . 5996 9 38 . 1 1 64 64 CYS N N 15 . 1 1 64 64 CYS H H 1 0.61 0.01 . . . . . . . . . . 5996 9 39 . 1 1 65 65 SER N N 15 . 1 1 65 65 SER H H 1 0.67 0.02 . . . . . . . . . . 5996 9 40 . 1 1 66 66 GLU N N 15 . 1 1 66 66 GLU H H 1 0.67 0.02 . . . . . . . . . . 5996 9 41 . 1 1 67 67 LEU N N 15 . 1 1 67 67 LEU H H 1 0.68 0.01 . . . . . . . . . . 5996 9 42 . 1 1 68 68 SER N N 15 . 1 1 68 68 SER H H 1 0.72 0.01 . . . . . . . . . . 5996 9 43 . 1 1 69 69 MET N N 15 . 1 1 69 69 MET H H 1 0.76 0.01 . . . . . . . . . . 5996 9 44 . 1 1 71 71 ALA N N 15 . 1 1 71 71 ALA H H 1 0.75 0.02 . . . . . . . . . . 5996 9 45 . 1 1 74 74 THR N N 15 . 1 1 74 74 THR H H 1 0.64 0.05 . . . . . . . . . . 5996 9 46 . 1 1 75 75 GLU N N 15 . 1 1 75 75 GLU H H 1 0.65 0.01 . . . . . . . . . . 5996 9 47 . 1 1 77 77 ALA N N 15 . 1 1 77 77 ALA H H 1 0.67 0.02 . . . . . . . . . . 5996 9 48 . 1 1 79 79 GLU N N 15 . 1 1 79 79 GLU H H 1 0.77 0.07 . . . . . . . . . . 5996 9 49 . 1 1 81 81 SER N N 15 . 1 1 81 81 SER H H 1 0.73 0.01 . . . . . . . . . . 5996 9 50 . 1 1 82 82 VAL N N 15 . 1 1 82 82 VAL H H 1 0.70 0.01 . . . . . . . . . . 5996 9 51 . 1 1 84 84 TYR N N 15 . 1 1 84 84 TYR H H 1 0.81 0.09 . . . . . . . . . . 5996 9 52 . 1 1 85 85 ASP N N 15 . 1 1 85 85 ASP H H 1 0.76 0.02 . . . . . . . . . . 5996 9 53 . 1 1 86 86 GLY N N 15 . 1 1 86 86 GLY H H 1 0.73 0.03 . . . . . . . . . . 5996 9 54 . 1 1 88 88 ASN N N 15 . 1 1 88 88 ASN H H 1 0.74 0.01 . . . . . . . . . . 5996 9 55 . 1 1 89 89 THR N N 15 . 1 1 89 89 THR H H 1 0.76 0.01 . . . . . . . . . . 5996 9 56 . 1 1 90 90 PHE N N 15 . 1 1 90 90 PHE H H 1 0.72 0.01 . . . . . . . . . . 5996 9 57 . 1 1 91 91 THR N N 15 . 1 1 91 91 THR H H 1 0.75 0.04 . . . . . . . . . . 5996 9 58 . 1 1 94 94 LYS N N 15 . 1 1 94 94 LYS H H 1 0.73 0.04 . . . . . . . . . . 5996 9 59 . 1 1 96 96 ASP N N 15 . 1 1 96 96 ASP H H 1 0.77 0.01 . . . . . . . . . . 5996 9 60 . 1 1 97 97 TYR N N 15 . 1 1 97 97 TYR H H 1 0.75 0.03 . . . . . . . . . . 5996 9 61 . 1 1 98 98 ASP N N 15 . 1 1 98 98 ASP H H 1 0.77 0.02 . . . . . . . . . . 5996 9 62 . 1 1 99 99 ASN N N 15 . 1 1 99 99 ASN H H 1 0.70 0.03 . . . . . . . . . . 5996 9 63 . 1 1 100 100 PHE N N 15 . 1 1 100 100 PHE H H 1 0.73 0.03 . . . . . . . . . . 5996 9 64 . 1 1 101 101 LEU N N 15 . 1 1 101 101 LEU H H 1 0.77 0.01 . . . . . . . . . . 5996 9 65 . 1 1 103 103 ALA N N 15 . 1 1 103 103 ALA H H 1 0.75 0.04 . . . . . . . . . . 5996 9 66 . 1 1 104 104 HIS N N 15 . 1 1 104 104 HIS H H 1 0.72 0.01 . . . . . . . . . . 5996 9 67 . 1 1 105 105 LEU N N 15 . 1 1 105 105 LEU H H 1 0.74 0.02 . . . . . . . . . . 5996 9 68 . 1 1 107 107 ASN N N 15 . 1 1 107 107 ASN H H 1 0.76 0.02 . . . . . . . . . . 5996 9 69 . 1 1 108 108 GLU N N 15 . 1 1 108 108 GLU H H 1 0.75 0.03 . . . . . . . . . . 5996 9 70 . 1 1 110 110 ASP N N 15 . 1 1 110 110 ASP H H 1 0.75 0.03 . . . . . . . . . . 5996 9 71 . 1 1 111 111 GLY N N 15 . 1 1 111 111 GLY H H 1 0.67 0.01 . . . . . . . . . . 5996 9 72 . 1 1 113 113 THR N N 15 . 1 1 113 113 THR H H 1 0.70 0.02 . . . . . . . . . . 5996 9 73 . 1 1 115 115 GLN N N 15 . 1 1 115 115 GLN H H 1 0.77 0.04 . . . . . . . . . . 5996 9 74 . 1 1 116 116 LEU N N 15 . 1 1 116 116 LEU H H 1 0.73 0.03 . . . . . . . . . . 5996 9 75 . 1 1 117 117 MET N N 15 . 1 1 117 117 MET H H 1 0.75 0.01 . . . . . . . . . . 5996 9 76 . 1 1 121 121 GLY N N 15 . 1 1 121 121 GLY H H 1 0.77 0.01 . . . . . . . . . . 5996 9 77 . 1 1 125 125 ASP N N 15 . 1 1 125 125 ASP H H 1 0.68 0.03 . . . . . . . . . . 5996 9 78 . 1 1 127 127 SER N N 15 . 1 1 127 127 SER H H 1 0.70 0.02 . . . . . . . . . . 5996 9 79 . 1 1 128 128 SER N N 15 . 1 1 128 128 SER H H 1 0.72 0.03 . . . . . . . . . . 5996 9 80 . 1 1 129 129 ASP N N 15 . 1 1 129 129 ASP H H 1 0.71 0.02 . . . . . . . . . . 5996 9 81 . 1 1 130 130 ILE N N 15 . 1 1 130 130 ILE H H 1 0.73 0.04 . . . . . . . . . . 5996 9 82 . 1 1 131 131 LYS N N 15 . 1 1 131 131 LYS H H 1 0.82 0.01 . . . . . . . . . . 5996 9 83 . 1 1 133 133 ARG N N 15 . 1 1 133 133 ARG H H 1 0.78 0.03 . . . . . . . . . . 5996 9 84 . 1 1 136 136 GLN N N 15 . 1 1 136 136 GLN H H 1 0.73 0.02 . . . . . . . . . . 5996 9 85 . 1 1 137 137 LEU N N 15 . 1 1 137 137 LEU H H 1 0.77 0.02 . . . . . . . . . . 5996 9 86 . 1 1 138 138 CYS N N 15 . 1 1 138 138 CYS H H 1 0.86 0.01 . . . . . . . . . . 5996 9 87 . 1 1 140 140 LYS N N 15 . 1 1 140 140 LYS H H 1 0.75 0.06 . . . . . . . . . . 5996 9 88 . 1 1 141 141 HIS N N 15 . 1 1 141 141 HIS H H 1 0.73 0.01 . . . . . . . . . . 5996 9 89 . 1 1 142 142 GLY N N 15 . 1 1 142 142 GLY H H 1 0.72 0.02 . . . . . . . . . . 5996 9 90 . 1 1 144 144 LEU N N 15 . 1 1 144 144 LEU H H 1 0.70 0.01 . . . . . . . . . . 5996 9 91 . 1 1 145 145 ARG N N 15 . 1 1 145 145 ARG H H 1 0.66 0.01 . . . . . . . . . . 5996 9 92 . 1 1 146 146 GLU N N 15 . 1 1 146 146 GLU H H 1 0.72 0.01 . . . . . . . . . . 5996 9 93 . 1 1 148 148 ILE N N 15 . 1 1 148 148 ILE H H 1 0.75 0.02 . . . . . . . . . . 5996 9 94 . 1 1 150 150 ASP N N 15 . 1 1 150 150 ASP H H 1 0.72 0.03 . . . . . . . . . . 5996 9 95 . 1 1 151 151 LEU N N 15 . 1 1 151 151 LEU H H 1 0.75 0.01 . . . . . . . . . . 5996 9 96 . 1 1 152 152 SER N N 15 . 1 1 152 152 SER H H 1 0.75 0.03 . . . . . . . . . . 5996 9 97 . 1 1 153 153 ASN N N 15 . 1 1 153 153 ASN H H 1 0.71 0.02 . . . . . . . . . . 5996 9 98 . 1 1 155 155 ASN N N 15 . 1 1 155 155 ASN H H 1 0.62 0.02 . . . . . . . . . . 5996 9 99 . 1 1 160 160 ALA N N 15 . 1 1 160 160 ALA H H 1 -0.18 0.01 . . . . . . . . . . 5996 9 100 . 1 1 162 162 GLU N N 15 . 1 1 162 162 GLU H H 1 -0.73 0.01 . . . . . . . . . . 5996 9 stop_ save_ ######################################## # Heteronuclear T1 relaxation values # ######################################## save_283_600_bound_t1 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode 283_600_bound_t1 _Heteronucl_T1_list.Entry_ID 5996 _Heteronucl_T1_list.ID 1 _Heteronucl_T1_list.Sample_condition_list_ID 1 _Heteronucl_T1_list.Sample_condition_list_label $283K _Heteronucl_T1_list.Spectrometer_frequency_1H 600 _Heteronucl_T1_list.T1_coherence_type Nz _Heteronucl_T1_list.T1_val_units ms _Heteronucl_T1_list.Details . _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID 1 '15N T1' 1 $sample_1 . 5996 1 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 3 3 ALA N N 15 1137.0 9.67 . . . . . 5996 1 2 . 1 1 4 4 SER N N 15 1236.7 10.7 . . . . . 5996 1 3 . 1 1 5 5 SER N N 15 1106.1 13.0 . . . . . 5996 1 4 . 1 1 6 6 THR N N 15 1038.3 9.27 . . . . . 5996 1 5 . 1 1 7 7 GLY N N 15 1134.5 13.6 . . . . . 5996 1 6 . 1 1 10 10 PHE N N 15 1090.1 10.8 . . . . . 5996 1 7 . 1 1 11 11 ASN N N 15 1138.2 14.6 . . . . . 5996 1 8 . 1 1 12 12 VAL N N 15 1230.7 8.10 . . . . . 5996 1 9 . 1 1 13 13 GLU N N 15 1167.7 9.63 . . . . . 5996 1 10 . 1 1 15 15 ILE N N 15 1155.3 4.87 . . . . . 5996 1 11 . 1 1 16 16 ASN N N 15 1154.9 7.95 . . . . . 5996 1 12 . 1 1 17 17 GLY N N 15 1119.1 13.5 . . . . . 5996 1 13 . 1 1 18 18 GLU N N 15 775.08 14.1 . . . . . 5996 1 14 . 1 1 22 22 ILE N N 15 1097.5 11.2 . . . . . 5996 1 15 . 1 1 23 23 ILE N N 15 1198.3 13.5 . . . . . 5996 1 16 . 1 1 26 26 SER N N 15 1154.5 9.75 . . . . . 5996 1 17 . 1 1 27 27 ASP N N 15 1189.4 9.11 . . . . . 5996 1 18 . 1 1 29 29 ARG N N 15 1098.1 12.5 . . . . . 5996 1 19 . 1 1 30 30 GLU N N 15 1117.3 6.43 . . . . . 5996 1 20 . 1 1 31 31 LYS N N 15 1093.6 11.0 . . . . . 5996 1 21 . 1 1 32 32 ILE N N 15 1087.2 11.8 . . . . . 5996 1 22 . 1 1 33 33 GLU N N 15 1137.9 8.98 . . . . . 5996 1 23 . 1 1 36 36 GLY N N 15 1135.5 8.14 . . . . . 5996 1 24 . 1 1 37 37 ASN N N 15 1034.4 17.0 . . . . . 5996 1 25 . 1 1 38 38 PHE N N 15 1101.5 9.27 . . . . . 5996 1 26 . 1 1 46 46 HIS N N 15 1163.5 8.88 . . . . . 5996 1 27 . 1 1 48 48 LEU N N 15 1122.7 9.22 . . . . . 5996 1 28 . 1 1 50 50 ASN N N 15 1039.4 22.3 . . . . . 5996 1 29 . 1 1 51 51 SER N N 15 1071.6 7.00 . . . . . 5996 1 30 . 1 1 52 52 LEU N N 15 1152.8 12.9 . . . . . 5996 1 31 . 1 1 54 54 LEU N N 15 1137.6 7.89 . . . . . 5996 1 32 . 1 1 55 55 LYS N N 15 1190.6 10.4 . . . . . 5996 1 33 . 1 1 61 61 ASP N N 15 1088.9 6.18 . . . . . 5996 1 34 . 1 1 66 66 GLU N N 15 1125.9 8.93 . . . . . 5996 1 35 . 1 1 67 67 LEU N N 15 1087.2 10.4 . . . . . 5996 1 36 . 1 1 68 68 SER N N 15 1180.2 8.43 . . . . . 5996 1 37 . 1 1 70 70 VAL N N 15 1074.9 13.7 . . . . . 5996 1 38 . 1 1 71 71 ALA N N 15 1111.8 14.3 . . . . . 5996 1 39 . 1 1 72 72 ASP N N 15 1165.7 7.30 . . . . . 5996 1 40 . 1 1 74 74 THR N N 15 1112.0 8.31 . . . . . 5996 1 41 . 1 1 75 75 GLU N N 15 1089.1 13.6 . . . . . 5996 1 42 . 1 1 76 76 LYS N N 15 1184.5 19.0 . . . . . 5996 1 43 . 1 1 78 78 GLY N N 15 1049.3 22.7 . . . . . 5996 1 44 . 1 1 79 79 GLU N N 15 1081.7 5.82 . . . . . 5996 1 45 . 1 1 80 80 TYR N N 15 1101.0 14.1 . . . . . 5996 1 46 . 1 1 81 81 SER N N 15 1119.9 8.03 . . . . . 5996 1 47 . 1 1 82 82 VAL N N 15 1077.7 7.57 . . . . . 5996 1 48 . 1 1 84 84 TYR N N 15 1192.6 11.8 . . . . . 5996 1 49 . 1 1 85 85 ASP N N 15 1129.1 9.20 . . . . . 5996 1 50 . 1 1 86 86 GLY N N 15 1143.8 6.62 . . . . . 5996 1 51 . 1 1 89 89 THR N N 15 1136.4 14.4 . . . . . 5996 1 52 . 1 1 90 90 PHE N N 15 1246.7 8.10 . . . . . 5996 1 53 . 1 1 91 91 THR N N 15 1041.8 16.9 . . . . . 5996 1 54 . 1 1 92 92 ILE N N 15 1126.0 15.9 . . . . . 5996 1 55 . 1 1 94 94 LYS N N 15 1178.9 7.64 . . . . . 5996 1 56 . 1 1 96 96 ASP N N 15 1103.2 12.3 . . . . . 5996 1 57 . 1 1 98 98 ASP N N 15 1161.0 13.2 . . . . . 5996 1 58 . 1 1 100 100 PHE N N 15 1209.4 12.4 . . . . . 5996 1 59 . 1 1 101 101 LEU N N 15 1162.7 15.5 . . . . . 5996 1 60 . 1 1 103 103 ALA N N 15 1187.8 16.6 . . . . . 5996 1 61 . 1 1 104 104 HIS N N 15 1232.5 10.9 . . . . . 5996 1 62 . 1 1 105 105 LEU N N 15 1133.6 18.5 . . . . . 5996 1 63 . 1 1 107 107 ASN N N 15 1090.8 11.6 . . . . . 5996 1 64 . 1 1 108 108 GLU N N 15 1187.7 9.63 . . . . . 5996 1 65 . 1 1 109 109 LYS N N 15 1110.1 6.71 . . . . . 5996 1 66 . 1 1 110 110 ASP N N 15 1048.6 16.9 . . . . . 5996 1 67 . 1 1 111 111 GLY N N 15 1118.3 3.92 . . . . . 5996 1 68 . 1 1 113 113 THR N N 15 1148.7 6.11 . . . . . 5996 1 69 . 1 1 114 114 PHE N N 15 1129.0 7.26 . . . . . 5996 1 70 . 1 1 115 115 GLN N N 15 1127.3 8.57 . . . . . 5996 1 71 . 1 1 116 116 LEU N N 15 1216.6 18.4 . . . . . 5996 1 72 . 1 1 117 117 MET N N 15 1214.1 10.3 . . . . . 5996 1 73 . 1 1 118 118 GLY N N 15 1171.0 18.7 . . . . . 5996 1 74 . 1 1 119 119 LEU N N 15 1175.7 12.0 . . . . . 5996 1 75 . 1 1 121 121 GLY N N 15 1145.3 28.1 . . . . . 5996 1 76 . 1 1 123 123 GLU N N 15 1128.6 7.36 . . . . . 5996 1 77 . 1 1 125 125 ASP N N 15 1121.6 8.01 . . . . . 5996 1 78 . 1 1 126 126 LEU N N 15 1173.8 7.78 . . . . . 5996 1 79 . 1 1 127 127 SER N N 15 1186.5 8.03 . . . . . 5996 1 80 . 1 1 129 129 ASP N N 15 1122.2 16.7 . . . . . 5996 1 81 . 1 1 130 130 ILE N N 15 1107.8 10.0 . . . . . 5996 1 82 . 1 1 131 131 LYS N N 15 1099.7 10.7 . . . . . 5996 1 83 . 1 1 133 133 ARG N N 15 1105.5 7.39 . . . . . 5996 1 84 . 1 1 135 135 ALA N N 15 1087.8 9.72 . . . . . 5996 1 85 . 1 1 136 136 GLN N N 15 1133.0 15.9 . . . . . 5996 1 86 . 1 1 137 137 LEU N N 15 1122.6 7.71 . . . . . 5996 1 87 . 1 1 138 138 CYS N N 15 1144.1 6.79 . . . . . 5996 1 88 . 1 1 140 140 LYS N N 15 1158.2 4.47 . . . . . 5996 1 89 . 1 1 141 141 HIS N N 15 1177.9 4.74 . . . . . 5996 1 90 . 1 1 142 142 GLY N N 15 1142.2 15.0 . . . . . 5996 1 91 . 1 1 144 144 LEU N N 15 1149.3 6.77 . . . . . 5996 1 92 . 1 1 145 145 ARG N N 15 1039.6 33.4 . . . . . 5996 1 93 . 1 1 148 148 ILE N N 15 1149.3 8.22 . . . . . 5996 1 94 . 1 1 151 151 LEU N N 15 1206.2 18.2 . . . . . 5996 1 95 . 1 1 152 152 SER N N 15 1034.2 24.5 . . . . . 5996 1 96 . 1 1 162 162 GLU N N 15 780.81 2.53 . . . . . 5996 1 stop_ save_ save_288_600_bound_t1 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode 288_600_bound_t1 _Heteronucl_T1_list.Entry_ID 5996 _Heteronucl_T1_list.ID 2 _Heteronucl_T1_list.Sample_condition_list_ID 2 _Heteronucl_T1_list.Sample_condition_list_label $288K _Heteronucl_T1_list.Spectrometer_frequency_1H 600 _Heteronucl_T1_list.T1_coherence_type Nz _Heteronucl_T1_list.T1_val_units ms _Heteronucl_T1_list.Details . _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID 1 '15N T1' 1 $sample_1 . 5996 2 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 3 3 ALA N N 15 990.62 16.19 . . . . . 5996 2 2 . 1 1 4 4 SER N N 15 1052.2 24.91 . . . . . 5996 2 3 . 1 1 5 5 SER N N 15 942.42 21.21 . . . . . 5996 2 4 . 1 1 6 6 THR N N 15 850.56 13.42 . . . . . 5996 2 5 . 1 1 7 7 GLY N N 15 934.16 16.47 . . . . . 5996 2 6 . 1 1 10 10 PHE N N 15 932.30 20.92 . . . . . 5996 2 7 . 1 1 12 12 VAL N N 15 1049.3 24.10 . . . . . 5996 2 8 . 1 1 13 13 GLU N N 15 976.89 8.23 . . . . . 5996 2 9 . 1 1 15 15 ILE N N 15 952.45 11.77 . . . . . 5996 2 10 . 1 1 16 16 ASN N N 15 953.33 12.42 . . . . . 5996 2 11 . 1 1 17 17 GLY N N 15 929.62 19.75 . . . . . 5996 2 12 . 1 1 18 18 GLU N N 15 941.97 15.31 . . . . . 5996 2 13 . 1 1 19 19 TRP N N 15 1004.4 16.63 . . . . . 5996 2 14 . 1 1 20 20 HIS N N 15 1005.9 16.06 . . . . . 5996 2 15 . 1 1 21 21 THR N N 15 983.27 27.16 . . . . . 5996 2 16 . 1 1 22 22 ILE N N 15 959.97 25.96 . . . . . 5996 2 17 . 1 1 23 23 ILE N N 15 954.21 13.44 . . . . . 5996 2 18 . 1 1 26 26 SER N N 15 986.47 9.49 . . . . . 5996 2 19 . 1 1 27 27 ASP N N 15 899.49 5.73 . . . . . 5996 2 20 . 1 1 29 29 ARG N N 15 942.24 17.82 . . . . . 5996 2 21 . 1 1 30 30 GLU N N 15 945.79 11.34 . . . . . 5996 2 22 . 1 1 31 31 LYS N N 15 898.87 14.48 . . . . . 5996 2 23 . 1 1 32 32 ILE N N 15 902.43 11.59 . . . . . 5996 2 24 . 1 1 33 33 GLU N N 15 951.69 14.39 . . . . . 5996 2 25 . 1 1 35 35 ASN N N 15 970.09 10.49 . . . . . 5996 2 26 . 1 1 36 36 GLY N N 15 1009.7 18.78 . . . . . 5996 2 27 . 1 1 37 37 ASN N N 15 871.56 35.77 . . . . . 5996 2 28 . 1 1 38 38 PHE N N 15 889.80 8.01 . . . . . 5996 2 29 . 1 1 39 39 ARG N N 15 935.96 15.75 . . . . . 5996 2 30 . 1 1 40 40 LEU N N 15 1019.4 11.24 . . . . . 5996 2 31 . 1 1 42 42 LEU N N 15 958.65 27.93 . . . . . 5996 2 32 . 1 1 45 45 ILE N N 15 999.69 17.13 . . . . . 5996 2 33 . 1 1 46 46 HIS N N 15 960.13 9.45 . . . . . 5996 2 34 . 1 1 48 48 LEU N N 15 947.17 15.06 . . . . . 5996 2 35 . 1 1 50 50 ASN N N 15 889.86 32.58 . . . . . 5996 2 36 . 1 1 51 51 SER N N 15 900.95 8.97 . . . . . 5996 2 37 . 1 1 52 52 LEU N N 15 962.72 14.40 . . . . . 5996 2 38 . 1 1 53 53 VAL N N 15 953.86 15.97 . . . . . 5996 2 39 . 1 1 54 54 LEU N N 15 942.59 17.14 . . . . . 5996 2 40 . 1 1 55 55 LYS N N 15 990.98 9.52 . . . . . 5996 2 41 . 1 1 57 57 HIS N N 15 954.13 18.66 . . . . . 5996 2 42 . 1 1 60 60 ARG N N 15 946.67 7.78 . . . . . 5996 2 43 . 1 1 61 61 ASP N N 15 920.41 24.79 . . . . . 5996 2 44 . 1 1 62 62 GLU N N 15 944.22 15.76 . . . . . 5996 2 45 . 1 1 64 64 CYS N N 15 992.33 24.65 . . . . . 5996 2 46 . 1 1 66 66 GLU N N 15 993.34 21.51 . . . . . 5996 2 47 . 1 1 67 67 LEU N N 15 925.46 11.14 . . . . . 5996 2 48 . 1 1 68 68 SER N N 15 1002.8 13.30 . . . . . 5996 2 49 . 1 1 69 69 MET N N 15 1004.2 11.90 . . . . . 5996 2 50 . 1 1 71 71 ALA N N 15 937.03 15.97 . . . . . 5996 2 51 . 1 1 72 72 ASP N N 15 1001.0 16.09 . . . . . 5996 2 52 . 1 1 74 74 THR N N 15 983.53 17.92 . . . . . 5996 2 53 . 1 1 75 75 GLU N N 15 930.62 17.50 . . . . . 5996 2 54 . 1 1 77 77 ALA N N 15 1004.9 30.61 . . . . . 5996 2 55 . 1 1 78 78 GLY N N 15 895.39 36.36 . . . . . 5996 2 56 . 1 1 79 79 GLU N N 15 913.95 13.17 . . . . . 5996 2 57 . 1 1 80 80 TYR N N 15 944.20 8.68 . . . . . 5996 2 58 . 1 1 81 81 SER N N 15 942.19 17.12 . . . . . 5996 2 59 . 1 1 82 82 VAL N N 15 916.84 6.04 . . . . . 5996 2 60 . 1 1 84 84 TYR N N 15 992.26 17.56 . . . . . 5996 2 61 . 1 1 85 85 ASP N N 15 954.63 14.61 . . . . . 5996 2 62 . 1 1 86 86 GLY N N 15 957.83 13.23 . . . . . 5996 2 63 . 1 1 87 87 PHE N N 15 950.40 12.90 . . . . . 5996 2 64 . 1 1 88 88 ASN N N 15 989.46 10.67 . . . . . 5996 2 65 . 1 1 89 89 THR N N 15 936.57 9.99 . . . . . 5996 2 66 . 1 1 90 90 PHE N N 15 1077.6 17.44 . . . . . 5996 2 67 . 1 1 91 91 THR N N 15 896.26 15.09 . . . . . 5996 2 68 . 1 1 92 92 ILE N N 15 995.62 13.25 . . . . . 5996 2 69 . 1 1 94 94 LYS N N 15 981.91 13.26 . . . . . 5996 2 70 . 1 1 95 95 THR N N 15 1006.9 26.05 . . . . . 5996 2 71 . 1 1 96 96 ASP N N 15 970.89 5.89 . . . . . 5996 2 72 . 1 1 97 97 TYR N N 15 951.60 13.56 . . . . . 5996 2 73 . 1 1 98 98 ASP N N 15 915.51 12.39 . . . . . 5996 2 74 . 1 1 100 100 PHE N N 15 1035.1 15.42 . . . . . 5996 2 75 . 1 1 101 101 LEU N N 15 994.95 22.22 . . . . . 5996 2 76 . 1 1 102 102 MET N N 15 971.89 9.51 . . . . . 5996 2 77 . 1 1 103 103 ALA N N 15 1056.1 12.30 . . . . . 5996 2 78 . 1 1 104 104 HIS N N 15 1075.2 12.79 . . . . . 5996 2 79 . 1 1 105 105 LEU N N 15 966.69 10.21 . . . . . 5996 2 80 . 1 1 107 107 ASN N N 15 906.26 16.80 . . . . . 5996 2 81 . 1 1 108 108 GLU N N 15 931.59 12.33 . . . . . 5996 2 82 . 1 1 109 109 LYS N N 15 926.11 14.47 . . . . . 5996 2 83 . 1 1 110 110 ASP N N 15 882.58 33.98 . . . . . 5996 2 84 . 1 1 111 111 GLY N N 15 950.91 17.13 . . . . . 5996 2 85 . 1 1 113 113 THR N N 15 977.57 20.09 . . . . . 5996 2 86 . 1 1 114 114 PHE N N 15 983.15 17.59 . . . . . 5996 2 87 . 1 1 115 115 GLN N N 15 949.87 6.78 . . . . . 5996 2 88 . 1 1 116 116 LEU N N 15 1001.4 14.89 . . . . . 5996 2 89 . 1 1 117 117 MET N N 15 983.80 17.30 . . . . . 5996 2 90 . 1 1 118 118 GLY N N 15 986.48 14.46 . . . . . 5996 2 91 . 1 1 121 121 GLY N N 15 971.17 18.06 . . . . . 5996 2 92 . 1 1 123 123 GLU N N 15 1010.2 14.21 . . . . . 5996 2 93 . 1 1 125 125 ASP N N 15 946.31 14.95 . . . . . 5996 2 94 . 1 1 126 126 LEU N N 15 964.52 40.20 . . . . . 5996 2 95 . 1 1 127 127 SER N N 15 991.96 15.03 . . . . . 5996 2 96 . 1 1 128 128 SER N N 15 872.75 42.73 . . . . . 5996 2 97 . 1 1 130 130 ILE N N 15 941.10 14.16 . . . . . 5996 2 98 . 1 1 131 131 LYS N N 15 928.52 15.83 . . . . . 5996 2 99 . 1 1 134 134 PHE N N 15 837.09 33.12 . . . . . 5996 2 100 . 1 1 135 135 ALA N N 15 915.99 13.37 . . . . . 5996 2 101 . 1 1 136 136 GLN N N 15 935.42 11.07 . . . . . 5996 2 102 . 1 1 137 137 LEU N N 15 937.14 10.63 . . . . . 5996 2 103 . 1 1 138 138 CYS N N 15 980.24 6.77 . . . . . 5996 2 104 . 1 1 140 140 LYS N N 15 963.47 13.79 . . . . . 5996 2 105 . 1 1 141 141 HIS N N 15 976.20 9.98 . . . . . 5996 2 106 . 1 1 142 142 GLY N N 15 973.03 11.59 . . . . . 5996 2 107 . 1 1 145 145 ARG N N 15 1021.0 14.89 . . . . . 5996 2 108 . 1 1 146 146 GLU N N 15 968.58 13.99 . . . . . 5996 2 109 . 1 1 148 148 ILE N N 15 951.16 12.07 . . . . . 5996 2 110 . 1 1 151 151 LEU N N 15 1015.2 18.98 . . . . . 5996 2 111 . 1 1 152 152 SER N N 15 870.70 19.56 . . . . . 5996 2 112 . 1 1 153 153 ASN N N 15 869.14 20.69 . . . . . 5996 2 113 . 1 1 160 160 ALA N N 15 687.27 13.27 . . . . . 5996 2 stop_ save_ save_293_600_bound_t1 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode 293_600_bound_t1 _Heteronucl_T1_list.Entry_ID 5996 _Heteronucl_T1_list.ID 3 _Heteronucl_T1_list.Sample_condition_list_ID 3 _Heteronucl_T1_list.Sample_condition_list_label $293K _Heteronucl_T1_list.Spectrometer_frequency_1H 600 _Heteronucl_T1_list.T1_coherence_type Nz _Heteronucl_T1_list.T1_val_units ms _Heteronucl_T1_list.Details . _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID 1 '15N T1' 1 $sample_1 . 5996 3 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 3 3 ALA N N 15 870.60 17.88 . . . . . 5996 3 2 . 1 1 5 5 SER N N 15 810.89 13.18 . . . . . 5996 3 3 . 1 1 6 6 THR N N 15 734.57 14.66 . . . . . 5996 3 4 . 1 1 7 7 GLY N N 15 801.14 24.00 . . . . . 5996 3 5 . 1 1 10 10 PHE N N 15 823.83 14.61 . . . . . 5996 3 6 . 1 1 11 11 ASN N N 15 832.88 15.95 . . . . . 5996 3 7 . 1 1 12 12 VAL N N 15 939.11 8.893 . . . . . 5996 3 8 . 1 1 13 13 GLU N N 15 895.67 7.283 . . . . . 5996 3 9 . 1 1 15 15 ILE N N 15 854.49 13.18 . . . . . 5996 3 10 . 1 1 16 16 ASN N N 15 835.80 8.877 . . . . . 5996 3 11 . 1 1 18 18 GLU N N 15 829.64 16.62 . . . . . 5996 3 12 . 1 1 19 19 TRP N N 15 883.13 32.31 . . . . . 5996 3 13 . 1 1 20 20 HIS N N 15 892.03 26.57 . . . . . 5996 3 14 . 1 1 22 22 ILE N N 15 859.52 12.93 . . . . . 5996 3 15 . 1 1 23 23 ILE N N 15 914.01 9.877 . . . . . 5996 3 16 . 1 1 26 26 SER N N 15 844.02 16.65 . . . . . 5996 3 17 . 1 1 27 27 ASP N N 15 798.73 10.91 . . . . . 5996 3 18 . 1 1 29 29 ARG N N 15 803.22 16.90 . . . . . 5996 3 19 . 1 1 30 30 GLU N N 15 807.07 13.24 . . . . . 5996 3 20 . 1 1 31 31 LYS N N 15 822.41 6.464 . . . . . 5996 3 21 . 1 1 32 32 ILE N N 15 746.89 26.95 . . . . . 5996 3 22 . 1 1 33 33 GLU N N 15 821.53 15.87 . . . . . 5996 3 23 . 1 1 36 36 GLY N N 15 820.05 17.45 . . . . . 5996 3 24 . 1 1 37 37 ASN N N 15 806.03 29.51 . . . . . 5996 3 25 . 1 1 39 39 ARG N N 15 819.60 16.85 . . . . . 5996 3 26 . 1 1 40 40 LEU N N 15 901.33 13.97 . . . . . 5996 3 27 . 1 1 43 43 GLU N N 15 790.64 23.95 . . . . . 5996 3 28 . 1 1 45 45 ILE N N 15 883.00 12.83 . . . . . 5996 3 29 . 1 1 46 46 HIS N N 15 804.92 24.85 . . . . . 5996 3 30 . 1 1 47 47 VAL N N 15 862.71 12.25 . . . . . 5996 3 31 . 1 1 48 48 LEU N N 15 815.60 20.15 . . . . . 5996 3 32 . 1 1 50 50 ASN N N 15 804.66 21.13 . . . . . 5996 3 33 . 1 1 51 51 SER N N 15 826.22 6.991 . . . . . 5996 3 34 . 1 1 52 52 LEU N N 15 908.17 5.446 . . . . . 5996 3 35 . 1 1 53 53 VAL N N 15 904.71 4.915 . . . . . 5996 3 36 . 1 1 54 54 LEU N N 15 856.36 9.301 . . . . . 5996 3 37 . 1 1 55 55 LYS N N 15 869.32 15.97 . . . . . 5996 3 38 . 1 1 57 57 HIS N N 15 875.80 17.55 . . . . . 5996 3 39 . 1 1 60 60 ARG N N 15 864.86 3.971 . . . . . 5996 3 40 . 1 1 61 61 ASP N N 15 798.99 20.45 . . . . . 5996 3 41 . 1 1 62 62 GLU N N 15 843.79 9.529 . . . . . 5996 3 42 . 1 1 64 64 CYS N N 15 897.68 7.500 . . . . . 5996 3 43 . 1 1 66 66 GLU N N 15 873.02 12.20 . . . . . 5996 3 44 . 1 1 67 67 LEU N N 15 802.84 15.92 . . . . . 5996 3 45 . 1 1 68 68 SER N N 15 923.05 5.712 . . . . . 5996 3 46 . 1 1 69 69 MET N N 15 866.89 8.687 . . . . . 5996 3 47 . 1 1 71 71 ALA N N 15 819.39 18.69 . . . . . 5996 3 48 . 1 1 72 72 ASP N N 15 875.00 17.28 . . . . . 5996 3 49 . 1 1 74 74 THR N N 15 822.13 8.297 . . . . . 5996 3 50 . 1 1 75 75 GLU N N 15 866.85 14.17 . . . . . 5996 3 51 . 1 1 76 76 LYS N N 15 897.81 13.48 . . . . . 5996 3 52 . 1 1 77 77 ALA N N 15 891.72 16.56 . . . . . 5996 3 53 . 1 1 78 78 GLY N N 15 818.51 23.66 . . . . . 5996 3 54 . 1 1 79 79 GLU N N 15 793.29 10.26 . . . . . 5996 3 55 . 1 1 80 80 TYR N N 15 787.44 17.21 . . . . . 5996 3 56 . 1 1 81 81 SER N N 15 849.06 9.296 . . . . . 5996 3 57 . 1 1 82 82 VAL N N 15 774.43 21.02 . . . . . 5996 3 58 . 1 1 83 83 THR N N 15 847.70 11.82 . . . . . 5996 3 59 . 1 1 84 84 TYR N N 15 897.26 7.670 . . . . . 5996 3 60 . 1 1 86 86 GLY N N 15 853.49 4.411 . . . . . 5996 3 61 . 1 1 87 87 PHE N N 15 879.31 9.177 . . . . . 5996 3 62 . 1 1 88 88 ASN N N 15 879.96 7.718 . . . . . 5996 3 63 . 1 1 89 89 THR N N 15 810.5 18.72 . . . . . 5996 3 64 . 1 1 90 90 PHE N N 15 907.89 13.76 . . . . . 5996 3 65 . 1 1 91 91 THR N N 15 794.66 10.18 . . . . . 5996 3 66 . 1 1 92 92 ILE N N 15 864.98 20.74 . . . . . 5996 3 67 . 1 1 94 94 LYS N N 15 860.82 12.98 . . . . . 5996 3 68 . 1 1 95 95 THR N N 15 922.94 12.86 . . . . . 5996 3 69 . 1 1 96 96 ASP N N 15 811.01 23.07 . . . . . 5996 3 70 . 1 1 97 97 TYR N N 15 813.32 15.53 . . . . . 5996 3 71 . 1 1 98 98 ASP N N 15 763.48 25.22 . . . . . 5996 3 72 . 1 1 101 101 LEU N N 15 843.63 21.10 . . . . . 5996 3 73 . 1 1 102 102 MET N N 15 861.70 10.51 . . . . . 5996 3 74 . 1 1 103 103 ALA N N 15 926.39 18.33 . . . . . 5996 3 75 . 1 1 104 104 HIS N N 15 894.45 6.495 . . . . . 5996 3 76 . 1 1 105 105 LEU N N 15 849.83 14.67 . . . . . 5996 3 77 . 1 1 108 108 GLU N N 15 866.11 7.481 . . . . . 5996 3 78 . 1 1 109 109 LYS N N 15 864.18 8.834 . . . . . 5996 3 79 . 1 1 110 110 ASP N N 15 773.91 28.02 . . . . . 5996 3 80 . 1 1 111 111 GLY N N 15 824.23 9.037 . . . . . 5996 3 81 . 1 1 115 115 GLN N N 15 822.79 17.40 . . . . . 5996 3 82 . 1 1 116 116 LEU N N 15 862.13 13.02 . . . . . 5996 3 83 . 1 1 117 117 MET N N 15 882.54 12.16 . . . . . 5996 3 84 . 1 1 118 118 GLY N N 15 887.38 9.989 . . . . . 5996 3 85 . 1 1 119 119 LEU N N 15 862.62 20.03 . . . . . 5996 3 86 . 1 1 120 120 TYR N N 15 967.68 11.26 . . . . . 5996 3 87 . 1 1 121 121 GLY N N 15 910.73 13.50 . . . . . 5996 3 88 . 1 1 123 123 GLU N N 15 939.16 7.010 . . . . . 5996 3 89 . 1 1 125 125 ASP N N 15 835.25 8.995 . . . . . 5996 3 90 . 1 1 128 128 SER N N 15 792.35 30.08 . . . . . 5996 3 91 . 1 1 129 129 ASP N N 15 799.95 8.804 . . . . . 5996 3 92 . 1 1 130 130 ILE N N 15 816.72 15.29 . . . . . 5996 3 93 . 1 1 131 131 LYS N N 15 802.88 13.53 . . . . . 5996 3 94 . 1 1 134 134 PHE N N 15 751.11 23.38 . . . . . 5996 3 95 . 1 1 135 135 ALA N N 15 783.21 14.05 . . . . . 5996 3 96 . 1 1 136 136 GLN N N 15 832.00 12.32 . . . . . 5996 3 97 . 1 1 137 137 LEU N N 15 810.82 16.53 . . . . . 5996 3 98 . 1 1 138 138 CYS N N 15 809.17 20.29 . . . . . 5996 3 99 . 1 1 141 141 HIS N N 15 843.53 16.78 . . . . . 5996 3 100 . 1 1 142 142 GLY N N 15 914.70 9.531 . . . . . 5996 3 101 . 1 1 143 143 ILE N N 15 867.83 30.59 . . . . . 5996 3 102 . 1 1 144 144 LEU N N 15 877.36 11.00 . . . . . 5996 3 103 . 1 1 145 145 ARG N N 15 893.23 8.928 . . . . . 5996 3 104 . 1 1 148 148 ILE N N 15 840.70 10.47 . . . . . 5996 3 105 . 1 1 151 151 LEU N N 15 905.11 11.06 . . . . . 5996 3 106 . 1 1 156 156 ARG N N 15 824.77 39.49 . . . . . 5996 3 107 . 1 1 160 160 ALA N N 15 673.61 14.30 . . . . . 5996 3 108 . 1 1 162 162 GLU N N 15 859.73 9.385 . . . . . 5996 3 stop_ save_ save_298_600_bound_t1 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode 298_600_bound_t1 _Heteronucl_T1_list.Entry_ID 5996 _Heteronucl_T1_list.ID 4 _Heteronucl_T1_list.Sample_condition_list_ID 4 _Heteronucl_T1_list.Sample_condition_list_label $298K _Heteronucl_T1_list.Spectrometer_frequency_1H 600 _Heteronucl_T1_list.T1_coherence_type Nz _Heteronucl_T1_list.T1_val_units ms _Heteronucl_T1_list.Details . _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID 1 '15N T1' 1 $sample_1 . 5996 4 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 3 3 ALA N N 15 830.68 29.55 . . . . . 5996 4 2 . 1 1 4 4 SER N N 15 866.21 33.83 . . . . . 5996 4 3 . 1 1 5 5 SER N N 15 748.18 46.40 . . . . . 5996 4 4 . 1 1 6 6 THR N N 15 697.53 43.50 . . . . . 5996 4 5 . 1 1 7 7 GLY N N 15 789.72 37.99 . . . . . 5996 4 6 . 1 1 10 10 PHE N N 15 802.83 49.41 . . . . . 5996 4 7 . 1 1 11 11 ASN N N 15 782.38 45.18 . . . . . 5996 4 8 . 1 1 12 12 VAL N N 15 869.96 28.28 . . . . . 5996 4 9 . 1 1 13 13 GLU N N 15 817.41 29.05 . . . . . 5996 4 10 . 1 1 15 15 ILE N N 15 781.01 27.27 . . . . . 5996 4 11 . 1 1 16 16 ASN N N 15 795.45 36.30 . . . . . 5996 4 12 . 1 1 17 17 GLY N N 15 771.69 41.09 . . . . . 5996 4 13 . 1 1 18 18 GLU N N 15 761.06 51.50 . . . . . 5996 4 14 . 1 1 19 19 TRP N N 15 809.80 40.78 . . . . . 5996 4 15 . 1 1 20 20 HIS N N 15 847.29 47.61 . . . . . 5996 4 16 . 1 1 21 21 THR N N 15 800.47 48.83 . . . . . 5996 4 17 . 1 1 22 22 ILE N N 15 789.82 26.56 . . . . . 5996 4 18 . 1 1 23 23 ILE N N 15 814.15 31.31 . . . . . 5996 4 19 . 1 1 26 26 SER N N 15 790.19 32.63 . . . . . 5996 4 20 . 1 1 27 27 ASP N N 15 768.68 29.13 . . . . . 5996 4 21 . 1 1 29 29 ARG N N 15 742.10 45.15 . . . . . 5996 4 22 . 1 1 30 30 GLU N N 15 758.96 38.57 . . . . . 5996 4 23 . 1 1 31 31 LYS N N 15 751.87 24.36 . . . . . 5996 4 24 . 1 1 32 32 ILE N N 15 764.35 33.55 . . . . . 5996 4 25 . 1 1 33 33 GLU N N 15 787.35 29.95 . . . . . 5996 4 26 . 1 1 35 35 ASN N N 15 823.92 51.56 . . . . . 5996 4 27 . 1 1 36 36 GLY N N 15 763.84 37.60 . . . . . 5996 4 28 . 1 1 37 37 ASN N N 15 753.77 63.99 . . . . . 5996 4 29 . 1 1 39 39 ARG N N 15 762.56 30.74 . . . . . 5996 4 30 . 1 1 40 40 LEU N N 15 827.80 31.38 . . . . . 5996 4 31 . 1 1 42 42 LEU N N 15 824.39 39.16 . . . . . 5996 4 32 . 1 1 43 43 GLU N N 15 707.83 39.63 . . . . . 5996 4 33 . 1 1 45 45 ILE N N 15 809.29 39.28 . . . . . 5996 4 34 . 1 1 46 46 HIS N N 15 780.33 32.38 . . . . . 5996 4 35 . 1 1 47 47 VAL N N 15 802.82 37.87 . . . . . 5996 4 36 . 1 1 48 48 LEU N N 15 771.06 29.47 . . . . . 5996 4 37 . 1 1 50 50 ASN N N 15 774.59 85.20 . . . . . 5996 4 38 . 1 1 51 51 SER N N 15 737.20 39.10 . . . . . 5996 4 39 . 1 1 52 52 LEU N N 15 802.03 40.33 . . . . . 5996 4 40 . 1 1 53 53 VAL N N 15 823.03 41.37 . . . . . 5996 4 41 . 1 1 54 54 LEU N N 15 784.38 23.62 . . . . . 5996 4 42 . 1 1 55 55 LYS N N 15 816.50 37.56 . . . . . 5996 4 43 . 1 1 57 57 HIS N N 15 807.12 30.17 . . . . . 5996 4 44 . 1 1 58 58 THR N N 15 751.24 44.58 . . . . . 5996 4 45 . 1 1 60 60 ARG N N 15 765.50 36.77 . . . . . 5996 4 46 . 1 1 61 61 ASP N N 15 770.53 43.13 . . . . . 5996 4 47 . 1 1 62 62 GLU N N 15 804.36 31.97 . . . . . 5996 4 48 . 1 1 64 64 CYS N N 15 822.96 41.98 . . . . . 5996 4 49 . 1 1 65 65 SER N N 15 808.58 39.17 . . . . . 5996 4 50 . 1 1 66 66 GLU N N 15 835.72 47.32 . . . . . 5996 4 51 . 1 1 67 67 LEU N N 15 780.60 38.90 . . . . . 5996 4 52 . 1 1 68 68 SER N N 15 830.88 45.14 . . . . . 5996 4 53 . 1 1 69 69 MET N N 15 785.08 50.34 . . . . . 5996 4 54 . 1 1 71 71 ALA N N 15 782.05 29.11 . . . . . 5996 4 55 . 1 1 72 72 ASP N N 15 813.98 35.76 . . . . . 5996 4 56 . 1 1 74 74 THR N N 15 814.52 21.22 . . . . . 5996 4 57 . 1 1 75 75 GLU N N 15 794.31 47.63 . . . . . 5996 4 58 . 1 1 76 76 LYS N N 15 795.79 21.85 . . . . . 5996 4 59 . 1 1 77 77 ALA N N 15 821.86 50.36 . . . . . 5996 4 60 . 1 1 78 78 GLY N N 15 790.43 66.29 . . . . . 5996 4 61 . 1 1 79 79 GLU N N 15 733.68 36.68 . . . . . 5996 4 62 . 1 1 80 80 TYR N N 15 768.99 36.34 . . . . . 5996 4 63 . 1 1 81 81 SER N N 15 785.11 35.17 . . . . . 5996 4 64 . 1 1 82 82 VAL N N 15 758.15 26.00 . . . . . 5996 4 65 . 1 1 83 83 THR N N 15 780.09 37.80 . . . . . 5996 4 66 . 1 1 84 84 TYR N N 15 823.08 45.48 . . . . . 5996 4 67 . 1 1 85 85 ASP N N 15 766.91 31.88 . . . . . 5996 4 68 . 1 1 86 86 GLY N N 15 790.15 33.28 . . . . . 5996 4 69 . 1 1 87 87 PHE N N 15 779.96 39.91 . . . . . 5996 4 70 . 1 1 88 88 ASN N N 15 816.70 27.27 . . . . . 5996 4 71 . 1 1 89 89 THR N N 15 787.09 35.12 . . . . . 5996 4 72 . 1 1 90 90 PHE N N 15 841.76 34.22 . . . . . 5996 4 73 . 1 1 91 91 THR N N 15 737.10 37.84 . . . . . 5996 4 74 . 1 1 92 92 ILE N N 15 804.79 37.23 . . . . . 5996 4 75 . 1 1 94 94 LYS N N 15 812.60 42.29 . . . . . 5996 4 76 . 1 1 95 95 THR N N 15 829.76 33.80 . . . . . 5996 4 77 . 1 1 96 96 ASP N N 15 800.69 35.95 . . . . . 5996 4 78 . 1 1 97 97 TYR N N 15 775.74 31.96 . . . . . 5996 4 79 . 1 1 99 99 ASN N N 15 833.26 34.67 . . . . . 5996 4 80 . 1 1 100 100 PHE N N 15 817.94 45.53 . . . . . 5996 4 81 . 1 1 101 101 LEU N N 15 816.19 36.66 . . . . . 5996 4 82 . 1 1 103 103 ALA N N 15 837.05 34.42 . . . . . 5996 4 83 . 1 1 104 104 HIS N N 15 871.91 26.37 . . . . . 5996 4 84 . 1 1 105 105 LEU N N 15 777.01 34.21 . . . . . 5996 4 85 . 1 1 107 107 ASN N N 15 750.83 29.12 . . . . . 5996 4 86 . 1 1 108 108 GLU N N 15 772.42 27.31 . . . . . 5996 4 87 . 1 1 109 109 LYS N N 15 781.45 30.70 . . . . . 5996 4 88 . 1 1 110 110 ASP N N 15 746.97 62.84 . . . . . 5996 4 89 . 1 1 111 111 GLY N N 15 777.87 31.80 . . . . . 5996 4 90 . 1 1 113 113 THR N N 15 813.33 40.68 . . . . . 5996 4 91 . 1 1 114 114 PHE N N 15 820.68 32.63 . . . . . 5996 4 92 . 1 1 115 115 GLN N N 15 769.00 34.75 . . . . . 5996 4 93 . 1 1 116 116 LEU N N 15 833.26 32.75 . . . . . 5996 4 94 . 1 1 117 117 MET N N 15 824.26 28.53 . . . . . 5996 4 95 . 1 1 118 118 GLY N N 15 814.73 39.49 . . . . . 5996 4 96 . 1 1 119 119 LEU N N 15 812.51 35.41 . . . . . 5996 4 97 . 1 1 121 121 GLY N N 15 800.04 32.68 . . . . . 5996 4 98 . 1 1 123 123 GLU N N 15 865.68 35.96 . . . . . 5996 4 99 . 1 1 125 125 ASP N N 15 777.81 38.37 . . . . . 5996 4 100 . 1 1 126 126 LEU N N 15 779.51 34.85 . . . . . 5996 4 101 . 1 1 127 127 SER N N 15 834.27 31.79 . . . . . 5996 4 102 . 1 1 128 128 SER N N 15 760.84 102.3 . . . . . 5996 4 103 . 1 1 130 130 ILE N N 15 768.69 31.40 . . . . . 5996 4 104 . 1 1 131 131 LYS N N 15 758.92 23.30 . . . . . 5996 4 105 . 1 1 133 133 ARG N N 15 760.39 33.85 . . . . . 5996 4 106 . 1 1 134 134 PHE N N 15 726.54 73.95 . . . . . 5996 4 107 . 1 1 135 135 ALA N N 15 730.06 45.58 . . . . . 5996 4 108 . 1 1 136 136 GLN N N 15 780.44 37.23 . . . . . 5996 4 109 . 1 1 137 137 LEU N N 15 774.96 31.66 . . . . . 5996 4 110 . 1 1 138 138 CYS N N 15 760.80 31.12 . . . . . 5996 4 111 . 1 1 141 141 HIS N N 15 820.81 31.22 . . . . . 5996 4 112 . 1 1 142 142 GLY N N 15 808.98 25.66 . . . . . 5996 4 113 . 1 1 143 143 ILE N N 15 826.78 31.54 . . . . . 5996 4 114 . 1 1 144 144 LEU N N 15 828.26 29.73 . . . . . 5996 4 115 . 1 1 145 145 ARG N N 15 838.03 29.86 . . . . . 5996 4 116 . 1 1 146 146 GLU N N 15 782.39 28.76 . . . . . 5996 4 117 . 1 1 148 148 ILE N N 15 786.73 29.97 . . . . . 5996 4 118 . 1 1 149 149 ILE N N 15 800.90 39.04 . . . . . 5996 4 119 . 1 1 150 150 ASP N N 15 827.88 28.08 . . . . . 5996 4 120 . 1 1 151 151 LEU N N 15 859.39 41.27 . . . . . 5996 4 121 . 1 1 152 152 SER N N 15 727.94 45.42 . . . . . 5996 4 122 . 1 1 153 153 ASN N N 15 740.89 52.53 . . . . . 5996 4 123 . 1 1 160 160 ALA N N 15 707.01 47.15 . . . . . 5996 4 124 . 1 1 162 162 GLU N N 15 903.77 32.55 . . . . . 5996 4 stop_ save_ save_303_600_bound_t1 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode 303_600_bound_t1 _Heteronucl_T1_list.Entry_ID 5996 _Heteronucl_T1_list.ID 5 _Heteronucl_T1_list.Sample_condition_list_ID 5 _Heteronucl_T1_list.Sample_condition_list_label $303K _Heteronucl_T1_list.Spectrometer_frequency_1H 600 _Heteronucl_T1_list.T1_coherence_type Nz _Heteronucl_T1_list.T1_val_units ms _Heteronucl_T1_list.Details . _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID 1 '15N T1' 1 $sample_1 . 5996 5 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 3 3 ALA N N 15 745.35 56.51 . . . . . 5996 5 2 . 1 1 4 4 SER N N 15 772.16 63.71 . . . . . 5996 5 3 . 1 1 5 5 SER N N 15 698.84 48.97 . . . . . 5996 5 4 . 1 1 6 6 THR N N 15 660.36 48.86 . . . . . 5996 5 5 . 1 1 7 7 GLY N N 15 672.52 47.90 . . . . . 5996 5 6 . 1 1 10 10 PHE N N 15 766.06 64.77 . . . . . 5996 5 7 . 1 1 11 11 ASN N N 15 720.98 54.20 . . . . . 5996 5 8 . 1 1 12 12 VAL N N 15 731.27 50.34 . . . . . 5996 5 9 . 1 1 13 13 GLU N N 15 671.20 44.36 . . . . . 5996 5 10 . 1 1 15 15 ILE N N 15 692.68 46.17 . . . . . 5996 5 11 . 1 1 16 16 ASN N N 15 665.46 43.96 . . . . . 5996 5 12 . 1 1 17 17 GLY N N 15 674.78 40.60 . . . . . 5996 5 13 . 1 1 18 18 GLU N N 15 684.12 46.60 . . . . . 5996 5 14 . 1 1 20 20 HIS N N 15 725.19 53.49 . . . . . 5996 5 15 . 1 1 21 21 THR N N 15 754.24 65.41 . . . . . 5996 5 16 . 1 1 22 22 ILE N N 15 695.61 41.41 . . . . . 5996 5 17 . 1 1 23 23 ILE N N 15 714.44 49.34 . . . . . 5996 5 18 . 1 1 27 27 ASP N N 15 655.39 41.11 . . . . . 5996 5 19 . 1 1 29 29 ARG N N 15 696.70 59.09 . . . . . 5996 5 20 . 1 1 31 31 LYS N N 15 662.40 44.85 . . . . . 5996 5 21 . 1 1 32 32 ILE N N 15 642.50 43.79 . . . . . 5996 5 22 . 1 1 33 33 GLU N N 15 695.79 46.29 . . . . . 5996 5 23 . 1 1 35 35 ASN N N 15 703.54 49.64 . . . . . 5996 5 24 . 1 1 36 36 GLY N N 15 654.51 44.87 . . . . . 5996 5 25 . 1 1 37 37 ASN N N 15 753.47 64.73 . . . . . 5996 5 26 . 1 1 39 39 ARG N N 15 678.44 43.05 . . . . . 5996 5 27 . 1 1 40 40 LEU N N 15 764.61 55.58 . . . . . 5996 5 28 . 1 1 42 42 LEU N N 15 721.88 47.12 . . . . . 5996 5 29 . 1 1 43 43 GLU N N 15 682.36 42.80 . . . . . 5996 5 30 . 1 1 45 45 ILE N N 15 685.65 47.58 . . . . . 5996 5 31 . 1 1 46 46 HIS N N 15 679.51 47.90 . . . . . 5996 5 32 . 1 1 47 47 VAL N N 15 689.89 48.03 . . . . . 5996 5 33 . 1 1 48 48 LEU N N 15 697.92 44.87 . . . . . 5996 5 34 . 1 1 50 50 ASN N N 15 799.96 64.77 . . . . . 5996 5 35 . 1 1 51 51 SER N N 15 726.02 46.35 . . . . . 5996 5 36 . 1 1 52 52 LEU N N 15 705.79 51.15 . . . . . 5996 5 37 . 1 1 53 53 VAL N N 15 713.50 46.97 . . . . . 5996 5 38 . 1 1 54 54 LEU N N 15 686.84 46.20 . . . . . 5996 5 39 . 1 1 55 55 LYS N N 15 745.58 54.81 . . . . . 5996 5 40 . 1 1 57 57 HIS N N 15 695.45 41.95 . . . . . 5996 5 41 . 1 1 58 58 THR N N 15 720.80 45.65 . . . . . 5996 5 42 . 1 1 60 60 ARG N N 15 684.26 44.26 . . . . . 5996 5 43 . 1 1 61 61 ASP N N 15 700.29 52.54 . . . . . 5996 5 44 . 1 1 62 62 GLU N N 15 698.17 51.37 . . . . . 5996 5 45 . 1 1 64 64 CYS N N 15 753.17 56.01 . . . . . 5996 5 46 . 1 1 65 65 SER N N 15 705.69 57.42 . . . . . 5996 5 47 . 1 1 66 66 GLU N N 15 723.67 55.79 . . . . . 5996 5 48 . 1 1 67 67 LEU N N 15 681.97 43.91 . . . . . 5996 5 49 . 1 1 68 68 SER N N 15 741.94 52.46 . . . . . 5996 5 50 . 1 1 69 69 MET N N 15 711.94 49.30 . . . . . 5996 5 51 . 1 1 71 71 ALA N N 15 673.63 42.48 . . . . . 5996 5 52 . 1 1 72 72 ASP N N 15 715.57 51.11 . . . . . 5996 5 53 . 1 1 74 74 THR N N 15 700.52 42.42 . . . . . 5996 5 54 . 1 1 75 75 GLU N N 15 725.04 60.67 . . . . . 5996 5 55 . 1 1 76 76 LYS N N 15 703.99 50.51 . . . . . 5996 5 56 . 1 1 77 77 ALA N N 15 764.12 64.90 . . . . . 5996 5 57 . 1 1 78 78 GLY N N 15 800.55 65.38 . . . . . 5996 5 58 . 1 1 79 79 GLU N N 15 692.06 45.51 . . . . . 5996 5 59 . 1 1 81 81 SER N N 15 689.79 44.55 . . . . . 5996 5 60 . 1 1 82 82 VAL N N 15 676.90 45.88 . . . . . 5996 5 61 . 1 1 83 83 THR N N 15 701.61 48.32 . . . . . 5996 5 62 . 1 1 84 84 TYR N N 15 734.36 52.33 . . . . . 5996 5 63 . 1 1 85 85 ASP N N 15 701.15 51.02 . . . . . 5996 5 64 . 1 1 86 86 GLY N N 15 697.04 46.52 . . . . . 5996 5 65 . 1 1 87 87 PHE N N 15 689.98 44.42 . . . . . 5996 5 66 . 1 1 89 89 THR N N 15 690.97 50.32 . . . . . 5996 5 67 . 1 1 90 90 PHE N N 15 738.95 56.72 . . . . . 5996 5 68 . 1 1 91 91 THR N N 15 680.88 41.67 . . . . . 5996 5 69 . 1 1 92 92 ILE N N 15 733.99 55.22 . . . . . 5996 5 70 . 1 1 94 94 LYS N N 15 690.03 47.55 . . . . . 5996 5 71 . 1 1 95 95 THR N N 15 719.58 53.61 . . . . . 5996 5 72 . 1 1 96 96 ASP N N 15 692.21 42.07 . . . . . 5996 5 73 . 1 1 97 97 TYR N N 15 650.50 45.85 . . . . . 5996 5 74 . 1 1 98 98 ASP N N 15 670.84 41.90 . . . . . 5996 5 75 . 1 1 99 99 ASN N N 15 697.83 44.09 . . . . . 5996 5 76 . 1 1 100 100 PHE N N 15 725.02 45.39 . . . . . 5996 5 77 . 1 1 102 102 MET N N 15 687.52 42.47 . . . . . 5996 5 78 . 1 1 103 103 ALA N N 15 721.13 52.43 . . . . . 5996 5 79 . 1 1 104 104 HIS N N 15 737.85 54.03 . . . . . 5996 5 80 . 1 1 105 105 LEU N N 15 692.58 48.85 . . . . . 5996 5 81 . 1 1 107 107 ASN N N 15 653.82 43.90 . . . . . 5996 5 82 . 1 1 108 108 GLU N N 15 686.95 46.08 . . . . . 5996 5 83 . 1 1 109 109 LYS N N 15 688.14 47.96 . . . . . 5996 5 84 . 1 1 110 110 ASP N N 15 733.29 60.80 . . . . . 5996 5 85 . 1 1 111 111 GLY N N 15 707.91 48.67 . . . . . 5996 5 86 . 1 1 113 113 THR N N 15 776.46 71.33 . . . . . 5996 5 87 . 1 1 114 114 PHE N N 15 692.94 45.45 . . . . . 5996 5 88 . 1 1 115 115 GLN N N 15 687.79 43.85 . . . . . 5996 5 89 . 1 1 116 116 LEU N N 15 700.01 47.50 . . . . . 5996 5 90 . 1 1 117 117 MET N N 15 703.59 46.68 . . . . . 5996 5 91 . 1 1 121 121 GLY N N 15 718.03 43.71 . . . . . 5996 5 92 . 1 1 123 123 GLU N N 15 773.44 70.89 . . . . . 5996 5 93 . 1 1 125 125 ASP N N 15 686.15 44.28 . . . . . 5996 5 94 . 1 1 126 126 LEU N N 15 747.64 58.88 . . . . . 5996 5 95 . 1 1 127 127 SER N N 15 725.32 48.44 . . . . . 5996 5 96 . 1 1 128 128 SER N N 15 795.83 61.10 . . . . . 5996 5 97 . 1 1 129 129 ASP N N 15 720.72 49.54 . . . . . 5996 5 98 . 1 1 131 131 LYS N N 15 671.91 44.28 . . . . . 5996 5 99 . 1 1 133 133 ARG N N 15 662.13 43.69 . . . . . 5996 5 100 . 1 1 134 134 PHE N N 15 747.25 53.65 . . . . . 5996 5 101 . 1 1 135 135 ALA N N 15 656.98 43.87 . . . . . 5996 5 102 . 1 1 136 136 GLN N N 15 664.19 46.91 . . . . . 5996 5 103 . 1 1 138 138 CYS N N 15 668.80 40.71 . . . . . 5996 5 104 . 1 1 141 141 HIS N N 15 708.65 47.17 . . . . . 5996 5 105 . 1 1 142 142 GLY N N 15 714.05 44.20 . . . . . 5996 5 106 . 1 1 143 143 ILE N N 15 743.16 55.02 . . . . . 5996 5 107 . 1 1 144 144 LEU N N 15 702.93 49.38 . . . . . 5996 5 108 . 1 1 145 145 ARG N N 15 712.76 51.75 . . . . . 5996 5 109 . 1 1 146 146 GLU N N 15 673.83 46.35 . . . . . 5996 5 110 . 1 1 148 148 ILE N N 15 673.35 45.44 . . . . . 5996 5 111 . 1 1 149 149 ILE N N 15 713.80 44.34 . . . . . 5996 5 112 . 1 1 150 150 ASP N N 15 700.52 49.69 . . . . . 5996 5 113 . 1 1 151 151 LEU N N 15 743.89 54.74 . . . . . 5996 5 114 . 1 1 152 152 SER N N 15 690.66 46.72 . . . . . 5996 5 115 . 1 1 153 153 ASN N N 15 709.81 52.31 . . . . . 5996 5 116 . 1 1 155 155 ASN N N 15 699.92 61.21 . . . . . 5996 5 117 . 1 1 156 156 ARG N N 15 717.60 51.20 . . . . . 5996 5 118 . 1 1 160 160 ALA N N 15 678.94 51.20 . . . . . 5996 5 119 . 1 1 162 162 GLU N N 15 837.09 77.65 . . . . . 5996 5 stop_ save_ save_308_600_bound_t1 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode 308_600_bound_t1 _Heteronucl_T1_list.Entry_ID 5996 _Heteronucl_T1_list.ID 6 _Heteronucl_T1_list.Sample_condition_list_ID 6 _Heteronucl_T1_list.Sample_condition_list_label $308K _Heteronucl_T1_list.Spectrometer_frequency_1H 600 _Heteronucl_T1_list.T1_coherence_type Nz _Heteronucl_T1_list.T1_val_units ms _Heteronucl_T1_list.Details . _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID 1 '15N T1' 1 $sample_1 . 5996 6 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 3 3 ALA N N 15 715.58 3.26 . . . . . 5996 6 2 . 1 1 4 4 SER N N 15 703.05 8.50 . . . . . 5996 6 3 . 1 1 6 6 THR N N 15 557.24 8.86 . . . . . 5996 6 4 . 1 1 10 10 PHE N N 15 667.60 21.1 . . . . . 5996 6 5 . 1 1 11 11 ASN N N 15 634.06 6.62 . . . . . 5996 6 6 . 1 1 12 12 VAL N N 15 735.70 7.04 . . . . . 5996 6 7 . 1 1 13 13 GLU N N 15 728.44 13.6 . . . . . 5996 6 8 . 1 1 16 16 ASN N N 15 673.84 13.6 . . . . . 5996 6 9 . 1 1 17 17 GLY N N 15 663.22 7.91 . . . . . 5996 6 10 . 1 1 18 18 GLU N N 15 648.59 12.3 . . . . . 5996 6 11 . 1 1 19 19 TRP N N 15 673.89 9.44 . . . . . 5996 6 12 . 1 1 21 21 THR N N 15 640.69 19.4 . . . . . 5996 6 13 . 1 1 22 22 ILE N N 15 654.44 6.62 . . . . . 5996 6 14 . 1 1 23 23 ILE N N 15 658.77 11.3 . . . . . 5996 6 15 . 1 1 26 26 SER N N 15 675.39 11.6 . . . . . 5996 6 16 . 1 1 27 27 ASP N N 15 621.58 25.8 . . . . . 5996 6 17 . 1 1 29 29 ARG N N 15 633.16 16.3 . . . . . 5996 6 18 . 1 1 30 30 GLU N N 15 617.94 12.4 . . . . . 5996 6 19 . 1 1 31 31 LYS N N 15 647.56 7.48 . . . . . 5996 6 20 . 1 1 32 32 ILE N N 15 588.62 15.2 . . . . . 5996 6 21 . 1 1 33 33 GLU N N 15 642.62 10.8 . . . . . 5996 6 22 . 1 1 35 35 ASN N N 15 620.10 24.4 . . . . . 5996 6 23 . 1 1 36 36 GLY N N 15 622.76 9.61 . . . . . 5996 6 24 . 1 1 38 38 PHE N N 15 629.70 11.1 . . . . . 5996 6 25 . 1 1 39 39 ARG N N 15 646.72 12.1 . . . . . 5996 6 26 . 1 1 40 40 LEU N N 15 702.56 7.90 . . . . . 5996 6 27 . 1 1 42 42 LEU N N 15 615.61 24.3 . . . . . 5996 6 28 . 1 1 43 43 GLU N N 15 615.91 5.69 . . . . . 5996 6 29 . 1 1 45 45 ILE N N 15 673.41 7.77 . . . . . 5996 6 30 . 1 1 46 46 HIS N N 15 688.15 9.79 . . . . . 5996 6 31 . 1 1 47 47 VAL N N 15 717.55 13.0 . . . . . 5996 6 32 . 1 1 48 48 LEU N N 15 665.36 3.57 . . . . . 5996 6 33 . 1 1 50 50 ASN N N 15 624.64 40.5 . . . . . 5996 6 34 . 1 1 51 51 SER N N 15 617.00 3.95 . . . . . 5996 6 35 . 1 1 52 52 LEU N N 15 673.54 7.89 . . . . . 5996 6 36 . 1 1 53 53 VAL N N 15 692.72 7.96 . . . . . 5996 6 37 . 1 1 54 54 LEU N N 15 666.46 5.77 . . . . . 5996 6 38 . 1 1 57 57 HIS N N 15 654.24 11.8 . . . . . 5996 6 39 . 1 1 60 60 ARG N N 15 650.73 6.01 . . . . . 5996 6 40 . 1 1 61 61 ASP N N 15 666.74 16.0 . . . . . 5996 6 41 . 1 1 62 62 GLU N N 15 663.00 3.19 . . . . . 5996 6 42 . 1 1 64 64 CYS N N 15 689.03 26.5 . . . . . 5996 6 43 . 1 1 65 65 SER N N 15 680.32 5.20 . . . . . 5996 6 44 . 1 1 66 66 GLU N N 15 687.98 9.06 . . . . . 5996 6 45 . 1 1 67 67 LEU N N 15 646.63 6.19 . . . . . 5996 6 46 . 1 1 68 68 SER N N 15 688.48 11.6 . . . . . 5996 6 47 . 1 1 69 69 MET N N 15 655.64 4.27 . . . . . 5996 6 48 . 1 1 71 71 ALA N N 15 659.93 4.10 . . . . . 5996 6 49 . 1 1 72 72 ASP N N 15 723.16 8.92 . . . . . 5996 6 50 . 1 1 74 74 THR N N 15 678.25 10.5 . . . . . 5996 6 51 . 1 1 75 75 GLU N N 15 676.99 14.4 . . . . . 5996 6 52 . 1 1 77 77 ALA N N 15 688.12 21.6 . . . . . 5996 6 53 . 1 1 78 78 GLY N N 15 688.71 26.9 . . . . . 5996 6 54 . 1 1 79 79 GLU N N 15 625.99 3.34 . . . . . 5996 6 55 . 1 1 80 80 TYR N N 15 644.81 7.79 . . . . . 5996 6 56 . 1 1 81 81 SER N N 15 649.11 3.02 . . . . . 5996 6 57 . 1 1 82 82 VAL N N 15 635.88 8.98 . . . . . 5996 6 58 . 1 1 84 84 TYR N N 15 715.46 7.99 . . . . . 5996 6 59 . 1 1 85 85 ASP N N 15 619.31 13.7 . . . . . 5996 6 60 . 1 1 86 86 GLY N N 15 652.64 6.42 . . . . . 5996 6 61 . 1 1 87 87 PHE N N 15 655.73 8.32 . . . . . 5996 6 62 . 1 1 88 88 ASN N N 15 685.76 6.93 . . . . . 5996 6 63 . 1 1 89 89 THR N N 15 647.86 7.47 . . . . . 5996 6 64 . 1 1 90 90 PHE N N 15 729.83 11.1 . . . . . 5996 6 65 . 1 1 91 91 THR N N 15 631.26 4.60 . . . . . 5996 6 66 . 1 1 92 92 ILE N N 15 645.24 9.26 . . . . . 5996 6 67 . 1 1 94 94 LYS N N 15 683.95 6.63 . . . . . 5996 6 68 . 1 1 95 95 THR N N 15 711.64 8.99 . . . . . 5996 6 69 . 1 1 96 96 ASP N N 15 652.45 14.3 . . . . . 5996 6 70 . 1 1 97 97 TYR N N 15 634.05 6.57 . . . . . 5996 6 71 . 1 1 98 98 ASP N N 15 635.11 5.53 . . . . . 5996 6 72 . 1 1 99 99 ASN N N 15 740.82 27.5 . . . . . 5996 6 73 . 1 1 100 100 PHE N N 15 693.45 5.80 . . . . . 5996 6 74 . 1 1 103 103 ALA N N 15 713.73 7.41 . . . . . 5996 6 75 . 1 1 104 104 HIS N N 15 734.68 5.55 . . . . . 5996 6 76 . 1 1 105 105 LEU N N 15 670.75 6.24 . . . . . 5996 6 77 . 1 1 107 107 ASN N N 15 635.62 5.77 . . . . . 5996 6 78 . 1 1 108 108 GLU N N 15 646.25 5.45 . . . . . 5996 6 79 . 1 1 109 109 LYS N N 15 649.57 6.19 . . . . . 5996 6 80 . 1 1 111 111 GLY N N 15 639.18 4.82 . . . . . 5996 6 81 . 1 1 114 114 PHE N N 15 687.11 4.07 . . . . . 5996 6 82 . 1 1 115 115 GLN N N 15 648.16 4.23 . . . . . 5996 6 83 . 1 1 116 116 LEU N N 15 673.39 4.91 . . . . . 5996 6 84 . 1 1 117 117 MET N N 15 701.62 6.70 . . . . . 5996 6 85 . 1 1 118 118 GLY N N 15 695.70 5.15 . . . . . 5996 6 86 . 1 1 121 121 GLY N N 15 673.49 3.48 . . . . . 5996 6 87 . 1 1 123 123 GLU N N 15 651.31 3.39 . . . . . 5996 6 88 . 1 1 125 125 ASP N N 15 664.39 8.75 . . . . . 5996 6 89 . 1 1 126 126 LEU N N 15 744.03 11.0 . . . . . 5996 6 90 . 1 1 127 127 SER N N 15 678.94 4.07 . . . . . 5996 6 91 . 1 1 129 129 ASP N N 15 654.72 9.14 . . . . . 5996 6 92 . 1 1 130 130 ILE N N 15 666.37 7.96 . . . . . 5996 6 93 . 1 1 131 131 LYS N N 15 637.60 4.47 . . . . . 5996 6 94 . 1 1 133 133 ARG N N 15 643.71 8.76 . . . . . 5996 6 95 . 1 1 136 136 GLN N N 15 653.30 10.2 . . . . . 5996 6 96 . 1 1 137 137 LEU N N 15 661.77 14.5 . . . . . 5996 6 97 . 1 1 138 138 CYS N N 15 647.43 25.3 . . . . . 5996 6 98 . 1 1 140 140 LYS N N 15 669.47 11.3 . . . . . 5996 6 99 . 1 1 142 142 GLY N N 15 724.49 16.7 . . . . . 5996 6 100 . 1 1 143 143 ILE N N 15 664.55 10.4 . . . . . 5996 6 101 . 1 1 144 144 LEU N N 15 726.21 8.83 . . . . . 5996 6 102 . 1 1 145 145 ARG N N 15 702.67 7.10 . . . . . 5996 6 103 . 1 1 146 146 GLU N N 15 648.37 14.9 . . . . . 5996 6 104 . 1 1 148 148 ILE N N 15 669.45 5.81 . . . . . 5996 6 105 . 1 1 150 150 ASP N N 15 706.20 8.85 . . . . . 5996 6 106 . 1 1 151 151 LEU N N 15 702.85 7.51 . . . . . 5996 6 107 . 1 1 152 152 SER N N 15 587.11 8.45 . . . . . 5996 6 108 . 1 1 153 153 ASN N N 15 591.28 19.1 . . . . . 5996 6 109 . 1 1 155 155 ASN N N 15 601.52 13.9 . . . . . 5996 6 110 . 1 1 160 160 ALA N N 15 652.71 17.8 . . . . . 5996 6 111 . 1 1 162 162 GLU N N 15 966.01 7.73 . . . . . 5996 6 stop_ save_ save_291_500_bound_t1 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode 291_500_bound_t1 _Heteronucl_T1_list.Entry_ID 5996 _Heteronucl_T1_list.ID 7 _Heteronucl_T1_list.Sample_condition_list_ID 7 _Heteronucl_T1_list.Sample_condition_list_label $291K _Heteronucl_T1_list.Spectrometer_frequency_1H 500 _Heteronucl_T1_list.T1_coherence_type Nz _Heteronucl_T1_list.T1_val_units ms _Heteronucl_T1_list.Details . _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID 1 '15N T1' 1 $sample_1 . 5996 7 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 3 3 ALA N N 15 842.01 13.16 . . . . . 5996 7 2 . 1 1 4 4 SER N N 15 880.14 28.27 . . . . . 5996 7 3 . 1 1 5 5 SER N N 15 807.37 32.16 . . . . . 5996 7 4 . 1 1 6 6 THR N N 15 802.51 35.76 . . . . . 5996 7 5 . 1 1 7 7 GLY N N 15 906.01 58.99 . . . . . 5996 7 6 . 1 1 11 11 ASN N N 15 851.83 64.52 . . . . . 5996 7 7 . 1 1 13 13 GLU N N 15 784.44 13.40 . . . . . 5996 7 8 . 1 1 15 15 ILE N N 15 789.58 6.809 . . . . . 5996 7 9 . 1 1 16 16 ASN N N 15 742.53 10.53 . . . . . 5996 7 10 . 1 1 17 17 GLY N N 15 728.14 18.29 . . . . . 5996 7 11 . 1 1 18 18 GLU N N 15 736.57 47.10 . . . . . 5996 7 12 . 1 1 19 19 TRP N N 15 776.25 42.14 . . . . . 5996 7 13 . 1 1 20 20 HIS N N 15 817.62 31.58 . . . . . 5996 7 14 . 1 1 22 22 ILE N N 15 805.96 74.75 . . . . . 5996 7 15 . 1 1 23 23 ILE N N 15 804.56 33.55 . . . . . 5996 7 16 . 1 1 26 26 SER N N 15 765.12 19.98 . . . . . 5996 7 17 . 1 1 27 27 ASP N N 15 744.50 12.74 . . . . . 5996 7 18 . 1 1 29 29 ARG N N 15 739.02 22.71 . . . . . 5996 7 19 . 1 1 30 30 GLU N N 15 758.57 16.52 . . . . . 5996 7 20 . 1 1 31 31 LYS N N 15 767.10 21.15 . . . . . 5996 7 21 . 1 1 32 32 ILE N N 15 701.47 49.01 . . . . . 5996 7 22 . 1 1 33 33 GLU N N 15 777.75 23.18 . . . . . 5996 7 23 . 1 1 36 36 GLY N N 15 786.20 47.74 . . . . . 5996 7 24 . 1 1 37 37 ASN N N 15 814.25 30.27 . . . . . 5996 7 25 . 1 1 39 39 ARG N N 15 780.67 29.71 . . . . . 5996 7 26 . 1 1 40 40 LEU N N 15 861.60 26.28 . . . . . 5996 7 27 . 1 1 45 45 ILE N N 15 752.25 17.78 . . . . . 5996 7 28 . 1 1 46 46 HIS N N 15 762.69 18.31 . . . . . 5996 7 29 . 1 1 47 47 VAL N N 15 756.93 20.98 . . . . . 5996 7 30 . 1 1 48 48 LEU N N 15 735.89 19.02 . . . . . 5996 7 31 . 1 1 50 50 ASN N N 15 851.36 30.47 . . . . . 5996 7 32 . 1 1 51 51 SER N N 15 802.14 13.40 . . . . . 5996 7 33 . 1 1 52 52 LEU N N 15 789.39 23.69 . . . . . 5996 7 34 . 1 1 54 54 LEU N N 15 764.21 20.45 . . . . . 5996 7 35 . 1 1 58 58 THR N N 15 744.23 30.35 . . . . . 5996 7 36 . 1 1 60 60 ARG N N 15 734.62 21.22 . . . . . 5996 7 37 . 1 1 61 61 ASP N N 15 759.23 18.94 . . . . . 5996 7 38 . 1 1 62 62 GLU N N 15 747.46 19.38 . . . . . 5996 7 39 . 1 1 64 64 CYS N N 15 835.43 23.58 . . . . . 5996 7 40 . 1 1 66 66 GLU N N 15 847.32 19.92 . . . . . 5996 7 41 . 1 1 67 67 LEU N N 15 764.33 22.10 . . . . . 5996 7 42 . 1 1 68 68 SER N N 15 808.48 16.04 . . . . . 5996 7 43 . 1 1 69 69 MET N N 15 749.11 27.56 . . . . . 5996 7 44 . 1 1 71 71 ALA N N 15 733.69 12.14 . . . . . 5996 7 45 . 1 1 72 72 ASP N N 15 818.67 20.24 . . . . . 5996 7 46 . 1 1 74 74 THR N N 15 808.98 25.78 . . . . . 5996 7 47 . 1 1 75 75 GLU N N 15 817.44 31.26 . . . . . 5996 7 48 . 1 1 77 77 ALA N N 15 857.55 23.16 . . . . . 5996 7 49 . 1 1 78 78 GLY N N 15 870.26 35.02 . . . . . 5996 7 50 . 1 1 79 79 GLU N N 15 784.85 27.01 . . . . . 5996 7 51 . 1 1 80 80 TYR N N 15 776.44 45.57 . . . . . 5996 7 52 . 1 1 81 81 SER N N 15 774.68 24.92 . . . . . 5996 7 53 . 1 1 82 82 VAL N N 15 775.75 30.66 . . . . . 5996 7 54 . 1 1 84 84 TYR N N 15 831.78 28.36 . . . . . 5996 7 55 . 1 1 85 85 ASP N N 15 786.57 26.12 . . . . . 5996 7 56 . 1 1 86 86 GLY N N 15 776.10 21.43 . . . . . 5996 7 57 . 1 1 87 87 PHE N N 15 767.39 27.98 . . . . . 5996 7 58 . 1 1 89 89 THR N N 15 774.78 12.91 . . . . . 5996 7 59 . 1 1 90 90 PHE N N 15 796.89 16.56 . . . . . 5996 7 60 . 1 1 91 91 THR N N 15 769.50 19.39 . . . . . 5996 7 61 . 1 1 94 94 LYS N N 15 793.80 18.14 . . . . . 5996 7 62 . 1 1 95 95 THR N N 15 828.74 31.83 . . . . . 5996 7 63 . 1 1 96 96 ASP N N 15 799.25 16.09 . . . . . 5996 7 64 . 1 1 98 98 ASP N N 15 816.13 30.03 . . . . . 5996 7 65 . 1 1 100 100 PHE N N 15 813.39 19.98 . . . . . 5996 7 66 . 1 1 103 103 ALA N N 15 797.49 34.36 . . . . . 5996 7 67 . 1 1 105 105 LEU N N 15 802.13 34.50 . . . . . 5996 7 68 . 1 1 107 107 ASN N N 15 783.50 25.42 . . . . . 5996 7 69 . 1 1 108 108 GLU N N 15 762.10 16.59 . . . . . 5996 7 70 . 1 1 109 109 LYS N N 15 786.93 24.19 . . . . . 5996 7 71 . 1 1 110 110 ASP N N 15 802.47 23.33 . . . . . 5996 7 72 . 1 1 111 111 GLY N N 15 790.38 23.03 . . . . . 5996 7 73 . 1 1 115 115 GLN N N 15 762.08 18.99 . . . . . 5996 7 74 . 1 1 117 117 MET N N 15 769.14 30.99 . . . . . 5996 7 75 . 1 1 118 118 GLY N N 15 840.01 36.14 . . . . . 5996 7 76 . 1 1 121 121 GLY N N 15 767.68 28.10 . . . . . 5996 7 77 . 1 1 123 123 GLU N N 15 840.38 29.22 . . . . . 5996 7 78 . 1 1 125 125 ASP N N 15 808.69 17.58 . . . . . 5996 7 79 . 1 1 126 126 LEU N N 15 876.89 27.39 . . . . . 5996 7 80 . 1 1 127 127 SER N N 15 857.28 28.89 . . . . . 5996 7 81 . 1 1 128 128 SER N N 15 879.95 31.59 . . . . . 5996 7 82 . 1 1 130 130 ILE N N 15 839.36 30.16 . . . . . 5996 7 83 . 1 1 131 131 LYS N N 15 788.81 30.25 . . . . . 5996 7 84 . 1 1 133 133 ARG N N 15 785.82 21.23 . . . . . 5996 7 85 . 1 1 136 136 GLN N N 15 748.72 12.19 . . . . . 5996 7 86 . 1 1 137 137 LEU N N 15 735.60 15.30 . . . . . 5996 7 87 . 1 1 138 138 CYS N N 15 744.62 20.67 . . . . . 5996 7 88 . 1 1 140 140 LYS N N 15 737.54 14.47 . . . . . 5996 7 89 . 1 1 141 141 HIS N N 15 806.95 10.68 . . . . . 5996 7 90 . 1 1 142 142 GLY N N 15 743.16 15.67 . . . . . 5996 7 91 . 1 1 144 144 LEU N N 15 753.38 12.71 . . . . . 5996 7 92 . 1 1 145 145 ARG N N 15 760.60 11.85 . . . . . 5996 7 93 . 1 1 146 146 GLU N N 15 753.75 10.32 . . . . . 5996 7 94 . 1 1 148 148 ILE N N 15 748.84 12.45 . . . . . 5996 7 95 . 1 1 150 150 ASP N N 15 775.61 21.26 . . . . . 5996 7 96 . 1 1 151 151 LEU N N 15 911.25 49.53 . . . . . 5996 7 97 . 1 1 152 152 SER N N 15 895.41 76.15 . . . . . 5996 7 98 . 1 1 153 153 ASN N N 15 854.57 46.46 . . . . . 5996 7 99 . 1 1 155 155 ASN N N 15 843.52 71.99 . . . . . 5996 7 100 . 1 1 160 160 ALA N N 15 678.43 19.73 . . . . . 5996 7 101 . 1 1 162 162 GLU N N 15 774.18 6.650 . . . . . 5996 7 stop_ save_ save_297_500_bound_t1 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode 297_500_bound_t1 _Heteronucl_T1_list.Entry_ID 5996 _Heteronucl_T1_list.ID 8 _Heteronucl_T1_list.Sample_condition_list_ID 8 _Heteronucl_T1_list.Sample_condition_list_label $297K _Heteronucl_T1_list.Spectrometer_frequency_1H 500 _Heteronucl_T1_list.T1_coherence_type Nz _Heteronucl_T1_list.T1_val_units ms _Heteronucl_T1_list.Details . _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID 1 '15N T1' 1 $sample_1 . 5996 8 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 3 3 ALA N N 15 753.03 28.87 . . . . . 5996 8 2 . 1 1 4 4 SER N N 15 783.99 24.55 . . . . . 5996 8 3 . 1 1 5 5 SER N N 15 729.60 20.11 . . . . . 5996 8 4 . 1 1 6 6 THR N N 15 707.50 25.96 . . . . . 5996 8 5 . 1 1 7 7 GLY N N 15 802.27 31.10 . . . . . 5996 8 6 . 1 1 10 10 PHE N N 15 844.43 25.17 . . . . . 5996 8 7 . 1 1 11 11 ASN N N 15 768.75 35.18 . . . . . 5996 8 8 . 1 1 12 12 VAL N N 15 708.24 14.54 . . . . . 5996 8 9 . 1 1 13 13 GLU N N 15 686.38 8.505 . . . . . 5996 8 10 . 1 1 15 15 ILE N N 15 633.70 10.33 . . . . . 5996 8 11 . 1 1 16 16 ASN N N 15 635.73 9.055 . . . . . 5996 8 12 . 1 1 17 17 GLY N N 15 626.88 11.45 . . . . . 5996 8 13 . 1 1 18 18 GLU N N 15 625.50 12.94 . . . . . 5996 8 14 . 1 1 19 19 TRP N N 15 687.15 23.63 . . . . . 5996 8 15 . 1 1 20 20 HIS N N 15 834.79 52.26 . . . . . 5996 8 16 . 1 1 21 21 THR N N 15 783.88 52.39 . . . . . 5996 8 17 . 1 1 22 22 ILE N N 15 670.50 33.08 . . . . . 5996 8 18 . 1 1 23 23 ILE N N 15 686.07 10.47 . . . . . 5996 8 19 . 1 1 26 26 SER N N 15 669.02 6.589 . . . . . 5996 8 20 . 1 1 27 27 ASP N N 15 636.54 11.89 . . . . . 5996 8 21 . 1 1 29 29 ARG N N 15 670.17 15.29 . . . . . 5996 8 22 . 1 1 30 30 GLU N N 15 666.87 10.25 . . . . . 5996 8 23 . 1 1 31 31 LYS N N 15 660.87 10.45 . . . . . 5996 8 24 . 1 1 32 32 ILE N N 15 631.41 20.96 . . . . . 5996 8 25 . 1 1 33 33 GLU N N 15 672.80 17.06 . . . . . 5996 8 26 . 1 1 36 36 GLY N N 15 707.14 37.21 . . . . . 5996 8 27 . 1 1 37 37 ASN N N 15 698.91 31.28 . . . . . 5996 8 28 . 1 1 42 42 LEU N N 15 717.45 54.76 . . . . . 5996 8 29 . 1 1 43 43 GLU N N 15 629.64 53.38 . . . . . 5996 8 30 . 1 1 45 45 ILE N N 15 648.03 15.65 . . . . . 5996 8 31 . 1 1 46 46 HIS N N 15 656.21 18.35 . . . . . 5996 8 32 . 1 1 47 47 VAL N N 15 656.85 16.98 . . . . . 5996 8 33 . 1 1 48 48 LEU N N 15 649.81 8.771 . . . . . 5996 8 34 . 1 1 50 50 ASN N N 15 747.43 35.98 . . . . . 5996 8 35 . 1 1 51 51 SER N N 15 704.37 14.12 . . . . . 5996 8 36 . 1 1 52 52 LEU N N 15 661.52 19.20 . . . . . 5996 8 37 . 1 1 54 54 LEU N N 15 634.93 17.49 . . . . . 5996 8 38 . 1 1 57 57 HIS N N 15 704.89 22.35 . . . . . 5996 8 39 . 1 1 58 58 THR N N 15 707.29 23.11 . . . . . 5996 8 40 . 1 1 60 60 ARG N N 15 654.03 14.91 . . . . . 5996 8 41 . 1 1 62 62 GLU N N 15 647.68 9.101 . . . . . 5996 8 42 . 1 1 64 64 CYS N N 15 711.17 13.2 . . . . . 5996 8 43 . 1 1 65 65 SER N N 15 716.88 30.85 . . . . . 5996 8 44 . 1 1 66 66 GLU N N 15 730.41 15.38 . . . . . 5996 8 45 . 1 1 67 67 LEU N N 15 668.01 23.35 . . . . . 5996 8 46 . 1 1 68 68 SER N N 15 702.34 12.93 . . . . . 5996 8 47 . 1 1 69 69 MET N N 15 639.94 11.10 . . . . . 5996 8 48 . 1 1 71 71 ALA N N 15 638.24 15.61 . . . . . 5996 8 49 . 1 1 74 74 THR N N 15 705.68 18.66 . . . . . 5996 8 50 . 1 1 75 75 GLU N N 15 747.75 11.86 . . . . . 5996 8 51 . 1 1 77 77 ALA N N 15 765.40 20.71 . . . . . 5996 8 52 . 1 1 78 78 GLY N N 15 793.66 30.26 . . . . . 5996 8 53 . 1 1 79 79 GLU N N 15 709.62 24.55 . . . . . 5996 8 54 . 1 1 80 80 TYR N N 15 652.38 18.22 . . . . . 5996 8 55 . 1 1 81 81 SER N N 15 680.21 16.43 . . . . . 5996 8 56 . 1 1 82 82 VAL N N 15 670.04 12.41 . . . . . 5996 8 57 . 1 1 84 84 TYR N N 15 734.21 15.44 . . . . . 5996 8 58 . 1 1 85 85 ASP N N 15 682.80 14.20 . . . . . 5996 8 59 . 1 1 87 87 PHE N N 15 667.24 16.74 . . . . . 5996 8 60 . 1 1 89 89 THR N N 15 657.91 12.52 . . . . . 5996 8 61 . 1 1 90 90 PHE N N 15 711.52 14.08 . . . . . 5996 8 62 . 1 1 91 91 THR N N 15 678.14 19.31 . . . . . 5996 8 63 . 1 1 92 92 ILE N N 15 725.06 21.31 . . . . . 5996 8 64 . 1 1 94 94 LYS N N 15 691.91 12.84 . . . . . 5996 8 65 . 1 1 95 95 THR N N 15 698.14 18.53 . . . . . 5996 8 66 . 1 1 97 97 TYR N N 15 625.62 11.03 . . . . . 5996 8 67 . 1 1 98 98 ASP N N 15 616.46 19.13 . . . . . 5996 8 68 . 1 1 100 100 PHE N N 15 703.34 19.58 . . . . . 5996 8 69 . 1 1 103 103 ALA N N 15 701.00 28.00 . . . . . 5996 8 70 . 1 1 104 104 HIS N N 15 692.54 5.442 . . . . . 5996 8 71 . 1 1 105 105 LEU N N 15 678.14 20.04 . . . . . 5996 8 72 . 1 1 107 107 ASN N N 15 649.68 11.58 . . . . . 5996 8 73 . 1 1 108 108 GLU N N 15 670.37 19.80 . . . . . 5996 8 74 . 1 1 109 109 LYS N N 15 686.13 16.8 . . . . . 5996 8 75 . 1 1 110 110 ASP N N 15 719.83 23.47 . . . . . 5996 8 76 . 1 1 111 111 GLY N N 15 703.11 12.21 . . . . . 5996 8 77 . 1 1 113 113 THR N N 15 692.80 10.68 . . . . . 5996 8 78 . 1 1 115 115 GLN N N 15 660.03 13.31 . . . . . 5996 8 79 . 1 1 117 117 MET N N 15 657.84 17.84 . . . . . 5996 8 80 . 1 1 118 118 GLY N N 15 701.88 26.41 . . . . . 5996 8 81 . 1 1 121 121 GLY N N 15 681.11 18.12 . . . . . 5996 8 82 . 1 1 123 123 GLU N N 15 702.34 13.48 . . . . . 5996 8 83 . 1 1 125 125 ASP N N 15 677.34 14.37 . . . . . 5996 8 84 . 1 1 126 126 LEU N N 15 769.45 19.16 . . . . . 5996 8 85 . 1 1 127 127 SER N N 15 720.61 22.73 . . . . . 5996 8 86 . 1 1 128 128 SER N N 15 773.37 40.81 . . . . . 5996 8 87 . 1 1 129 129 ASP N N 15 650.21 11.79 . . . . . 5996 8 88 . 1 1 130 130 ILE N N 15 726.83 17.22 . . . . . 5996 8 89 . 1 1 131 131 LYS N N 15 683.99 26.48 . . . . . 5996 8 90 . 1 1 133 133 ARG N N 15 671.36 14.84 . . . . . 5996 8 91 . 1 1 136 136 GLN N N 15 640.87 14.62 . . . . . 5996 8 92 . 1 1 137 137 LEU N N 15 641.75 8.964 . . . . . 5996 8 93 . 1 1 138 138 CYS N N 15 665.22 11.79 . . . . . 5996 8 94 . 1 1 140 140 LYS N N 15 647.14 9.142 . . . . . 5996 8 95 . 1 1 141 141 HIS N N 15 697.53 12.54 . . . . . 5996 8 96 . 1 1 142 142 GLY N N 15 663.77 7.617 . . . . . 5996 8 97 . 1 1 144 144 LEU N N 15 678.41 15.66 . . . . . 5996 8 98 . 1 1 145 145 ARG N N 15 680.65 6.304 . . . . . 5996 8 99 . 1 1 146 146 GLU N N 15 652.26 12.49 . . . . . 5996 8 100 . 1 1 148 148 ILE N N 15 662.48 8.285 . . . . . 5996 8 101 . 1 1 150 150 ASP N N 15 680.44 9.213 . . . . . 5996 8 102 . 1 1 151 151 LEU N N 15 739.00 22.55 . . . . . 5996 8 103 . 1 1 152 152 SER N N 15 703.89 27.66 . . . . . 5996 8 104 . 1 1 153 153 ASN N N 15 724.86 23.42 . . . . . 5996 8 105 . 1 1 155 155 ASN N N 15 728.87 67.13 . . . . . 5996 8 106 . 1 1 160 160 ALA N N 15 682.55 18.08 . . . . . 5996 8 107 . 1 1 162 162 GLU N N 15 803.48 6.180 . . . . . 5996 8 stop_ save_ save_302_500_bound_t1 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode 302_500_bound_t1 _Heteronucl_T1_list.Entry_ID 5996 _Heteronucl_T1_list.ID 9 _Heteronucl_T1_list.Sample_condition_list_ID 9 _Heteronucl_T1_list.Sample_condition_list_label $302K _Heteronucl_T1_list.Spectrometer_frequency_1H 500 _Heteronucl_T1_list.T1_coherence_type Nz _Heteronucl_T1_list.T1_val_units ms _Heteronucl_T1_list.Details . _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID 1 '15N T1' 1 $sample_1 . 5996 9 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 3 3 ALA N N 15 680.48 7.96 . . . . . 5996 9 2 . 1 1 4 4 SER N N 15 694.45 14.8 . . . . . 5996 9 3 . 1 1 6 6 THR N N 15 563.04 35.0 . . . . . 5996 9 4 . 1 1 10 10 PHE N N 15 764.20 19.9 . . . . . 5996 9 5 . 1 1 11 11 ASN N N 15 660.73 15.5 . . . . . 5996 9 6 . 1 1 12 12 VAL N N 15 635.77 22.9 . . . . . 5996 9 7 . 1 1 13 13 GLU N N 15 601.41 17.8 . . . . . 5996 9 8 . 1 1 16 16 ASN N N 15 550.30 37.0 . . . . . 5996 9 9 . 1 1 17 17 GLY N N 15 572.61 11.3 . . . . . 5996 9 10 . 1 1 18 18 GLU N N 15 630.80 12.4 . . . . . 5996 9 11 . 1 1 19 19 TRP N N 15 611.57 21.8 . . . . . 5996 9 12 . 1 1 21 21 THR N N 15 728.15 40.0 . . . . . 5996 9 13 . 1 1 22 22 ILE N N 15 620.45 21.8 . . . . . 5996 9 14 . 1 1 23 23 ILE N N 15 608.92 24.8 . . . . . 5996 9 15 . 1 1 26 26 SER N N 15 582.78 17.6 . . . . . 5996 9 16 . 1 1 27 27 ASP N N 15 570.76 17.4 . . . . . 5996 9 17 . 1 1 29 29 ARG N N 15 603.86 5.59 . . . . . 5996 9 18 . 1 1 30 30 GLU N N 15 591.68 9.31 . . . . . 5996 9 19 . 1 1 31 31 LYS N N 15 589.16 13.0 . . . . . 5996 9 20 . 1 1 32 32 ILE N N 15 551.87 8.44 . . . . . 5996 9 21 . 1 1 33 33 GLU N N 15 479.69 107. . . . . . 5996 9 22 . 1 1 35 35 ASN N N 15 627.20 18.7 . . . . . 5996 9 23 . 1 1 36 36 GLY N N 15 594.19 15.7 . . . . . 5996 9 24 . 1 1 39 39 ARG N N 15 551.80 40.0 . . . . . 5996 9 25 . 1 1 40 40 LEU N N 15 562.64 101. . . . . . 5996 9 26 . 1 1 42 42 LEU N N 15 605.23 44.6 . . . . . 5996 9 27 . 1 1 43 43 GLU N N 15 572.28 14.5 . . . . . 5996 9 28 . 1 1 46 46 HIS N N 15 591.66 15.9 . . . . . 5996 9 29 . 1 1 47 47 VAL N N 15 611.63 7.64 . . . . . 5996 9 30 . 1 1 48 48 LEU N N 15 587.86 11.3 . . . . . 5996 9 31 . 1 1 50 50 ASN N N 15 725.17 36.9 . . . . . 5996 9 32 . 1 1 51 51 SER N N 15 628.38 13.1 . . . . . 5996 9 33 . 1 1 52 52 LEU N N 15 615.30 10.2 . . . . . 5996 9 34 . 1 1 54 54 LEU N N 15 579.91 9.28 . . . . . 5996 9 35 . 1 1 60 60 ARG N N 15 593.62 13.7 . . . . . 5996 9 36 . 1 1 61 61 ASP N N 15 619.58 10.7 . . . . . 5996 9 37 . 1 1 62 62 GLU N N 15 617.78 18.0 . . . . . 5996 9 38 . 1 1 64 64 CYS N N 15 667.42 9.27 . . . . . 5996 9 39 . 1 1 65 65 SER N N 15 667.34 21.5 . . . . . 5996 9 40 . 1 1 66 66 GLU N N 15 650.54 8.94 . . . . . 5996 9 41 . 1 1 67 67 LEU N N 15 601.76 12.4 . . . . . 5996 9 42 . 1 1 68 68 SER N N 15 642.49 10.7 . . . . . 5996 9 43 . 1 1 69 69 MET N N 15 605.78 17.1 . . . . . 5996 9 44 . 1 1 71 71 ALA N N 15 579.72 8.28 . . . . . 5996 9 45 . 1 1 74 74 THR N N 15 625.14 16.5 . . . . . 5996 9 46 . 1 1 75 75 GLU N N 15 655.74 15.4 . . . . . 5996 9 47 . 1 1 77 77 ALA N N 15 685.44 18.0 . . . . . 5996 9 48 . 1 1 79 79 GLU N N 15 607.62 18.5 . . . . . 5996 9 49 . 1 1 81 81 SER N N 15 604.48 9.91 . . . . . 5996 9 50 . 1 1 82 82 VAL N N 15 584.27 8.11 . . . . . 5996 9 51 . 1 1 84 84 TYR N N 15 613.25 12.2 . . . . . 5996 9 52 . 1 1 85 85 ASP N N 15 626.19 15.5 . . . . . 5996 9 53 . 1 1 86 86 GLY N N 15 602.77 8.27 . . . . . 5996 9 54 . 1 1 88 88 ASN N N 15 608.73 21.4 . . . . . 5996 9 55 . 1 1 89 89 THR N N 15 577.26 12.5 . . . . . 5996 9 56 . 1 1 90 90 PHE N N 15 645.39 16.5 . . . . . 5996 9 57 . 1 1 91 91 THR N N 15 584.63 8.18 . . . . . 5996 9 58 . 1 1 94 94 LYS N N 15 568.84 57.8 . . . . . 5996 9 59 . 1 1 96 96 ASP N N 15 537.47 63.0 . . . . . 5996 9 60 . 1 1 97 97 TYR N N 15 569.26 16.3 . . . . . 5996 9 61 . 1 1 98 98 ASP N N 15 584.39 5.48 . . . . . 5996 9 62 . 1 1 99 99 ASN N N 15 608.22 11.0 . . . . . 5996 9 63 . 1 1 100 100 PHE N N 15 640.18 11.47 . . . . . 5996 9 64 . 1 1 101 101 LEU N N 15 599.50 15.08 . . . . . 5996 9 65 . 1 1 103 103 ALA N N 15 614.60 18.47 . . . . . 5996 9 66 . 1 1 104 104 HIS N N 15 655.19 10.28 . . . . . 5996 9 67 . 1 1 105 105 LEU N N 15 605.87 14.50 . . . . . 5996 9 68 . 1 1 107 107 ASN N N 15 548.29 8.27 . . . . . 5996 9 69 . 1 1 108 108 GLU N N 15 595.61 9.71 . . . . . 5996 9 70 . 1 1 110 110 ASP N N 15 638.75 30.82 . . . . . 5996 9 71 . 1 1 111 111 GLY N N 15 644.36 7.01 . . . . . 5996 9 72 . 1 1 113 113 THR N N 15 635.06 6.63 . . . . . 5996 9 73 . 1 1 115 115 GLN N N 15 609.53 8.28 . . . . . 5996 9 74 . 1 1 116 116 LEU N N 15 607.05 9.54 . . . . . 5996 9 75 . 1 1 117 117 MET N N 15 602.40 8.59 . . . . . 5996 9 76 . 1 1 121 121 GLY N N 15 606.99 19.08 . . . . . 5996 9 77 . 1 1 125 125 ASP N N 15 610.23 33.22 . . . . . 5996 9 78 . 1 1 127 127 SER N N 15 637.45 14.97 . . . . . 5996 9 79 . 1 1 128 128 SER N N 15 727.34 26.67 . . . . . 5996 9 80 . 1 1 129 129 ASP N N 15 617.98 16.21 . . . . . 5996 9 81 . 1 1 130 130 ILE N N 15 626.67 21.42 . . . . . 5996 9 82 . 1 1 131 131 LYS N N 15 597.38 12.26 . . . . . 5996 9 83 . 1 1 133 133 ARG N N 15 573.41 10.58 . . . . . 5996 9 84 . 1 1 136 136 GLN N N 15 555.51 16.62 . . . . . 5996 9 85 . 1 1 137 137 LEU N N 15 588.94 15.71 . . . . . 5996 9 86 . 1 1 138 138 CYS N N 15 572.33 17.01 . . . . . 5996 9 87 . 1 1 140 140 LYS N N 15 567.04 10.15 . . . . . 5996 9 88 . 1 1 141 141 HIS N N 15 614.00 19.13 . . . . . 5996 9 89 . 1 1 142 142 GLY N N 15 598.99 9.31 . . . . . 5996 9 90 . 1 1 144 144 LEU N N 15 607.05 14.83 . . . . . 5996 9 91 . 1 1 145 145 ARG N N 15 642.01 8.44 . . . . . 5996 9 92 . 1 1 146 146 GLU N N 15 602.61 4.77 . . . . . 5996 9 93 . 1 1 148 148 ILE N N 15 557.44 41.01 . . . . . 5996 9 94 . 1 1 150 150 ASP N N 15 613.52 8.55 . . . . . 5996 9 95 . 1 1 151 151 LEU N N 15 665.63 21.26 . . . . . 5996 9 96 . 1 1 152 152 SER N N 15 638.16 14.15 . . . . . 5996 9 97 . 1 1 153 153 ASN N N 15 631.58 17.90 . . . . . 5996 9 98 . 1 1 155 155 ASN N N 15 603.11 26.27 . . . . . 5996 9 99 . 1 1 160 160 ALA N N 15 698.72 12.67 . . . . . 5996 9 100 . 1 1 162 162 GLU N N 15 874.36 23.31 . . . . . 5996 9 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_283_600_bound_t2 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 283_600_bound_t2 _Heteronucl_T2_list.Entry_ID 5996 _Heteronucl_T2_list.ID 1 _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $283K _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 600 _Heteronucl_T2_list.T2_coherence_type Nx _Heteronucl_T2_list.T2_val_units ms _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 1 '15N T2' 1 $sample_1 . 5996 1 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 ALA N N 15 56.03 2.72 . . . . . . . 5996 1 2 . 1 1 4 4 SER N N 15 57.05 3.62 . . . . . . . 5996 1 3 . 1 1 5 5 SER N N 15 47.09 1.45 . . . . . . . 5996 1 4 . 1 1 6 6 THR N N 15 48.21 1.67 . . . . . . . 5996 1 5 . 1 1 7 7 GLY N N 15 51.15 1.70 . . . . . . . 5996 1 6 . 1 1 10 10 PHE N N 15 56.37 1.52 . . . . . . . 5996 1 7 . 1 1 11 11 ASN N N 15 53.45 0.88 . . . . . . . 5996 1 8 . 1 1 12 12 VAL N N 15 54.11 2.92 . . . . . . . 5996 1 9 . 1 1 13 13 GLU N N 15 50.33 2.26 . . . . . . . 5996 1 10 . 1 1 15 15 ILE N N 15 54.61 2.10 . . . . . . . 5996 1 11 . 1 1 16 16 ASN N N 15 47.01 1.96 . . . . . . . 5996 1 12 . 1 1 17 17 GLY N N 15 58.26 3.94 . . . . . . . 5996 1 13 . 1 1 18 18 GLU N N 15 128.45 9.05 . . . . . . . 5996 1 14 . 1 1 22 22 ILE N N 15 51.42 3.08 . . . . . . . 5996 1 15 . 1 1 23 23 ILE N N 15 53.49 2.26 . . . . . . . 5996 1 16 . 1 1 26 26 SER N N 15 52.63 3.00 . . . . . . . 5996 1 17 . 1 1 27 27 ASP N N 15 48.78 1.88 . . . . . . . 5996 1 18 . 1 1 29 29 ARG N N 15 63.74 3.06 . . . . . . . 5996 1 19 . 1 1 30 30 GLU N N 15 55.23 2.17 . . . . . . . 5996 1 20 . 1 1 31 31 LYS N N 15 50.50 3.09 . . . . . . . 5996 1 21 . 1 1 32 32 ILE N N 15 55.64 1.51 . . . . . . . 5996 1 22 . 1 1 33 33 GLU N N 15 53.54 1.64 . . . . . . . 5996 1 23 . 1 1 36 36 GLY N N 15 49.67 1.35 . . . . . . . 5996 1 24 . 1 1 37 37 ASN N N 15 50.43 2.56 . . . . . . . 5996 1 25 . 1 1 38 38 PHE N N 15 50.33 2.21 . . . . . . . 5996 1 26 . 1 1 46 46 HIS N N 15 52.53 3.39 . . . . . . . 5996 1 27 . 1 1 48 48 LEU N N 15 57.00 1.88 . . . . . . . 5996 1 28 . 1 1 50 50 ASN N N 15 55.31 2.06 . . . . . . . 5996 1 29 . 1 1 51 51 SER N N 15 56.93 2.78 . . . . . . . 5996 1 30 . 1 1 52 52 LEU N N 15 55.46 3.03 . . . . . . . 5996 1 31 . 1 1 54 54 LEU N N 15 56.57 3.01 . . . . . . . 5996 1 32 . 1 1 55 55 LYS N N 15 52.41 2.33 . . . . . . . 5996 1 33 . 1 1 61 61 ASP N N 15 55.25 3.97 . . . . . . . 5996 1 34 . 1 1 66 66 GLU N N 15 53.73 2.79 . . . . . . . 5996 1 35 . 1 1 67 67 LEU N N 15 55.69 2.57 . . . . . . . 5996 1 36 . 1 1 68 68 SER N N 15 49.87 2.71 . . . . . . . 5996 1 37 . 1 1 70 70 VAL N N 15 54.34 2.30 . . . . . . . 5996 1 38 . 1 1 71 71 ALA N N 15 57.85 2.56 . . . . . . . 5996 1 39 . 1 1 72 72 ASP N N 15 52.64 1.80 . . . . . . . 5996 1 40 . 1 1 74 74 THR N N 15 60.69 2.53 . . . . . . . 5996 1 41 . 1 1 75 75 GLU N N 15 61.77 3.00 . . . . . . . 5996 1 42 . 1 1 76 76 LYS N N 15 52.75 2.16 . . . . . . . 5996 1 43 . 1 1 78 78 GLY N N 15 60.86 1.46 . . . . . . . 5996 1 44 . 1 1 79 79 GLU N N 15 47.25 2.03 . . . . . . . 5996 1 45 . 1 1 80 80 TYR N N 15 54.92 3.12 . . . . . . . 5996 1 46 . 1 1 81 81 SER N N 15 54.77 2.21 . . . . . . . 5996 1 47 . 1 1 82 82 VAL N N 15 53.87 1.86 . . . . . . . 5996 1 48 . 1 1 84 84 TYR N N 15 54.73 1.93 . . . . . . . 5996 1 49 . 1 1 85 85 ASP N N 15 57.09 2.34 . . . . . . . 5996 1 50 . 1 1 86 86 GLY N N 15 52.09 2.02 . . . . . . . 5996 1 51 . 1 1 89 89 THR N N 15 54.83 2.93 . . . . . . . 5996 1 52 . 1 1 90 90 PHE N N 15 49.44 2.21 . . . . . . . 5996 1 53 . 1 1 91 91 THR N N 15 55.86 2.28 . . . . . . . 5996 1 54 . 1 1 92 92 ILE N N 15 49.14 1.29 . . . . . . . 5996 1 55 . 1 1 94 94 LYS N N 15 52.36 2.56 . . . . . . . 5996 1 56 . 1 1 96 96 ASP N N 15 48.22 1.27 . . . . . . . 5996 1 57 . 1 1 98 98 ASP N N 15 52.57 1.70 . . . . . . . 5996 1 58 . 1 1 100 100 PHE N N 15 50.16 2.12 . . . . . . . 5996 1 59 . 1 1 101 101 LEU N N 15 49.40 4.04 . . . . . . . 5996 1 60 . 1 1 103 103 ALA N N 15 52.75 2.46 . . . . . . . 5996 1 61 . 1 1 104 104 HIS N N 15 60.28 3.09 . . . . . . . 5996 1 62 . 1 1 105 105 LEU N N 15 52.51 3.05 . . . . . . . 5996 1 63 . 1 1 107 107 ASN N N 15 57.31 4.33 . . . . . . . 5996 1 64 . 1 1 108 108 GLU N N 15 53.82 2.14 . . . . . . . 5996 1 65 . 1 1 109 109 LYS N N 15 56.62 2.83 . . . . . . . 5996 1 66 . 1 1 110 110 ASP N N 15 54.75 1.18 . . . . . . . 5996 1 67 . 1 1 111 111 GLY N N 15 56.49 2.43 . . . . . . . 5996 1 68 . 1 1 113 113 THR N N 15 59.63 1.89 . . . . . . . 5996 1 69 . 1 1 114 114 PHE N N 15 61.87 3.90 . . . . . . . 5996 1 70 . 1 1 115 115 GLN N N 15 53.25 1.12 . . . . . . . 5996 1 71 . 1 1 116 116 LEU N N 15 49.91 2.25 . . . . . . . 5996 1 72 . 1 1 117 117 MET N N 15 50.01 2.09 . . . . . . . 5996 1 73 . 1 1 118 118 GLY N N 15 48.02 2.58 . . . . . . . 5996 1 74 . 1 1 119 119 LEU N N 15 48.97 2.07 . . . . . . . 5996 1 75 . 1 1 121 121 GLY N N 15 48.21 3.92 . . . . . . . 5996 1 76 . 1 1 123 123 GLU N N 15 58.07 2.59 . . . . . . . 5996 1 77 . 1 1 125 125 ASP N N 15 48.49 2.12 . . . . . . . 5996 1 78 . 1 1 126 126 LEU N N 15 52.00 2.35 . . . . . . . 5996 1 79 . 1 1 127 127 SER N N 15 56.27 2.36 . . . . . . . 5996 1 80 . 1 1 129 129 ASP N N 15 49.35 1.59 . . . . . . . 5996 1 81 . 1 1 130 130 ILE N N 15 47.80 2.60 . . . . . . . 5996 1 82 . 1 1 131 131 LYS N N 15 47.67 2.22 . . . . . . . 5996 1 83 . 1 1 133 133 ARG N N 15 48.89 1.74 . . . . . . . 5996 1 84 . 1 1 135 135 ALA N N 15 51.47 2.63 . . . . . . . 5996 1 85 . 1 1 136 136 GLN N N 15 55.29 2.46 . . . . . . . 5996 1 86 . 1 1 137 137 LEU N N 15 49.87 2.43 . . . . . . . 5996 1 87 . 1 1 138 138 CYS N N 15 51.87 2.36 . . . . . . . 5996 1 88 . 1 1 140 140 LYS N N 15 53.01 3.35 . . . . . . . 5996 1 89 . 1 1 141 141 HIS N N 15 54.76 0.80 . . . . . . . 5996 1 90 . 1 1 142 142 GLY N N 15 53.66 2.08 . . . . . . . 5996 1 91 . 1 1 144 144 LEU N N 15 61.40 3.62 . . . . . . . 5996 1 92 . 1 1 145 145 ARG N N 15 63.33 2.17 . . . . . . . 5996 1 93 . 1 1 148 148 ILE N N 15 56.96 2.40 . . . . . . . 5996 1 94 . 1 1 151 151 LEU N N 15 50.91 1.75 . . . . . . . 5996 1 95 . 1 1 152 152 SER N N 15 49.16 1.29 . . . . . . . 5996 1 96 . 1 1 162 162 GLU N N 15 178.30 9.15 . . . . . . . 5996 1 stop_ save_ save_288_600_bound_t2 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 288_600_bound_t2 _Heteronucl_T2_list.Entry_ID 5996 _Heteronucl_T2_list.ID 2 _Heteronucl_T2_list.Sample_condition_list_ID 2 _Heteronucl_T2_list.Sample_condition_list_label $288K _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 600 _Heteronucl_T2_list.T2_coherence_type Nx _Heteronucl_T2_list.T2_val_units ms _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 1 '15N T2' 1 $sample_1 . 5996 2 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 ALA N N 15 70.24 3.28 . . . . . . . 5996 2 2 . 1 1 4 4 SER N N 15 72.43 3.00 . . . . . . . 5996 2 3 . 1 1 5 5 SER N N 15 60.93 3.06 . . . . . . . 5996 2 4 . 1 1 6 6 THR N N 15 61.25 2.15 . . . . . . . 5996 2 5 . 1 1 7 7 GLY N N 15 73.00 3.59 . . . . . . . 5996 2 6 . 1 1 10 10 PHE N N 15 72.99 2.01 . . . . . . . 5996 2 7 . 1 1 12 12 VAL N N 15 66.91 2.64 . . . . . . . 5996 2 8 . 1 1 13 13 GLU N N 15 57.84 1.69 . . . . . . . 5996 2 9 . 1 1 15 15 ILE N N 15 70.27 3.15 . . . . . . . 5996 2 10 . 1 1 16 16 ASN N N 15 60.34 2.58 . . . . . . . 5996 2 11 . 1 1 17 17 GLY N N 15 70.39 3.33 . . . . . . . 5996 2 12 . 1 1 18 18 GLU N N 15 147.78 9.00 . . . . . . . 5996 2 13 . 1 1 19 19 TRP N N 15 62.04 3.48 . . . . . . . 5996 2 14 . 1 1 20 20 HIS N N 15 52.04 3.46 . . . . . . . 5996 2 15 . 1 1 21 21 THR N N 15 62.83 2.71 . . . . . . . 5996 2 16 . 1 1 22 22 ILE N N 15 62.41 3.83 . . . . . . . 5996 2 17 . 1 1 23 23 ILE N N 15 68.43 2.74 . . . . . . . 5996 2 18 . 1 1 26 26 SER N N 15 70.11 3.45 . . . . . . . 5996 2 19 . 1 1 27 27 ASP N N 15 67.39 2.36 . . . . . . . 5996 2 20 . 1 1 29 29 ARG N N 15 71.87 1.94 . . . . . . . 5996 2 21 . 1 1 30 30 GLU N N 15 67.63 2.54 . . . . . . . 5996 2 22 . 1 1 31 31 LYS N N 15 62.85 3.05 . . . . . . . 5996 2 23 . 1 1 32 32 ILE N N 15 66.67 2.80 . . . . . . . 5996 2 24 . 1 1 33 33 GLU N N 15 65.93 3.14 . . . . . . . 5996 2 25 . 1 1 35 35 ASN N N 15 65.28 2.39 . . . . . . . 5996 2 26 . 1 1 36 36 GLY N N 15 63.02 2.31 . . . . . . . 5996 2 27 . 1 1 37 37 ASN N N 15 60.19 2.38 . . . . . . . 5996 2 28 . 1 1 38 38 PHE N N 15 65.12 2.24 . . . . . . . 5996 2 29 . 1 1 39 39 ARG N N 15 60.84 2.71 . . . . . . . 5996 2 30 . 1 1 40 40 LEU N N 15 61.41 2.39 . . . . . . . 5996 2 31 . 1 1 42 42 LEU N N 15 58.48 1.49 . . . . . . . 5996 2 32 . 1 1 45 45 ILE N N 15 67.98 3.05 . . . . . . . 5996 2 33 . 1 1 46 46 HIS N N 15 64.17 3.27 . . . . . . . 5996 2 34 . 1 1 48 48 LEU N N 15 71.07 2.35 . . . . . . . 5996 2 35 . 1 1 50 50 ASN N N 15 67.35 2.26 . . . . . . . 5996 2 36 . 1 1 51 51 SER N N 15 70.62 2.03 . . . . . . . 5996 2 37 . 1 1 52 52 LEU N N 15 69.64 2.74 . . . . . . . 5996 2 38 . 1 1 53 53 VAL N N 15 67.18 2.98 . . . . . . . 5996 2 39 . 1 1 54 54 LEU N N 15 70.17 2.40 . . . . . . . 5996 2 40 . 1 1 55 55 LYS N N 15 63.26 2.12 . . . . . . . 5996 2 41 . 1 1 57 57 HIS N N 15 47.43 2.38 . . . . . . . 5996 2 42 . 1 1 60 60 ARG N N 15 73.44 3.93 . . . . . . . 5996 2 43 . 1 1 61 61 ASP N N 15 65.80 2.17 . . . . . . . 5996 2 44 . 1 1 62 62 GLU N N 15 27.69 2.73 . . . . . . . 5996 2 45 . 1 1 64 64 CYS N N 15 67.12 2.55 . . . . . . . 5996 2 46 . 1 1 66 66 GLU N N 15 65.08 2.86 . . . . . . . 5996 2 47 . 1 1 67 67 LEU N N 15 67.61 2.87 . . . . . . . 5996 2 48 . 1 1 68 68 SER N N 15 68.47 2.16 . . . . . . . 5996 2 49 . 1 1 69 69 MET N N 15 62.47 2.26 . . . . . . . 5996 2 50 . 1 1 71 71 ALA N N 15 69.40 2.80 . . . . . . . 5996 2 51 . 1 1 72 72 ASP N N 15 70.73 2.84 . . . . . . . 5996 2 52 . 1 1 74 74 THR N N 15 76.76 3.05 . . . . . . . 5996 2 53 . 1 1 75 75 GLU N N 15 76.38 2.84 . . . . . . . 5996 2 54 . 1 1 77 77 ALA N N 15 67.97 2.59 . . . . . . . 5996 2 55 . 1 1 78 78 GLY N N 15 72.04 2.82 . . . . . . . 5996 2 56 . 1 1 79 79 GLU N N 15 61.16 1.98 . . . . . . . 5996 2 57 . 1 1 80 80 TYR N N 15 64.24 2.10 . . . . . . . 5996 2 58 . 1 1 81 81 SER N N 15 68.23 2.34 . . . . . . . 5996 2 59 . 1 1 82 82 VAL N N 15 66.52 2.31 . . . . . . . 5996 2 60 . 1 1 84 84 TYR N N 15 69.19 1.19 . . . . . . . 5996 2 61 . 1 1 85 85 ASP N N 15 70.11 2.02 . . . . . . . 5996 2 62 . 1 1 86 86 GLY N N 15 65.84 2.03 . . . . . . . 5996 2 63 . 1 1 87 87 PHE N N 15 64.97 3.23 . . . . . . . 5996 2 64 . 1 1 88 88 ASN N N 15 67.58 2.25 . . . . . . . 5996 2 65 . 1 1 89 89 THR N N 15 69.44 2.63 . . . . . . . 5996 2 66 . 1 1 90 90 PHE N N 15 62.02 2.72 . . . . . . . 5996 2 67 . 1 1 91 91 THR N N 15 68.00 2.41 . . . . . . . 5996 2 68 . 1 1 92 92 ILE N N 15 65.06 1.21 . . . . . . . 5996 2 69 . 1 1 94 94 LYS N N 15 59.97 1.53 . . . . . . . 5996 2 70 . 1 1 95 95 THR N N 15 60.63 3.40 . . . . . . . 5996 2 71 . 1 1 96 96 ASP N N 15 60.35 2.42 . . . . . . . 5996 2 72 . 1 1 97 97 TYR N N 15 62.22 2.23 . . . . . . . 5996 2 73 . 1 1 98 98 ASP N N 15 65.77 2.54 . . . . . . . 5996 2 74 . 1 1 100 100 PHE N N 15 61.05 2.38 . . . . . . . 5996 2 75 . 1 1 101 101 LEU N N 15 61.49 2.62 . . . . . . . 5996 2 76 . 1 1 102 102 MET N N 15 65.84 2.85 . . . . . . . 5996 2 77 . 1 1 103 103 ALA N N 15 62.87 2.83 . . . . . . . 5996 2 78 . 1 1 104 104 HIS N N 15 72.14 2.57 . . . . . . . 5996 2 79 . 1 1 105 105 LEU N N 15 64.45 2.58 . . . . . . . 5996 2 80 . 1 1 107 107 ASN N N 15 73.21 4.45 . . . . . . . 5996 2 81 . 1 1 108 108 GLU N N 15 66.90 3.44 . . . . . . . 5996 2 82 . 1 1 109 109 LYS N N 15 69.28 2.60 . . . . . . . 5996 2 83 . 1 1 110 110 ASP N N 15 68.39 2.52 . . . . . . . 5996 2 84 . 1 1 111 111 GLY N N 15 70.43 2.88 . . . . . . . 5996 2 85 . 1 1 113 113 THR N N 15 72.76 2.68 . . . . . . . 5996 2 86 . 1 1 114 114 PHE N N 15 70.08 2.21 . . . . . . . 5996 2 87 . 1 1 115 115 GLN N N 15 68.33 2.97 . . . . . . . 5996 2 88 . 1 1 116 116 LEU N N 15 61.92 2.53 . . . . . . . 5996 2 89 . 1 1 117 117 MET N N 15 65.59 4.05 . . . . . . . 5996 2 90 . 1 1 118 118 GLY N N 15 61.44 2.46 . . . . . . . 5996 2 91 . 1 1 121 121 GLY N N 15 58.90 1.11 . . . . . . . 5996 2 92 . 1 1 123 123 GLU N N 15 64.34 2.70 . . . . . . . 5996 2 93 . 1 1 125 125 ASP N N 15 62.73 2.28 . . . . . . . 5996 2 94 . 1 1 126 126 LEU N N 15 78.21 5.50 . . . . . . . 5996 2 95 . 1 1 127 127 SER N N 15 72.68 1.81 . . . . . . . 5996 2 96 . 1 1 128 128 SER N N 15 63.30 2.92 . . . . . . . 5996 2 97 . 1 1 130 130 ILE N N 15 62.88 2.60 . . . . . . . 5996 2 98 . 1 1 131 131 LYS N N 15 64.31 2.07 . . . . . . . 5996 2 99 . 1 1 134 134 PHE N N 15 58.16 2.34 . . . . . . . 5996 2 100 . 1 1 135 135 ALA N N 15 63.35 1.94 . . . . . . . 5996 2 101 . 1 1 136 136 GLN N N 15 67.59 2.58 . . . . . . . 5996 2 102 . 1 1 137 137 LEU N N 15 64.42 2.42 . . . . . . . 5996 2 103 . 1 1 138 138 CYS N N 15 68.16 2.32 . . . . . . . 5996 2 104 . 1 1 140 140 LYS N N 15 63.92 2.30 . . . . . . . 5996 2 105 . 1 1 141 141 HIS N N 15 67.75 2.48 . . . . . . . 5996 2 106 . 1 1 142 142 GLY N N 15 66.19 2.14 . . . . . . . 5996 2 107 . 1 1 145 145 ARG N N 15 68.42 2.95 . . . . . . . 5996 2 108 . 1 1 146 146 GLU N N 15 68.37 2.83 . . . . . . . 5996 2 109 . 1 1 148 148 ILE N N 15 68.53 2.74 . . . . . . . 5996 2 110 . 1 1 151 151 LEU N N 15 71.37 5.41 . . . . . . . 5996 2 111 . 1 1 152 152 SER N N 15 45.71 3.27 . . . . . . . 5996 2 112 . 1 1 153 153 ASN N N 15 49.46 3.41 . . . . . . . 5996 2 113 . 1 1 160 160 ALA N N 15 81.45 3.60 . . . . . . . 5996 2 stop_ save_ save_293_600_bound_t2 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 293_600_bound_t2 _Heteronucl_T2_list.Entry_ID 5996 _Heteronucl_T2_list.ID 3 _Heteronucl_T2_list.Sample_condition_list_ID 3 _Heteronucl_T2_list.Sample_condition_list_label $293K _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 600 _Heteronucl_T2_list.T2_coherence_type Nx _Heteronucl_T2_list.T2_val_units ms _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 1 '15N T2' 1 $sample_1 . 5996 3 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 ALA N N 15 77.99 2.15 . . . . . . . 5996 3 2 . 1 1 5 5 SER N N 15 50.18 5.23 . . . . . . . 5996 3 3 . 1 1 6 6 THR N N 15 57.64 1.50 . . . . . . . 5996 3 4 . 1 1 7 7 GLY N N 15 76.00 7.38 . . . . . . . 5996 3 5 . 1 1 10 10 PHE N N 15 77.53 4.62 . . . . . . . 5996 3 6 . 1 1 11 11 ASN N N 15 69.75 4.33 . . . . . . . 5996 3 7 . 1 1 12 12 VAL N N 15 75.72 2.76 . . . . . . . 5996 3 8 . 1 1 13 13 GLU N N 15 49.04 12.77 . . . . . . . 5996 3 9 . 1 1 15 15 ILE N N 15 74.44 4.80 . . . . . . . 5996 3 10 . 1 1 16 16 ASN N N 15 64.62 5.30 . . . . . . . 5996 3 11 . 1 1 18 18 GLU N N 15 58.58 3.79 . . . . . . . 5996 3 12 . 1 1 19 19 TRP N N 15 64.61 3.01 . . . . . . . 5996 3 13 . 1 1 20 20 HIS N N 15 68.86 1.18 . . . . . . . 5996 3 14 . 1 1 22 22 ILE N N 15 82.78 6.96 . . . . . . . 5996 3 15 . 1 1 23 23 ILE N N 15 64.02 1.80 . . . . . . . 5996 3 16 . 1 1 26 26 SER N N 15 86.84 5.89 . . . . . . . 5996 3 17 . 1 1 27 27 ASP N N 15 74.21 5.49 . . . . . . . 5996 3 18 . 1 1 29 29 ARG N N 15 77.73 5.28 . . . . . . . 5996 3 19 . 1 1 30 30 GLU N N 15 67.52 4.78 . . . . . . . 5996 3 20 . 1 1 31 31 LYS N N 15 53.71 3.94 . . . . . . . 5996 3 21 . 1 1 32 32 ILE N N 15 72.99 3.29 . . . . . . . 5996 3 22 . 1 1 33 33 GLU N N 15 56.88 3.63 . . . . . . . 5996 3 23 . 1 1 36 36 GLY N N 15 73.63 3.40 . . . . . . . 5996 3 24 . 1 1 37 37 ASN N N 15 62.15 8.00 . . . . . . . 5996 3 25 . 1 1 39 39 ARG N N 15 60.91 3.34 . . . . . . . 5996 3 26 . 1 1 40 40 LEU N N 15 55.07 2.47 . . . . . . . 5996 3 27 . 1 1 43 43 GLU N N 15 53.82 6.92 . . . . . . . 5996 3 28 . 1 1 45 45 ILE N N 15 66.34 8.66 . . . . . . . 5996 3 29 . 1 1 46 46 HIS N N 15 78.36 3.37 . . . . . . . 5996 3 30 . 1 1 47 47 VAL N N 15 80.45 4.63 . . . . . . . 5996 3 31 . 1 1 48 48 LEU N N 15 68.78 15.78 . . . . . . . 5996 3 32 . 1 1 50 50 ASN N N 15 69.93 2.57 . . . . . . . 5996 3 33 . 1 1 51 51 SER N N 15 64.62 2.13 . . . . . . . 5996 3 34 . 1 1 52 52 LEU N N 15 54.32 1.98 . . . . . . . 5996 3 35 . 1 1 53 53 VAL N N 15 78.81 2.03 . . . . . . . 5996 3 36 . 1 1 54 54 LEU N N 15 75.31 2.72 . . . . . . . 5996 3 37 . 1 1 55 55 LYS N N 15 64.73 2.55 . . . . . . . 5996 3 38 . 1 1 57 57 HIS N N 15 51.89 2.50 . . . . . . . 5996 3 39 . 1 1 60 60 ARG N N 15 66.93 4.82 . . . . . . . 5996 3 40 . 1 1 61 61 ASP N N 15 79.24 12.63 . . . . . . . 5996 3 41 . 1 1 62 62 GLU N N 15 33.82 1.40 . . . . . . . 5996 3 42 . 1 1 64 64 CYS N N 15 67.91 6.56 . . . . . . . 5996 3 43 . 1 1 66 66 GLU N N 15 83.90 3.96 . . . . . . . 5996 3 44 . 1 1 67 67 LEU N N 15 65.41 7.34 . . . . . . . 5996 3 45 . 1 1 68 68 SER N N 15 67.43 3.38 . . . . . . . 5996 3 46 . 1 1 69 69 MET N N 15 65.29 1.89 . . . . . . . 5996 3 47 . 1 1 71 71 ALA N N 15 74.97 3.53 . . . . . . . 5996 3 48 . 1 1 72 72 ASP N N 15 68.98 2.65 . . . . . . . 5996 3 49 . 1 1 74 74 THR N N 15 69.78 1.96 . . . . . . . 5996 3 50 . 1 1 75 75 GLU N N 15 61.65 4.30 . . . . . . . 5996 3 51 . 1 1 76 76 LYS N N 15 43.42 5.89 . . . . . . . 5996 3 52 . 1 1 77 77 ALA N N 15 66.13 1.90 . . . . . . . 5996 3 53 . 1 1 78 78 GLY N N 15 69.38 6.64 . . . . . . . 5996 3 54 . 1 1 79 79 GLU N N 15 54.73 2.76 . . . . . . . 5996 3 55 . 1 1 80 80 TYR N N 15 67.29 3.49 . . . . . . . 5996 3 56 . 1 1 81 81 SER N N 15 68.07 2.18 . . . . . . . 5996 3 57 . 1 1 82 82 VAL N N 15 69.12 2.09 . . . . . . . 5996 3 58 . 1 1 83 83 THR N N 15 66.89 10.05 . . . . . . . 5996 3 59 . 1 1 84 84 TYR N N 15 76.97 4.93 . . . . . . . 5996 3 60 . 1 1 86 86 GLY N N 15 75.21 7.96 . . . . . . . 5996 3 61 . 1 1 87 87 PHE N N 15 58.62 6.21 . . . . . . . 5996 3 62 . 1 1 88 88 ASN N N 15 68.88 10.55 . . . . . . . 5996 3 63 . 1 1 89 89 THR N N 15 75.50 3.62 . . . . . . . 5996 3 64 . 1 1 90 90 PHE N N 15 51.36 3.27 . . . . . . . 5996 3 65 . 1 1 91 91 THR N N 15 65.27 4.01 . . . . . . . 5996 3 66 . 1 1 92 92 ILE N N 15 66.62 4.00 . . . . . . . 5996 3 67 . 1 1 94 94 LYS N N 15 66.30 3.38 . . . . . . . 5996 3 68 . 1 1 95 95 THR N N 15 56.21 6.70 . . . . . . . 5996 3 69 . 1 1 96 96 ASP N N 15 55.99 1.63 . . . . . . . 5996 3 70 . 1 1 97 97 TYR N N 15 58.65 2.58 . . . . . . . 5996 3 71 . 1 1 98 98 ASP N N 15 76.98 3.62 . . . . . . . 5996 3 72 . 1 1 101 101 LEU N N 15 32.83 6.83 . . . . . . . 5996 3 73 . 1 1 102 102 MET N N 15 71.55 4.33 . . . . . . . 5996 3 74 . 1 1 103 103 ALA N N 15 63.78 2.57 . . . . . . . 5996 3 75 . 1 1 104 104 HIS N N 15 80.85 15.75 . . . . . . . 5996 3 76 . 1 1 105 105 LEU N N 15 69.16 5.70 . . . . . . . 5996 3 77 . 1 1 108 108 GLU N N 15 58.68 4.27 . . . . . . . 5996 3 78 . 1 1 109 109 LYS N N 15 73.04 4.31 . . . . . . . 5996 3 79 . 1 1 110 110 ASP N N 15 70.91 9.26 . . . . . . . 5996 3 80 . 1 1 111 111 GLY N N 15 71.47 4.05 . . . . . . . 5996 3 81 . 1 1 115 115 GLN N N 15 58.96 2.39 . . . . . . . 5996 3 82 . 1 1 116 116 LEU N N 15 73.67 2.30 . . . . . . . 5996 3 83 . 1 1 117 117 MET N N 15 79.42 1.43 . . . . . . . 5996 3 84 . 1 1 118 118 GLY N N 15 76.49 5.41 . . . . . . . 5996 3 85 . 1 1 119 119 LEU N N 15 66.81 1.40 . . . . . . . 5996 3 86 . 1 1 120 120 TYR N N 15 87.17 2.60 . . . . . . . 5996 3 87 . 1 1 121 121 GLY N N 15 67.20 2.68 . . . . . . . 5996 3 88 . 1 1 123 123 GLU N N 15 68.28 1.89 . . . . . . . 5996 3 89 . 1 1 125 125 ASP N N 15 58.69 0.66 . . . . . . . 5996 3 90 . 1 1 128 128 SER N N 15 61.20 5.41 . . . . . . . 5996 3 91 . 1 1 129 129 ASP N N 15 60.20 6.36 . . . . . . . 5996 3 92 . 1 1 130 130 ILE N N 15 66.92 3.22 . . . . . . . 5996 3 93 . 1 1 131 131 LYS N N 15 60.75 19.43 . . . . . . . 5996 3 94 . 1 1 134 134 PHE N N 15 56.15 2.49 . . . . . . . 5996 3 95 . 1 1 135 135 ALA N N 15 73.76 3.13 . . . . . . . 5996 3 96 . 1 1 136 136 GLN N N 15 53.50 2.36 . . . . . . . 5996 3 97 . 1 1 137 137 LEU N N 15 60.90 3.81 . . . . . . . 5996 3 98 . 1 1 138 138 CYS N N 15 82.49 3.45 . . . . . . . 5996 3 99 . 1 1 141 141 HIS N N 15 84.32 3.87 . . . . . . . 5996 3 100 . 1 1 142 142 GLY N N 15 63.52 2.25 . . . . . . . 5996 3 101 . 1 1 143 143 ILE N N 15 54.91 3.83 . . . . . . . 5996 3 102 . 1 1 144 144 LEU N N 15 70.30 6.28 . . . . . . . 5996 3 103 . 1 1 145 145 ARG N N 15 78.18 2.90 . . . . . . . 5996 3 104 . 1 1 148 148 ILE N N 15 70.82 5.22 . . . . . . . 5996 3 105 . 1 1 151 151 LEU N N 15 67.78 4.57 . . . . . . . 5996 3 106 . 1 1 156 156 ARG N N 15 91.46 2.60 . . . . . . . 5996 3 107 . 1 1 160 160 ALA N N 15 93.52 4.40 . . . . . . . 5996 3 108 . 1 1 162 162 GLU N N 15 240.81 3.53 . . . . . . . 5996 3 stop_ save_ save_298_600_bound_t2 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 298_600_bound_t2 _Heteronucl_T2_list.Entry_ID 5996 _Heteronucl_T2_list.ID 4 _Heteronucl_T2_list.Sample_condition_list_ID 4 _Heteronucl_T2_list.Sample_condition_list_label $298K _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 600 _Heteronucl_T2_list.T2_coherence_type Nx _Heteronucl_T2_list.T2_val_units ms _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 1 '15N T2' 1 $sample_1 . 5996 4 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 ALA N N 15 88.64 6.86 . . . . . . . 5996 4 2 . 1 1 4 4 SER N N 15 87.48 5.35 . . . . . . . 5996 4 3 . 1 1 5 5 SER N N 15 57.50 2.63 . . . . . . . 5996 4 4 . 1 1 6 6 THR N N 15 50.37 2.56 . . . . . . . 5996 4 5 . 1 1 7 7 GLY N N 15 82.83 5.04 . . . . . . . 5996 4 6 . 1 1 10 10 PHE N N 15 80.17 7.02 . . . . . . . 5996 4 7 . 1 1 11 11 ASN N N 15 62.87 3.38 . . . . . . . 5996 4 8 . 1 1 12 12 VAL N N 15 91.17 5.63 . . . . . . . 5996 4 9 . 1 1 13 13 GLU N N 15 52.65 2.28 . . . . . . . 5996 4 10 . 1 1 15 15 ILE N N 15 93.00 6.74 . . . . . . . 5996 4 11 . 1 1 16 16 ASN N N 15 59.41 2.81 . . . . . . . 5996 4 12 . 1 1 17 17 GLY N N 15 85.82 4.64 . . . . . . . 5996 4 13 . 1 1 18 18 GLU N N 15 93.29 4.17 . . . . . . . 5996 4 14 . 1 1 19 19 TRP N N 15 66.23 0.88 . . . . . . . 5996 4 15 . 1 1 20 20 HIS N N 15 67.21 2.04 . . . . . . . 5996 4 16 . 1 1 21 21 THR N N 15 75.32 3.22 . . . . . . . 5996 4 17 . 1 1 22 22 ILE N N 15 84.10 3.47 . . . . . . . 5996 4 18 . 1 1 23 23 ILE N N 15 93.69 5.48 . . . . . . . 5996 4 19 . 1 1 26 26 SER N N 15 77.17 3.08 . . . . . . . 5996 4 20 . 1 1 27 27 ASP N N 15 58.33 2.57 . . . . . . . 5996 4 21 . 1 1 29 29 ARG N N 15 79.73 7.06 . . . . . . . 5996 4 22 . 1 1 30 30 GLU N N 15 59.85 2.50 . . . . . . . 5996 4 23 . 1 1 31 31 LYS N N 15 90.10 5.56 . . . . . . . 5996 4 24 . 1 1 32 32 ILE N N 15 55.56 1.19 . . . . . . . 5996 4 25 . 1 1 33 33 GLU N N 15 71.51 7.16 . . . . . . . 5996 4 26 . 1 1 35 35 ASN N N 15 166.48 42.22 . . . . . . . 5996 4 27 . 1 1 36 36 GLY N N 15 73.45 4.17 . . . . . . . 5996 4 28 . 1 1 37 37 ASN N N 15 59.73 1.84 . . . . . . . 5996 4 29 . 1 1 39 39 ARG N N 15 75.66 4.23 . . . . . . . 5996 4 30 . 1 1 40 40 LEU N N 15 79.20 5.35 . . . . . . . 5996 4 31 . 1 1 42 42 LEU N N 15 84.66 11.88 . . . . . . . 5996 4 32 . 1 1 43 43 GLU N N 15 58.39 2.27 . . . . . . . 5996 4 33 . 1 1 45 45 ILE N N 15 74.90 5.35 . . . . . . . 5996 4 34 . 1 1 46 46 HIS N N 15 93.81 4.30 . . . . . . . 5996 4 35 . 1 1 47 47 VAL N N 15 91.41 6.03 . . . . . . . 5996 4 36 . 1 1 48 48 LEU N N 15 89.03 5.91 . . . . . . . 5996 4 37 . 1 1 50 50 ASN N N 15 80.19 5.34 . . . . . . . 5996 4 38 . 1 1 51 51 SER N N 15 76.44 5.15 . . . . . . . 5996 4 39 . 1 1 52 52 LEU N N 15 83.49 6.56 . . . . . . . 5996 4 40 . 1 1 53 53 VAL N N 15 80.78 5.18 . . . . . . . 5996 4 41 . 1 1 54 54 LEU N N 15 86.01 6.43 . . . . . . . 5996 4 42 . 1 1 55 55 LYS N N 15 72.00 2.11 . . . . . . . 5996 4 43 . 1 1 57 57 HIS N N 15 72.59 7.39 . . . . . . . 5996 4 44 . 1 1 58 58 THR N N 15 69.21 1.62 . . . . . . . 5996 4 45 . 1 1 60 60 ARG N N 15 81.59 6.16 . . . . . . . 5996 4 46 . 1 1 61 61 ASP N N 15 88.71 3.60 . . . . . . . 5996 4 47 . 1 1 62 62 GLU N N 15 38.78 3.15 . . . . . . . 5996 4 48 . 1 1 64 64 CYS N N 15 92.30 6.92 . . . . . . . 5996 4 49 . 1 1 65 65 SER N N 15 91.42 9.11 . . . . . . . 5996 4 50 . 1 1 66 66 GLU N N 15 88.77 6.62 . . . . . . . 5996 4 51 . 1 1 67 67 LEU N N 15 80.08 6.33 . . . . . . . 5996 4 52 . 1 1 68 68 SER N N 15 86.58 5.15 . . . . . . . 5996 4 53 . 1 1 69 69 MET N N 15 86.75 7.56 . . . . . . . 5996 4 54 . 1 1 71 71 ALA N N 15 89.93 6.53 . . . . . . . 5996 4 55 . 1 1 72 72 ASP N N 15 80.87 5.74 . . . . . . . 5996 4 56 . 1 1 74 74 THR N N 15 64.94 2.29 . . . . . . . 5996 4 57 . 1 1 75 75 GLU N N 15 98.71 8.86 . . . . . . . 5996 4 58 . 1 1 76 76 LYS N N 15 62.09 1.51 . . . . . . . 5996 4 59 . 1 1 77 77 ALA N N 15 78.64 4.96 . . . . . . . 5996 4 60 . 1 1 78 78 GLY N N 15 86.55 5.98 . . . . . . . 5996 4 61 . 1 1 79 79 GLU N N 15 54.04 2.53 . . . . . . . 5996 4 62 . 1 1 80 80 TYR N N 15 75.99 5.05 . . . . . . . 5996 4 63 . 1 1 81 81 SER N N 15 91.83 6.43 . . . . . . . 5996 4 64 . 1 1 82 82 VAL N N 15 57.88 2.73 . . . . . . . 5996 4 65 . 1 1 83 83 THR N N 15 90.41 8.72 . . . . . . . 5996 4 66 . 1 1 84 84 TYR N N 15 85.78 5.88 . . . . . . . 5996 4 67 . 1 1 85 85 ASP N N 15 88.56 6.43 . . . . . . . 5996 4 68 . 1 1 86 86 GLY N N 15 80.00 5.18 . . . . . . . 5996 4 69 . 1 1 87 87 PHE N N 15 73.15 4.58 . . . . . . . 5996 4 70 . 1 1 88 88 ASN N N 15 84.34 6.28 . . . . . . . 5996 4 71 . 1 1 89 89 THR N N 15 79.34 4.88 . . . . . . . 5996 4 72 . 1 1 90 90 PHE N N 15 59.53 2.22 . . . . . . . 5996 4 73 . 1 1 91 91 THR N N 15 77.07 6.63 . . . . . . . 5996 4 74 . 1 1 92 92 ILE N N 15 77.68 6.33 . . . . . . . 5996 4 75 . 1 1 94 94 LYS N N 15 71.76 10.37 . . . . . . . 5996 4 76 . 1 1 95 95 THR N N 15 74.52 3.63 . . . . . . . 5996 4 77 . 1 1 96 96 ASP N N 15 60.60 3.06 . . . . . . . 5996 4 78 . 1 1 97 97 TYR N N 15 78.86 8.00 . . . . . . . 5996 4 79 . 1 1 99 99 ASN N N 15 58.36 2.79 . . . . . . . 5996 4 80 . 1 1 100 100 PHE N N 15 74.34 4.71 . . . . . . . 5996 4 81 . 1 1 101 101 LEU N N 15 79.52 3.21 . . . . . . . 5996 4 82 . 1 1 103 103 ALA N N 15 77.36 3.62 . . . . . . . 5996 4 83 . 1 1 104 104 HIS N N 15 90.17 6.40 . . . . . . . 5996 4 84 . 1 1 105 105 LEU N N 15 73.06 3.83 . . . . . . . 5996 4 85 . 1 1 107 107 ASN N N 15 86.05 7.63 . . . . . . . 5996 4 86 . 1 1 108 108 GLU N N 15 83.39 8.24 . . . . . . . 5996 4 87 . 1 1 109 109 LYS N N 15 76.10 5.10 . . . . . . . 5996 4 88 . 1 1 110 110 ASP N N 15 89.04 9.95 . . . . . . . 5996 4 89 . 1 1 111 111 GLY N N 15 75.96 6.50 . . . . . . . 5996 4 90 . 1 1 113 113 THR N N 15 90.72 5.99 . . . . . . . 5996 4 91 . 1 1 114 114 PHE N N 15 84.98 4.92 . . . . . . . 5996 4 92 . 1 1 115 115 GLN N N 15 73.18 3.18 . . . . . . . 5996 4 93 . 1 1 116 116 LEU N N 15 76.28 2.83 . . . . . . . 5996 4 94 . 1 1 117 117 MET N N 15 81.94 6.12 . . . . . . . 5996 4 95 . 1 1 118 118 GLY N N 15 77.40 1.95 . . . . . . . 5996 4 96 . 1 1 119 119 LEU N N 15 93.65 6.13 . . . . . . . 5996 4 97 . 1 1 121 121 GLY N N 15 75.97 4.16 . . . . . . . 5996 4 98 . 1 1 123 123 GLU N N 15 82.96 4.15 . . . . . . . 5996 4 99 . 1 1 125 125 ASP N N 15 80.81 8.34 . . . . . . . 5996 4 100 . 1 1 126 126 LEU N N 15 87.67 6.78 . . . . . . . 5996 4 101 . 1 1 127 127 SER N N 15 91.31 7.24 . . . . . . . 5996 4 102 . 1 1 128 128 SER N N 15 61.16 1.81 . . . . . . . 5996 4 103 . 1 1 130 130 ILE N N 15 57.51 3.42 . . . . . . . 5996 4 104 . 1 1 131 131 LYS N N 15 77.12 6.41 . . . . . . . 5996 4 105 . 1 1 133 133 ARG N N 15 61.44 2.17 . . . . . . . 5996 4 106 . 1 1 134 134 PHE N N 15 56.39 2.08 . . . . . . . 5996 4 107 . 1 1 135 135 ALA N N 15 81.48 6.38 . . . . . . . 5996 4 108 . 1 1 136 136 GLN N N 15 74.19 4.98 . . . . . . . 5996 4 109 . 1 1 137 137 LEU N N 15 78.39 7.20 . . . . . . . 5996 4 110 . 1 1 138 138 CYS N N 15 81.46 3.93 . . . . . . . 5996 4 111 . 1 1 141 141 HIS N N 15 69.58 8.08 . . . . . . . 5996 4 112 . 1 1 142 142 GLY N N 15 75.65 4.99 . . . . . . . 5996 4 113 . 1 1 143 143 ILE N N 15 51.27 4.01 . . . . . . . 5996 4 114 . 1 1 144 144 LEU N N 15 97.31 6.64 . . . . . . . 5996 4 115 . 1 1 145 145 ARG N N 15 86.34 6.27 . . . . . . . 5996 4 116 . 1 1 146 146 GLU N N 15 74.96 6.59 . . . . . . . 5996 4 117 . 1 1 148 148 ILE N N 15 78.61 4.96 . . . . . . . 5996 4 118 . 1 1 149 149 ILE N N 15 88.21 4.91 . . . . . . . 5996 4 119 . 1 1 150 150 ASP N N 15 105.35 11.06 . . . . . . . 5996 4 120 . 1 1 151 151 LEU N N 15 84.17 4.68 . . . . . . . 5996 4 121 . 1 1 152 152 SER N N 15 54.07 2.54 . . . . . . . 5996 4 122 . 1 1 153 153 ASN N N 15 57.09 2.88 . . . . . . . 5996 4 123 . 1 1 160 160 ALA N N 15 123.35 14.43 . . . . . . . 5996 4 124 . 1 1 162 162 GLU N N 15 251.74 22.66 . . . . . . . 5996 4 stop_ save_ save_303_600_bound_t2 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 303_600_bound_t2 _Heteronucl_T2_list.Entry_ID 5996 _Heteronucl_T2_list.ID 5 _Heteronucl_T2_list.Sample_condition_list_ID 5 _Heteronucl_T2_list.Sample_condition_list_label $303K _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 600 _Heteronucl_T2_list.T2_coherence_type Nx _Heteronucl_T2_list.T2_val_units ms _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 1 '15N T2' 1 $sample_1 . 5996 5 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 ALA N N 15 92.13 5.62 . . . . . . . 5996 5 2 . 1 1 4 4 SER N N 15 103.37 5.60 . . . . . . . 5996 5 3 . 1 1 5 5 SER N N 15 81.25 5.71 . . . . . . . 5996 5 4 . 1 1 6 6 THR N N 15 78.14 7.52 . . . . . . . 5996 5 5 . 1 1 7 7 GLY N N 15 104.67 5.27 . . . . . . . 5996 5 6 . 1 1 10 10 PHE N N 15 89.85 6.97 . . . . . . . 5996 5 7 . 1 1 11 11 ASN N N 15 91.27 6.81 . . . . . . . 5996 5 8 . 1 1 12 12 VAL N N 15 90.87 3.31 . . . . . . . 5996 5 9 . 1 1 13 13 GLU N N 15 57.98 0.26 . . . . . . . 5996 5 10 . 1 1 15 15 ILE N N 15 83.07 2.87 . . . . . . . 5996 5 11 . 1 1 16 16 ASN N N 15 60.03 2.83 . . . . . . . 5996 5 12 . 1 1 17 17 GLY N N 15 89.42 5.02 . . . . . . . 5996 5 13 . 1 1 18 18 GLU N N 15 75.91 4.32 . . . . . . . 5996 5 14 . 1 1 20 20 HIS N N 15 86.47 6.25 . . . . . . . 5996 5 15 . 1 1 21 21 THR N N 15 92.45 6.76 . . . . . . . 5996 5 16 . 1 1 22 22 ILE N N 15 92.60 3.80 . . . . . . . 5996 5 17 . 1 1 23 23 ILE N N 15 81.19 3.60 . . . . . . . 5996 5 18 . 1 1 27 27 ASP N N 15 79.01 8.80 . . . . . . . 5996 5 19 . 1 1 29 29 ARG N N 15 88.89 4.36 . . . . . . . 5996 5 20 . 1 1 31 31 LYS N N 15 79.24 4.85 . . . . . . . 5996 5 21 . 1 1 32 32 ILE N N 15 97.00 7.26 . . . . . . . 5996 5 22 . 1 1 33 33 GLU N N 15 49.79 4.57 . . . . . . . 5996 5 23 . 1 1 35 35 ASN N N 15 94.35 3.53 . . . . . . . 5996 5 24 . 1 1 36 36 GLY N N 15 77.90 0.39 . . . . . . . 5996 5 25 . 1 1 37 37 ASN N N 15 92.51 3.70 . . . . . . . 5996 5 26 . 1 1 39 39 ARG N N 15 79.69 6.31 . . . . . . . 5996 5 27 . 1 1 40 40 LEU N N 15 86.24 5.50 . . . . . . . 5996 5 28 . 1 1 42 42 LEU N N 15 108.11 11.37 . . . . . . . 5996 5 29 . 1 1 43 43 GLU N N 15 77.07 3.60 . . . . . . . 5996 5 30 . 1 1 45 45 ILE N N 15 87.39 6.16 . . . . . . . 5996 5 31 . 1 1 46 46 HIS N N 15 90.00 5.68 . . . . . . . 5996 5 32 . 1 1 47 47 VAL N N 15 90.64 4.45 . . . . . . . 5996 5 33 . 1 1 48 48 LEU N N 15 91.02 15.90 . . . . . . . 5996 5 34 . 1 1 50 50 ASN N N 15 98.59 7.39 . . . . . . . 5996 5 35 . 1 1 51 51 SER N N 15 96.47 86.55 . . . . . . . 5996 5 36 . 1 1 52 52 LEU N N 15 91.56 4.93 . . . . . . . 5996 5 37 . 1 1 53 53 VAL N N 15 85.92 6.46 . . . . . . . 5996 5 38 . 1 1 54 54 LEU N N 15 87.55 5.13 . . . . . . . 5996 5 39 . 1 1 55 55 LYS N N 15 82.82 2.53 . . . . . . . 5996 5 40 . 1 1 57 57 HIS N N 15 84.34 4.80 . . . . . . . 5996 5 41 . 1 1 58 58 THR N N 15 81.50 3.60 . . . . . . . 5996 5 42 . 1 1 60 60 ARG N N 15 92.94 12.68 . . . . . . . 5996 5 43 . 1 1 61 61 ASP N N 15 90.63 2.89 . . . . . . . 5996 5 44 . 1 1 62 62 GLU N N 15 48.25 1.33 . . . . . . . 5996 5 45 . 1 1 64 64 CYS N N 15 94.36 3.70 . . . . . . . 5996 5 46 . 1 1 65 65 SER N N 15 97.52 5.44 . . . . . . . 5996 5 47 . 1 1 66 66 GLU N N 15 92.05 4.20 . . . . . . . 5996 5 48 . 1 1 67 67 LEU N N 15 81.24 7.31 . . . . . . . 5996 5 49 . 1 1 68 68 SER N N 15 96.36 4.37 . . . . . . . 5996 5 50 . 1 1 69 69 MET N N 15 89.98 4.41 . . . . . . . 5996 5 51 . 1 1 71 71 ALA N N 15 92.17 5.49 . . . . . . . 5996 5 52 . 1 1 72 72 ASP N N 15 87.45 4.24 . . . . . . . 5996 5 53 . 1 1 74 74 THR N N 15 90.32 6.72 . . . . . . . 5996 5 54 . 1 1 75 75 GLU N N 15 92.05 7.14 . . . . . . . 5996 5 55 . 1 1 76 76 LYS N N 15 88.56 3.09 . . . . . . . 5996 5 56 . 1 1 77 77 ALA N N 15 92.08 4.43 . . . . . . . 5996 5 57 . 1 1 78 78 GLY N N 15 116.03 5.79 . . . . . . . 5996 5 58 . 1 1 79 79 GLU N N 15 78.32 6.45 . . . . . . . 5996 5 59 . 1 1 81 81 SER N N 15 90.93 4.80 . . . . . . . 5996 5 60 . 1 1 82 82 VAL N N 15 78.63 8.51 . . . . . . . 5996 5 61 . 1 1 83 83 THR N N 15 103.06 4.38 . . . . . . . 5996 5 62 . 1 1 84 84 TYR N N 15 93.26 4.74 . . . . . . . 5996 5 63 . 1 1 85 85 ASP N N 15 93.67 6.43 . . . . . . . 5996 5 64 . 1 1 86 86 GLY N N 15 92.63 4.82 . . . . . . . 5996 5 65 . 1 1 87 87 PHE N N 15 88.91 5.46 . . . . . . . 5996 5 66 . 1 1 89 89 THR N N 15 89.44 6.14 . . . . . . . 5996 5 67 . 1 1 90 90 PHE N N 15 60.18 3.07 . . . . . . . 5996 5 68 . 1 1 91 91 THR N N 15 91.53 4.03 . . . . . . . 5996 5 69 . 1 1 92 92 ILE N N 15 90.66 5.06 . . . . . . . 5996 5 70 . 1 1 94 94 LYS N N 15 83.61 3.94 . . . . . . . 5996 5 71 . 1 1 95 95 THR N N 15 80.35 4.12 . . . . . . . 5996 5 72 . 1 1 96 96 ASP N N 15 86.78 6.95 . . . . . . . 5996 5 73 . 1 1 97 97 TYR N N 15 79.66 6.28 . . . . . . . 5996 5 74 . 1 1 98 98 ASP N N 15 74.78 5.52 . . . . . . . 5996 5 75 . 1 1 99 99 ASN N N 15 85.58 6.82 . . . . . . . 5996 5 76 . 1 1 100 100 PHE N N 15 80.97 6.66 . . . . . . . 5996 5 77 . 1 1 102 102 MET N N 15 97.52 4.84 . . . . . . . 5996 5 78 . 1 1 103 103 ALA N N 15 87.16 3.47 . . . . . . . 5996 5 79 . 1 1 104 104 HIS N N 15 99.91 5.29 . . . . . . . 5996 5 80 . 1 1 105 105 LEU N N 15 88.04 5.62 . . . . . . . 5996 5 81 . 1 1 107 107 ASN N N 15 86.11 4.83 . . . . . . . 5996 5 82 . 1 1 108 108 GLU N N 15 84.11 5.61 . . . . . . . 5996 5 83 . 1 1 109 109 LYS N N 15 89.55 7.04 . . . . . . . 5996 5 84 . 1 1 110 110 ASP N N 15 92.72 2.93 . . . . . . . 5996 5 85 . 1 1 111 111 GLY N N 15 91.68 6.22 . . . . . . . 5996 5 86 . 1 1 113 113 THR N N 15 104.78 4.27 . . . . . . . 5996 5 87 . 1 1 114 114 PHE N N 15 89.50 3.30 . . . . . . . 5996 5 88 . 1 1 115 115 GLN N N 15 89.98 6.82 . . . . . . . 5996 5 89 . 1 1 116 116 LEU N N 15 87.39 3.77 . . . . . . . 5996 5 90 . 1 1 117 117 MET N N 15 84.61 3.88 . . . . . . . 5996 5 91 . 1 1 121 121 GLY N N 15 81.24 4.95 . . . . . . . 5996 5 92 . 1 1 123 123 GLU N N 15 89.57 3.33 . . . . . . . 5996 5 93 . 1 1 125 125 ASP N N 15 82.10 8.96 . . . . . . . 5996 5 94 . 1 1 126 126 LEU N N 15 90.57 6.37 . . . . . . . 5996 5 95 . 1 1 127 127 SER N N 15 93.34 5.14 . . . . . . . 5996 5 96 . 1 1 128 128 SER N N 15 87.92 6.52 . . . . . . . 5996 5 97 . 1 1 129 129 ASP N N 15 85.14 6.47 . . . . . . . 5996 5 98 . 1 1 131 131 LYS N N 15 86.47 5.02 . . . . . . . 5996 5 99 . 1 1 133 133 ARG N N 15 61.37 1.63 . . . . . . . 5996 5 100 . 1 1 134 134 PHE N N 15 61.26 0.80 . . . . . . . 5996 5 101 . 1 1 135 135 ALA N N 15 82.79 4.90 . . . . . . . 5996 5 102 . 1 1 136 136 GLN N N 15 82.29 6.80 . . . . . . . 5996 5 103 . 1 1 138 138 CYS N N 15 79.64 7.23 . . . . . . . 5996 5 104 . 1 1 141 141 HIS N N 15 84.37 8.44 . . . . . . . 5996 5 105 . 1 1 142 142 GLY N N 15 77.23 4.25 . . . . . . . 5996 5 106 . 1 1 143 143 ILE N N 15 64.00 1.48 . . . . . . . 5996 5 107 . 1 1 144 144 LEU N N 15 91.99 5.29 . . . . . . . 5996 5 108 . 1 1 145 145 ARG N N 15 87.75 4.79 . . . . . . . 5996 5 109 . 1 1 146 146 GLU N N 15 84.80 4.88 . . . . . . . 5996 5 110 . 1 1 148 148 ILE N N 15 84.18 6.86 . . . . . . . 5996 5 111 . 1 1 149 149 ILE N N 15 98.80 7.36 . . . . . . . 5996 5 112 . 1 1 150 150 ASP N N 15 96.99 3.61 . . . . . . . 5996 5 113 . 1 1 151 151 LEU N N 15 89.22 5.54 . . . . . . . 5996 5 114 . 1 1 152 152 SER N N 15 77.12 4.08 . . . . . . . 5996 5 115 . 1 1 153 153 ASN N N 15 77.57 5.51 . . . . . . . 5996 5 116 . 1 1 155 155 ASN N N 15 67.62 1.20 . . . . . . . 5996 5 117 . 1 1 156 156 ARG N N 15 50.75 2.17 . . . . . . . 5996 5 118 . 1 1 160 160 ALA N N 15 152.07 7.89 . . . . . . . 5996 5 119 . 1 1 162 162 GLU N N 15 266.65 15.65 . . . . . . . 5996 5 stop_ save_ save_308_600_bound_t2 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 308_600_bound_t2 _Heteronucl_T2_list.Entry_ID 5996 _Heteronucl_T2_list.ID 6 _Heteronucl_T2_list.Sample_condition_list_ID 6 _Heteronucl_T2_list.Sample_condition_list_label $308K _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 600 _Heteronucl_T2_list.T2_coherence_type Nx _Heteronucl_T2_list.T2_val_units ms _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 1 '15N T2' 1 $sample_1 . 5996 6 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 ALA N N 15 107.72 7.17 . . . . . . . 5996 6 2 . 1 1 4 4 SER N N 15 112.72 5.20 . . . . . . . 5996 6 3 . 1 1 6 6 THR N N 15 76.47 4.78 . . . . . . . 5996 6 4 . 1 1 10 10 PHE N N 15 99.73 4.32 . . . . . . . 5996 6 5 . 1 1 11 11 ASN N N 15 96.72 8.22 . . . . . . . 5996 6 6 . 1 1 12 12 VAL N N 15 115.35 6.04 . . . . . . . 5996 6 7 . 1 1 13 13 GLU N N 15 80.49 9.66 . . . . . . . 5996 6 8 . 1 1 16 16 ASN N N 15 82.77 5.47 . . . . . . . 5996 6 9 . 1 1 17 17 GLY N N 15 104.07 5.71 . . . . . . . 5996 6 10 . 1 1 18 18 GLU N N 15 76.19 5.22 . . . . . . . 5996 6 11 . 1 1 19 19 TRP N N 15 97.80 6.21 . . . . . . . 5996 6 12 . 1 1 21 21 THR N N 15 106.36 6.71 . . . . . . . 5996 6 13 . 1 1 22 22 ILE N N 15 107.36 5.68 . . . . . . . 5996 6 14 . 1 1 23 23 ILE N N 15 97.80 6.54 . . . . . . . 5996 6 15 . 1 1 26 26 SER N N 15 92.45 5.08 . . . . . . . 5996 6 16 . 1 1 27 27 ASP N N 15 78.87 5.03 . . . . . . . 5996 6 17 . 1 1 29 29 ARG N N 15 103.08 6.65 . . . . . . . 5996 6 18 . 1 1 30 30 GLU N N 15 87.51 6.77 . . . . . . . 5996 6 19 . 1 1 31 31 LYS N N 15 138.40 5.79 . . . . . . . 5996 6 20 . 1 1 32 32 ILE N N 15 115.87 9.47 . . . . . . . 5996 6 21 . 1 1 33 33 GLU N N 15 75.36 5.92 . . . . . . . 5996 6 22 . 1 1 35 35 ASN N N 15 141.27 3.65 . . . . . . . 5996 6 23 . 1 1 36 36 GLY N N 15 91.49 4.88 . . . . . . . 5996 6 24 . 1 1 38 38 PHE N N 15 85.02 6.49 . . . . . . . 5996 6 25 . 1 1 39 39 ARG N N 15 84.44 5.88 . . . . . . . 5996 6 26 . 1 1 40 40 LEU N N 15 94.39 7.73 . . . . . . . 5996 6 27 . 1 1 42 42 LEU N N 15 116.48 2.81 . . . . . . . 5996 6 28 . 1 1 43 43 GLU N N 15 89.64 7.37 . . . . . . . 5996 6 29 . 1 1 45 45 ILE N N 15 93.65 7.54 . . . . . . . 5996 6 30 . 1 1 46 46 HIS N N 15 95.93 4.84 . . . . . . . 5996 6 31 . 1 1 47 47 VAL N N 15 98.00 4.72 . . . . . . . 5996 6 32 . 1 1 48 48 LEU N N 15 98.78 9.59 . . . . . . . 5996 6 33 . 1 1 50 50 ASN N N 15 85.76 6.36 . . . . . . . 5996 6 34 . 1 1 51 51 SER N N 15 90.02 18.26 . . . . . . . 5996 6 35 . 1 1 52 52 LEU N N 15 103.78 3.89 . . . . . . . 5996 6 36 . 1 1 53 53 VAL N N 15 93.73 3.32 . . . . . . . 5996 6 37 . 1 1 54 54 LEU N N 15 97.92 5.93 . . . . . . . 5996 6 38 . 1 1 57 57 HIS N N 15 73.75 2.64 . . . . . . . 5996 6 39 . 1 1 60 60 ARG N N 15 90.45 4.74 . . . . . . . 5996 6 40 . 1 1 61 61 ASP N N 15 67.63 6.23 . . . . . . . 5996 6 41 . 1 1 62 62 GLU N N 15 53.51 5.68 . . . . . . . 5996 6 42 . 1 1 64 64 CYS N N 15 88.79 5.30 . . . . . . . 5996 6 43 . 1 1 65 65 SER N N 15 114.22 4.05 . . . . . . . 5996 6 44 . 1 1 66 66 GLU N N 15 108.53 7.49 . . . . . . . 5996 6 45 . 1 1 67 67 LEU N N 15 87.33 4.91 . . . . . . . 5996 6 46 . 1 1 68 68 SER N N 15 105.68 5.72 . . . . . . . 5996 6 47 . 1 1 69 69 MET N N 15 100.66 5.02 . . . . . . . 5996 6 48 . 1 1 71 71 ALA N N 15 100.46 5.64 . . . . . . . 5996 6 49 . 1 1 72 72 ASP N N 15 101.46 4.27 . . . . . . . 5996 6 50 . 1 1 74 74 THR N N 15 104.25 6.27 . . . . . . . 5996 6 51 . 1 1 75 75 GLU N N 15 90.49 7.15 . . . . . . . 5996 6 52 . 1 1 77 77 ALA N N 15 99.88 6.05 . . . . . . . 5996 6 53 . 1 1 78 78 GLY N N 15 89.31 5.30 . . . . . . . 5996 6 54 . 1 1 79 79 GLU N N 15 83.74 4.84 . . . . . . . 5996 6 55 . 1 1 80 80 TYR N N 15 89.60 2.85 . . . . . . . 5996 6 56 . 1 1 81 81 SER N N 15 110.47 6.04 . . . . . . . 5996 6 57 . 1 1 82 82 VAL N N 15 88.52 8.18 . . . . . . . 5996 6 58 . 1 1 84 84 TYR N N 15 114.73 3.31 . . . . . . . 5996 6 59 . 1 1 85 85 ASP N N 15 102.38 7.66 . . . . . . . 5996 6 60 . 1 1 86 86 GLY N N 15 103.02 4.16 . . . . . . . 5996 6 61 . 1 1 87 87 PHE N N 15 93.80 5.97 . . . . . . . 5996 6 62 . 1 1 88 88 ASN N N 15 90.25 3.45 . . . . . . . 5996 6 63 . 1 1 89 89 THR N N 15 93.22 6.05 . . . . . . . 5996 6 64 . 1 1 90 90 PHE N N 15 84.51 3.66 . . . . . . . 5996 6 65 . 1 1 91 91 THR N N 15 113.73 5.70 . . . . . . . 5996 6 66 . 1 1 92 92 ILE N N 15 96.38 6.74 . . . . . . . 5996 6 67 . 1 1 94 94 LYS N N 15 89.94 3.90 . . . . . . . 5996 6 68 . 1 1 95 95 THR N N 15 96.22 6.06 . . . . . . . 5996 6 69 . 1 1 96 96 ASP N N 15 85.78 6.59 . . . . . . . 5996 6 70 . 1 1 97 97 TYR N N 15 98.90 8.19 . . . . . . . 5996 6 71 . 1 1 98 98 ASP N N 15 90.40 5.09 . . . . . . . 5996 6 72 . 1 1 99 99 ASN N N 15 45.84 6.23 . . . . . . . 5996 6 73 . 1 1 100 100 PHE N N 15 90.38 7.07 . . . . . . . 5996 6 74 . 1 1 103 103 ALA N N 15 103.27 5.21 . . . . . . . 5996 6 75 . 1 1 104 104 HIS N N 15 115.83 7.82 . . . . . . . 5996 6 76 . 1 1 105 105 LEU N N 15 95.50 5.56 . . . . . . . 5996 6 77 . 1 1 107 107 ASN N N 15 96.98 6.91 . . . . . . . 5996 6 78 . 1 1 108 108 GLU N N 15 104.89 2.88 . . . . . . . 5996 6 79 . 1 1 109 109 LYS N N 15 97.78 6.99 . . . . . . . 5996 6 80 . 1 1 111 111 GLY N N 15 103.48 6.22 . . . . . . . 5996 6 81 . 1 1 114 114 PHE N N 15 109.10 5.14 . . . . . . . 5996 6 82 . 1 1 115 115 GLN N N 15 94.51 5.67 . . . . . . . 5996 6 83 . 1 1 116 116 LEU N N 15 105.32 5.30 . . . . . . . 5996 6 84 . 1 1 117 117 MET N N 15 98.31 5.08 . . . . . . . 5996 6 85 . 1 1 118 118 GLY N N 15 99.59 7.14 . . . . . . . 5996 6 86 . 1 1 121 121 GLY N N 15 94.17 2.31 . . . . . . . 5996 6 87 . 1 1 123 123 GLU N N 15 97.46 7.92 . . . . . . . 5996 6 88 . 1 1 125 125 ASP N N 15 86.11 7.03 . . . . . . . 5996 6 89 . 1 1 126 126 LEU N N 15 97.38 4.62 . . . . . . . 5996 6 90 . 1 1 127 127 SER N N 15 113.53 13.92 . . . . . . . 5996 6 91 . 1 1 129 129 ASP N N 15 84.74 5.84 . . . . . . . 5996 6 92 . 1 1 130 130 ILE N N 15 85.85 6.13 . . . . . . . 5996 6 93 . 1 1 131 131 LYS N N 15 101.05 5.90 . . . . . . . 5996 6 94 . 1 1 133 133 ARG N N 15 90.50 5.31 . . . . . . . 5996 6 95 . 1 1 136 136 GLN N N 15 96.33 5.01 . . . . . . . 5996 6 96 . 1 1 137 137 LEU N N 15 86.03 4.71 . . . . . . . 5996 6 97 . 1 1 138 138 CYS N N 15 119.78 7.52 . . . . . . . 5996 6 98 . 1 1 140 140 LYS N N 15 86.38 4.63 . . . . . . . 5996 6 99 . 1 1 142 142 GLY N N 15 75.00 2.68 . . . . . . . 5996 6 100 . 1 1 143 143 ILE N N 15 83.27 6.44 . . . . . . . 5996 6 101 . 1 1 144 144 LEU N N 15 111.11 5.72 . . . . . . . 5996 6 102 . 1 1 145 145 ARG N N 15 109.22 5.47 . . . . . . . 5996 6 103 . 1 1 146 146 GLU N N 15 118.30 7.23 . . . . . . . 5996 6 104 . 1 1 148 148 ILE N N 15 91.33 3.55 . . . . . . . 5996 6 105 . 1 1 150 150 ASP N N 15 125.13 2.94 . . . . . . . 5996 6 106 . 1 1 151 151 LEU N N 15 101.32 5.45 . . . . . . . 5996 6 107 . 1 1 152 152 SER N N 15 82.28 5.07 . . . . . . . 5996 6 108 . 1 1 153 153 ASN N N 15 78.41 13.04 . . . . . . . 5996 6 109 . 1 1 155 155 ASN N N 15 85.43 7.10 . . . . . . . 5996 6 110 . 1 1 160 160 ALA N N 15 173.84 4.25 . . . . . . . 5996 6 111 . 1 1 162 162 GLU N N 15 292.98 4.74 . . . . . . . 5996 6 stop_ save_ save_291_500_bound_t2 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 291_500_bound_t2 _Heteronucl_T2_list.Entry_ID 5996 _Heteronucl_T2_list.ID 7 _Heteronucl_T2_list.Sample_condition_list_ID 7 _Heteronucl_T2_list.Sample_condition_list_label $291K _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 500 _Heteronucl_T2_list.T2_coherence_type Nx _Heteronucl_T2_list.T2_val_units ms _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 1 '15N T2' 1 $sample_1 . 5996 7 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 ALA N N 15 79.21 2.14 . . . . . . . 5996 7 2 . 1 1 4 4 SER N N 15 79.79 3.16 . . . . . . . 5996 7 3 . 1 1 5 5 SER N N 15 68.96 3.42 . . . . . . . 5996 7 4 . 1 1 6 6 THR N N 15 74.00 3.93 . . . . . . . 5996 7 5 . 1 1 7 7 GLY N N 15 78.56 2.35 . . . . . . . 5996 7 6 . 1 1 11 11 ASN N N 15 78.98 5.46 . . . . . . . 5996 7 7 . 1 1 13 13 GLU N N 15 65.40 3.54 . . . . . . . 5996 7 8 . 1 1 15 15 ILE N N 15 71.08 3.55 . . . . . . . 5996 7 9 . 1 1 16 16 ASN N N 15 65.50 2.74 . . . . . . . 5996 7 10 . 1 1 17 17 GLY N N 15 71.41 3.18 . . . . . . . 5996 7 11 . 1 1 18 18 GLU N N 15 46.13 2.11 . . . . . . . 5996 7 12 . 1 1 19 19 TRP N N 15 62.50 3.51 . . . . . . . 5996 7 13 . 1 1 20 20 HIS N N 15 63.70 3.18 . . . . . . . 5996 7 14 . 1 1 22 22 ILE N N 15 63.88 4.94 . . . . . . . 5996 7 15 . 1 1 23 23 ILE N N 15 76.66 6.71 . . . . . . . 5996 7 16 . 1 1 26 26 SER N N 15 71.82 2.65 . . . . . . . 5996 7 17 . 1 1 27 27 ASP N N 15 73.75 2.43 . . . . . . . 5996 7 18 . 1 1 29 29 ARG N N 15 74.87 4.87 . . . . . . . 5996 7 19 . 1 1 30 30 GLU N N 15 70.29 2.82 . . . . . . . 5996 7 20 . 1 1 31 31 LYS N N 15 67.49 3.92 . . . . . . . 5996 7 21 . 1 1 32 32 ILE N N 15 68.45 4.70 . . . . . . . 5996 7 22 . 1 1 33 33 GLU N N 15 71.39 3.14 . . . . . . . 5996 7 23 . 1 1 36 36 GLY N N 15 72.42 5.25 . . . . . . . 5996 7 24 . 1 1 37 37 ASN N N 15 74.01 3.57 . . . . . . . 5996 7 25 . 1 1 39 39 ARG N N 15 62.98 1.39 . . . . . . . 5996 7 26 . 1 1 40 40 LEU N N 15 66.67 5.03 . . . . . . . 5996 7 27 . 1 1 45 45 ILE N N 15 68.55 3.68 . . . . . . . 5996 7 28 . 1 1 46 46 HIS N N 15 74.91 3.87 . . . . . . . 5996 7 29 . 1 1 47 47 VAL N N 15 71.74 3.05 . . . . . . . 5996 7 30 . 1 1 48 48 LEU N N 15 75.92 4.65 . . . . . . . 5996 7 31 . 1 1 50 50 ASN N N 15 74.49 4.90 . . . . . . . 5996 7 32 . 1 1 51 51 SER N N 15 78.67 3.80 . . . . . . . 5996 7 33 . 1 1 52 52 LEU N N 15 73.97 3.27 . . . . . . . 5996 7 34 . 1 1 54 54 LEU N N 15 75.28 2.45 . . . . . . . 5996 7 35 . 1 1 58 58 THR N N 15 59.95 0.82 . . . . . . . 5996 7 36 . 1 1 60 60 ARG N N 15 78.76 3.81 . . . . . . . 5996 7 37 . 1 1 61 61 ASP N N 15 74.62 3.20 . . . . . . . 5996 7 38 . 1 1 62 62 GLU N N 15 64.71 0.95 . . . . . . . 5996 7 39 . 1 1 64 64 CYS N N 15 77.46 1.71 . . . . . . . 5996 7 40 . 1 1 66 66 GLU N N 15 73.14 3.19 . . . . . . . 5996 7 41 . 1 1 67 67 LEU N N 15 74.47 1.99 . . . . . . . 5996 7 42 . 1 1 68 68 SER N N 15 71.78 2.92 . . . . . . . 5996 7 43 . 1 1 69 69 MET N N 15 69.28 4.84 . . . . . . . 5996 7 44 . 1 1 71 71 ALA N N 15 78.22 3.95 . . . . . . . 5996 7 45 . 1 1 72 72 ASP N N 15 75.78 2.46 . . . . . . . 5996 7 46 . 1 1 74 74 THR N N 15 84.60 4.55 . . . . . . . 5996 7 47 . 1 1 75 75 GLU N N 15 81.40 4.03 . . . . . . . 5996 7 48 . 1 1 77 77 ALA N N 15 79.46 4.04 . . . . . . . 5996 7 49 . 1 1 78 78 GLY N N 15 91.77 5.12 . . . . . . . 5996 7 50 . 1 1 79 79 GLU N N 15 68.79 3.81 . . . . . . . 5996 7 51 . 1 1 80 80 TYR N N 15 70.82 4.68 . . . . . . . 5996 7 52 . 1 1 81 81 SER N N 15 76.57 3.75 . . . . . . . 5996 7 53 . 1 1 82 82 VAL N N 15 77.78 4.35 . . . . . . . 5996 7 54 . 1 1 84 84 TYR N N 15 74.70 3.91 . . . . . . . 5996 7 55 . 1 1 85 85 ASP N N 15 74.57 4.59 . . . . . . . 5996 7 56 . 1 1 86 86 GLY N N 15 70.76 2.83 . . . . . . . 5996 7 57 . 1 1 87 87 PHE N N 15 70.70 3.75 . . . . . . . 5996 7 58 . 1 1 89 89 THR N N 15 71.69 3.18 . . . . . . . 5996 7 59 . 1 1 90 90 PHE N N 15 64.06 2.41 . . . . . . . 5996 7 60 . 1 1 91 91 THR N N 15 75.68 3.55 . . . . . . . 5996 7 61 . 1 1 94 94 LYS N N 15 70.24 3.53 . . . . . . . 5996 7 62 . 1 1 95 95 THR N N 15 64.45 3.18 . . . . . . . 5996 7 63 . 1 1 96 96 ASP N N 15 63.46 2.24 . . . . . . . 5996 7 64 . 1 1 98 98 ASP N N 15 70.12 2.93 . . . . . . . 5996 7 65 . 1 1 100 100 PHE N N 15 66.42 3.25 . . . . . . . 5996 7 66 . 1 1 103 103 ALA N N 15 68.40 3.85 . . . . . . . 5996 7 67 . 1 1 105 105 LEU N N 15 73.89 4.10 . . . . . . . 5996 7 68 . 1 1 107 107 ASN N N 15 72.01 2.08 . . . . . . . 5996 7 69 . 1 1 108 108 GLU N N 15 72.70 2.08 . . . . . . . 5996 7 70 . 1 1 109 109 LYS N N 15 77.76 4.09 . . . . . . . 5996 7 71 . 1 1 110 110 ASP N N 15 79.93 3.16 . . . . . . . 5996 7 72 . 1 1 111 111 GLY N N 15 78.72 4.06 . . . . . . . 5996 7 73 . 1 1 115 115 GLN N N 15 73.41 4.60 . . . . . . . 5996 7 74 . 1 1 117 117 MET N N 15 68.92 1.37 . . . . . . . 5996 7 75 . 1 1 118 118 GLY N N 15 68.74 3.96 . . . . . . . 5996 7 76 . 1 1 121 121 GLY N N 15 67.96 3.32 . . . . . . . 5996 7 77 . 1 1 123 123 GLU N N 15 69.37 2.43 . . . . . . . 5996 7 78 . 1 1 125 125 ASP N N 15 70.93 2.86 . . . . . . . 5996 7 79 . 1 1 126 126 LEU N N 15 75.77 3.19 . . . . . . . 5996 7 80 . 1 1 127 127 SER N N 15 73.17 2.70 . . . . . . . 5996 7 81 . 1 1 128 128 SER N N 15 75.28 2.50 . . . . . . . 5996 7 82 . 1 1 130 130 ILE N N 15 73.23 4.55 . . . . . . . 5996 7 83 . 1 1 131 131 LYS N N 15 70.03 4.00 . . . . . . . 5996 7 84 . 1 1 133 133 ARG N N 15 69.50 3.93 . . . . . . . 5996 7 85 . 1 1 136 136 GLN N N 15 69.77 4.77 . . . . . . . 5996 7 86 . 1 1 137 137 LEU N N 15 68.86 4.46 . . . . . . . 5996 7 87 . 1 1 138 138 CYS N N 15 68.42 4.02 . . . . . . . 5996 7 88 . 1 1 140 140 LYS N N 15 69.83 2.33 . . . . . . . 5996 7 89 . 1 1 141 141 HIS N N 15 73.12 3.07 . . . . . . . 5996 7 90 . 1 1 142 142 GLY N N 15 74.34 3.40 . . . . . . . 5996 7 91 . 1 1 144 144 LEU N N 15 78.41 2.78 . . . . . . . 5996 7 92 . 1 1 145 145 ARG N N 15 74.95 3.50 . . . . . . . 5996 7 93 . 1 1 146 146 GLU N N 15 72.06 3.15 . . . . . . . 5996 7 94 . 1 1 148 148 ILE N N 15 73.49 2.70 . . . . . . . 5996 7 95 . 1 1 150 150 ASP N N 15 79.73 4.48 . . . . . . . 5996 7 96 . 1 1 151 151 LEU N N 15 70.22 6.26 . . . . . . . 5996 7 97 . 1 1 152 152 SER N N 15 55.64 4.32 . . . . . . . 5996 7 98 . 1 1 153 153 ASN N N 15 63.51 2.67 . . . . . . . 5996 7 99 . 1 1 155 155 ASN N N 15 62.43 17.1 . . . . . . . 5996 7 100 . 1 1 160 160 ALA N N 15 120.6 5.70 . . . . . . . 5996 7 101 . 1 1 162 162 GLU N N 15 258.7 12.8 . . . . . . . 5996 7 stop_ save_ save_297_500_bound_t2 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 297_500_bound_t2 _Heteronucl_T2_list.Entry_ID 5996 _Heteronucl_T2_list.ID 8 _Heteronucl_T2_list.Sample_condition_list_ID 8 _Heteronucl_T2_list.Sample_condition_list_label $297K _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 500 _Heteronucl_T2_list.T2_coherence_type Nx _Heteronucl_T2_list.T2_val_units ms _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 1 '15N T2' 1 $sample_1 . 5996 8 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 ALA N N 15 89.57 3.45 . . . . . . . 5996 8 2 . 1 1 4 4 SER N N 15 87.09 3.50 . . . . . . . 5996 8 3 . 1 1 5 5 SER N N 15 80.66 3.40 . . . . . . . 5996 8 4 . 1 1 6 6 THR N N 15 79.50 4.04 . . . . . . . 5996 8 5 . 1 1 7 7 GLY N N 15 97.24 2.45 . . . . . . . 5996 8 6 . 1 1 10 10 PHE N N 15 99.71 3.78 . . . . . . . 5996 8 7 . 1 1 11 11 ASN N N 15 90.00 3.57 . . . . . . . 5996 8 8 . 1 1 12 12 VAL N N 15 80.41 3.02 . . . . . . . 5996 8 9 . 1 1 13 13 GLU N N 15 66.51 1.56 . . . . . . . 5996 8 10 . 1 1 15 15 ILE N N 15 82.00 3.18 . . . . . . . 5996 8 11 . 1 1 16 16 ASN N N 15 68.87 2.96 . . . . . . . 5996 8 12 . 1 1 17 17 GLY N N 15 81.16 3.70 . . . . . . . 5996 8 13 . 1 1 18 18 GLU N N 15 110.2 3.88 . . . . . . . 5996 8 14 . 1 1 19 19 TRP N N 15 78.26 4.43 . . . . . . . 5996 8 15 . 1 1 20 20 HIS N N 15 70.65 12.4 . . . . . . . 5996 8 16 . 1 1 21 21 THR N N 15 86.88 5.47 . . . . . . . 5996 8 17 . 1 1 22 22 ILE N N 15 76.72 5.03 . . . . . . . 5996 8 18 . 1 1 23 23 ILE N N 15 78.96 2.78 . . . . . . . 5996 8 19 . 1 1 26 26 SER N N 15 83.27 2.73 . . . . . . . 5996 8 20 . 1 1 27 27 ASP N N 15 81.97 4.48 . . . . . . . 5996 8 21 . 1 1 29 29 ARG N N 15 84.03 2.54 . . . . . . . 5996 8 22 . 1 1 30 30 GLU N N 15 80.29 2.73 . . . . . . . 5996 8 23 . 1 1 31 31 LYS N N 15 75.61 2.41 . . . . . . . 5996 8 24 . 1 1 32 32 ILE N N 15 80.25 3.45 . . . . . . . 5996 8 25 . 1 1 33 33 GLU N N 15 81.05 3.93 . . . . . . . 5996 8 26 . 1 1 36 36 GLY N N 15 82.25 4.74 . . . . . . . 5996 8 27 . 1 1 37 37 ASN N N 15 85.79 2.96 . . . . . . . 5996 8 28 . 1 1 42 42 LEU N N 15 73.54 6.72 . . . . . . . 5996 8 29 . 1 1 43 43 GLU N N 15 68.67 3.14 . . . . . . . 5996 8 30 . 1 1 45 45 ILE N N 15 82.90 3.16 . . . . . . . 5996 8 31 . 1 1 46 46 HIS N N 15 83.30 2.19 . . . . . . . 5996 8 32 . 1 1 47 47 VAL N N 15 84.43 2.83 . . . . . . . 5996 8 33 . 1 1 48 48 LEU N N 15 84.39 3.13 . . . . . . . 5996 8 34 . 1 1 50 50 ASN N N 15 82.58 3.64 . . . . . . . 5996 8 35 . 1 1 51 51 SER N N 15 89.80 4.41 . . . . . . . 5996 8 36 . 1 1 52 52 LEU N N 15 84.01 3.25 . . . . . . . 5996 8 37 . 1 1 54 54 LEU N N 15 81.87 1.89 . . . . . . . 5996 8 38 . 1 1 57 57 HIS N N 15 70.09 4.57 . . . . . . . 5996 8 39 . 1 1 58 58 THR N N 15 68.36 1.94 . . . . . . . 5996 8 40 . 1 1 60 60 ARG N N 15 91.11 3.07 . . . . . . . 5996 8 41 . 1 1 62 62 GLU N N 15 41.63 3.05 . . . . . . . 5996 8 42 . 1 1 64 64 CYS N N 15 90.08 3.11 . . . . . . . 5996 8 43 . 1 1 65 65 SER N N 15 86.93 3.35 . . . . . . . 5996 8 44 . 1 1 66 66 GLU N N 15 85.06 3.30 . . . . . . . 5996 8 45 . 1 1 67 67 LEU N N 15 85.26 3.60 . . . . . . . 5996 8 46 . 1 1 68 68 SER N N 15 83.87 2.89 . . . . . . . 5996 8 47 . 1 1 69 69 MET N N 15 78.31 3.74 . . . . . . . 5996 8 48 . 1 1 71 71 ALA N N 15 85.88 3.92 . . . . . . . 5996 8 49 . 1 1 74 74 THR N N 15 87.71 4.05 . . . . . . . 5996 8 50 . 1 1 75 75 GLU N N 15 92.57 5.10 . . . . . . . 5996 8 51 . 1 1 77 77 ALA N N 15 90.50 3.83 . . . . . . . 5996 8 52 . 1 1 78 78 GLY N N 15 99.70 5.56 . . . . . . . 5996 8 53 . 1 1 79 79 GLU N N 15 79.33 3.45 . . . . . . . 5996 8 54 . 1 1 80 80 TYR N N 15 85.85 2.38 . . . . . . . 5996 8 55 . 1 1 81 81 SER N N 15 85.30 3.11 . . . . . . . 5996 8 56 . 1 1 82 82 VAL N N 15 92.66 8.00 . . . . . . . 5996 8 57 . 1 1 84 84 TYR N N 15 81.56 2.40 . . . . . . . 5996 8 58 . 1 1 85 85 ASP N N 15 84.43 4.16 . . . . . . . 5996 8 59 . 1 1 87 87 PHE N N 15 81.89 2.75 . . . . . . . 5996 8 60 . 1 1 89 89 THR N N 15 81.89 4.22 . . . . . . . 5996 8 61 . 1 1 90 90 PHE N N 15 64.81 3.20 . . . . . . . 5996 8 62 . 1 1 91 91 THR N N 15 83.68 3.02 . . . . . . . 5996 8 63 . 1 1 92 92 ILE N N 15 78.25 3.12 . . . . . . . 5996 8 64 . 1 1 94 94 LYS N N 15 78.19 3.18 . . . . . . . 5996 8 65 . 1 1 95 95 THR N N 15 59.27 5.05 . . . . . . . 5996 8 66 . 1 1 97 97 TYR N N 15 75.32 2.40 . . . . . . . 5996 8 67 . 1 1 98 98 ASP N N 15 77.96 3.99 . . . . . . . 5996 8 68 . 1 1 100 100 PHE N N 15 68.92 2.77 . . . . . . . 5996 8 69 . 1 1 103 103 ALA N N 15 80.34 4.36 . . . . . . . 5996 8 70 . 1 1 104 104 HIS N N 15 89.07 3.97 . . . . . . . 5996 8 71 . 1 1 105 105 LEU N N 15 77.81 4.04 . . . . . . . 5996 8 72 . 1 1 107 107 ASN N N 15 83.32 2.94 . . . . . . . 5996 8 73 . 1 1 108 108 GLU N N 15 82.84 2.43 . . . . . . . 5996 8 74 . 1 1 109 109 LYS N N 15 86.17 2.81 . . . . . . . 5996 8 75 . 1 1 110 110 ASP N N 15 88.74 1.85 . . . . . . . 5996 8 76 . 1 1 111 111 GLY N N 15 90.31 3.63 . . . . . . . 5996 8 77 . 1 1 113 113 THR N N 15 89.53 3.26 . . . . . . . 5996 8 78 . 1 1 115 115 GLN N N 15 82.34 3.68 . . . . . . . 5996 8 79 . 1 1 117 117 MET N N 15 78.65 4.47 . . . . . . . 5996 8 80 . 1 1 118 118 GLY N N 15 76.17 2.99 . . . . . . . 5996 8 81 . 1 1 121 121 GLY N N 15 76.70 4.34 . . . . . . . 5996 8 82 . 1 1 123 123 GLU N N 15 80.29 3.20 . . . . . . . 5996 8 83 . 1 1 125 125 ASP N N 15 81.93 4.42 . . . . . . . 5996 8 84 . 1 1 126 126 LEU N N 15 84.30 2.64 . . . . . . . 5996 8 85 . 1 1 127 127 SER N N 15 86.15 3.71 . . . . . . . 5996 8 86 . 1 1 128 128 SER N N 15 82.45 3.61 . . . . . . . 5996 8 87 . 1 1 129 129 ASP N N 15 79.63 3.30 . . . . . . . 5996 8 88 . 1 1 130 130 ILE N N 15 81.01 4.03 . . . . . . . 5996 8 89 . 1 1 131 131 LYS N N 15 77.27 2.89 . . . . . . . 5996 8 90 . 1 1 133 133 ARG N N 15 79.57 2.49 . . . . . . . 5996 8 91 . 1 1 136 136 GLN N N 15 79.59 2.40 . . . . . . . 5996 8 92 . 1 1 137 137 LEU N N 15 79.13 4.36 . . . . . . . 5996 8 93 . 1 1 138 138 CYS N N 15 76.27 2.24 . . . . . . . 5996 8 94 . 1 1 140 140 LYS N N 15 79.76 3.34 . . . . . . . 5996 8 95 . 1 1 141 141 HIS N N 15 83.75 2.61 . . . . . . . 5996 8 96 . 1 1 142 142 GLY N N 15 83.95 3.99 . . . . . . . 5996 8 97 . 1 1 144 144 LEU N N 15 88.12 4.60 . . . . . . . 5996 8 98 . 1 1 145 145 ARG N N 15 81.71 2.54 . . . . . . . 5996 8 99 . 1 1 146 146 GLU N N 15 80.63 3.11 . . . . . . . 5996 8 100 . 1 1 148 148 ILE N N 15 83.49 4.51 . . . . . . . 5996 8 101 . 1 1 150 150 ASP N N 15 87.69 3.70 . . . . . . . 5996 8 102 . 1 1 151 151 LEU N N 15 77.44 3.97 . . . . . . . 5996 8 103 . 1 1 152 152 SER N N 15 67.52 1.92 . . . . . . . 5996 8 104 . 1 1 153 153 ASN N N 15 57.61 3.65 . . . . . . . 5996 8 105 . 1 1 155 155 ASN N N 15 72.18 5.47 . . . . . . . 5996 8 106 . 1 1 160 160 ALA N N 15 148.3 4.67 . . . . . . . 5996 8 107 . 1 1 162 162 GLU N N 15 291.6 10.3 . . . . . . . 5996 8 stop_ save_ save_302_500_bound_t2 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 302_500_bound_t2 _Heteronucl_T2_list.Entry_ID 5996 _Heteronucl_T2_list.ID 9 _Heteronucl_T2_list.Sample_condition_list_ID 9 _Heteronucl_T2_list.Sample_condition_list_label $302K _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 500 _Heteronucl_T2_list.T2_coherence_type Nx _Heteronucl_T2_list.T2_val_units ms _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 1 '15N T2' 1 $sample_1 . 5996 9 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 ALA N N 15 99.44 5.07 . . . . . . . 5996 9 2 . 1 1 4 4 SER N N 15 103.4 3.13 . . . . . . . 5996 9 3 . 1 1 6 6 THR N N 15 95.90 2.95 . . . . . . . 5996 9 4 . 1 1 10 10 PHE N N 15 119.5 6.01 . . . . . . . 5996 9 5 . 1 1 11 11 ASN N N 15 103.3 4.82 . . . . . . . 5996 9 6 . 1 1 12 12 VAL N N 15 91.12 3.05 . . . . . . . 5996 9 7 . 1 1 13 13 GLU N N 15 83.27 3.75 . . . . . . . 5996 9 8 . 1 1 16 16 ASN N N 15 82.80 2.35 . . . . . . . 5996 9 9 . 1 1 17 17 GLY N N 15 90.64 3.46 . . . . . . . 5996 9 10 . 1 1 18 18 GLU N N 15 102.1 4.29 . . . . . . . 5996 9 11 . 1 1 19 19 TRP N N 15 86.52 4.61 . . . . . . . 5996 9 12 . 1 1 21 21 THR N N 15 89.45 4.12 . . . . . . . 5996 9 13 . 1 1 22 22 ILE N N 15 84.10 4.56 . . . . . . . 5996 9 14 . 1 1 23 23 ILE N N 15 91.56 3.55 . . . . . . . 5996 9 15 . 1 1 26 26 SER N N 15 93.06 2.47 . . . . . . . 5996 9 16 . 1 1 27 27 ASP N N 15 91.00 3.66 . . . . . . . 5996 9 17 . 1 1 29 29 ARG N N 15 101.5 3.36 . . . . . . . 5996 9 18 . 1 1 30 30 GLU N N 15 93.22 2.81 . . . . . . . 5996 9 19 . 1 1 31 31 LYS N N 15 85.92 2.88 . . . . . . . 5996 9 20 . 1 1 32 32 ILE N N 15 92.52 4.13 . . . . . . . 5996 9 21 . 1 1 33 33 GLU N N 15 92.61 4.73 . . . . . . . 5996 9 22 . 1 1 35 35 ASN N N 15 97.80 3.28 . . . . . . . 5996 9 23 . 1 1 36 36 GLY N N 15 94.23 2.34 . . . . . . . 5996 9 24 . 1 1 39 39 ARG N N 15 88.00 4.82 . . . . . . . 5996 9 25 . 1 1 40 40 LEU N N 15 90.27 3.41 . . . . . . . 5996 9 26 . 1 1 42 42 LEU N N 15 85.23 7.79 . . . . . . . 5996 9 27 . 1 1 43 43 GLU N N 15 79.13 8.43 . . . . . . . 5996 9 28 . 1 1 46 46 HIS N N 15 94.78 3.44 . . . . . . . 5996 9 29 . 1 1 47 47 VAL N N 15 100.0 3.36 . . . . . . . 5996 9 30 . 1 1 48 48 LEU N N 15 96.59 3.38 . . . . . . . 5996 9 31 . 1 1 50 50 ASN N N 15 102.9 7.45 . . . . . . . 5996 9 32 . 1 1 51 51 SER N N 15 108.2 9.13 . . . . . . . 5996 9 33 . 1 1 52 52 LEU N N 15 94.56 4.52 . . . . . . . 5996 9 34 . 1 1 54 54 LEU N N 15 94.91 5.39 . . . . . . . 5996 9 35 . 1 1 60 60 ARG N N 15 103.0 4.37 . . . . . . . 5996 9 36 . 1 1 61 61 ASP N N 15 103.0 3.55 . . . . . . . 5996 9 37 . 1 1 62 62 GLU N N 15 57.55 3.75 . . . . . . . 5996 9 38 . 1 1 64 64 CYS N N 15 101.2 3.67 . . . . . . . 5996 9 39 . 1 1 65 65 SER N N 15 98.01 6.16 . . . . . . . 5996 9 40 . 1 1 66 66 GLU N N 15 97.14 3.83 . . . . . . . 5996 9 41 . 1 1 67 67 LEU N N 15 93.26 4.11 . . . . . . . 5996 9 42 . 1 1 68 68 SER N N 15 96.88 4.29 . . . . . . . 5996 9 43 . 1 1 69 69 MET N N 15 87.71 4.88 . . . . . . . 5996 9 44 . 1 1 71 71 ALA N N 15 94.20 3.15 . . . . . . . 5996 9 45 . 1 1 74 74 THR N N 15 102.3 3.97 . . . . . . . 5996 9 46 . 1 1 75 75 GLU N N 15 105.3 3.21 . . . . . . . 5996 9 47 . 1 1 77 77 ALA N N 15 108.2 4.30 . . . . . . . 5996 9 48 . 1 1 79 79 GLU N N 15 87.27 3.99 . . . . . . . 5996 9 49 . 1 1 81 81 SER N N 15 92.14 3.02 . . . . . . . 5996 9 50 . 1 1 82 82 VAL N N 15 90.60 3.04 . . . . . . . 5996 9 51 . 1 1 84 84 TYR N N 15 95.19 3.10 . . . . . . . 5996 9 52 . 1 1 85 85 ASP N N 15 95.69 4.16 . . . . . . . 5996 9 53 . 1 1 86 86 GLY N N 15 91.28 3.69 . . . . . . . 5996 9 54 . 1 1 88 88 ASN N N 15 93.00 2.49 . . . . . . . 5996 9 55 . 1 1 89 89 THR N N 15 93.81 3.55 . . . . . . . 5996 9 56 . 1 1 90 90 PHE N N 15 80.00 4.41 . . . . . . . 5996 9 57 . 1 1 91 91 THR N N 15 95.54 4.28 . . . . . . . 5996 9 58 . 1 1 94 94 LYS N N 15 88.47 2.60 . . . . . . . 5996 9 59 . 1 1 96 96 ASP N N 15 81.42 4.68 . . . . . . . 5996 9 60 . 1 1 97 97 TYR N N 15 81.88 3.67 . . . . . . . 5996 9 61 . 1 1 98 98 ASP N N 15 88.86 3.93 . . . . . . . 5996 9 62 . 1 1 99 99 ASN N N 15 83.84 2.99 . . . . . . . 5996 9 63 . 1 1 100 100 PHE N N 15 82.19 2.83 . . . . . . . 5996 9 64 . 1 1 101 101 LEU N N 15 83.56 4.62 . . . . . . . 5996 9 65 . 1 1 103 103 ALA N N 15 85.85 2.79 . . . . . . . 5996 9 66 . 1 1 104 104 HIS N N 15 96.29 4.74 . . . . . . . 5996 9 67 . 1 1 105 105 LEU N N 15 88.69 4.78 . . . . . . . 5996 9 68 . 1 1 107 107 ASN N N 15 91.52 4.55 . . . . . . . 5996 9 69 . 1 1 108 108 GLU N N 15 93.81 4.04 . . . . . . . 5996 9 70 . 1 1 110 110 ASP N N 15 102.8 4.87 . . . . . . . 5996 9 71 . 1 1 111 111 GLY N N 15 105.5 4.05 . . . . . . . 5996 9 72 . 1 1 113 113 THR N N 15 99.64 4.33 . . . . . . . 5996 9 73 . 1 1 115 115 GLN N N 15 92.48 3.99 . . . . . . . 5996 9 74 . 1 1 116 116 LEU N N 15 91.06 3.88 . . . . . . . 5996 9 75 . 1 1 117 117 MET N N 15 88.82 3.80 . . . . . . . 5996 9 76 . 1 1 121 121 GLY N N 15 87.99 4.42 . . . . . . . 5996 9 77 . 1 1 125 125 ASP N N 15 95.29 5.47 . . . . . . . 5996 9 78 . 1 1 127 127 SER N N 15 99.46 3.76 . . . . . . . 5996 9 79 . 1 1 128 128 SER N N 15 102.9 6.95 . . . . . . . 5996 9 80 . 1 1 129 129 ASP N N 15 88.38 4.26 . . . . . . . 5996 9 81 . 1 1 130 130 ILE N N 15 89.64 4.74 . . . . . . . 5996 9 82 . 1 1 131 131 LYS N N 15 88.12 2.57 . . . . . . . 5996 9 83 . 1 1 133 133 ARG N N 15 85.25 4.26 . . . . . . . 5996 9 84 . 1 1 136 136 GLN N N 15 87.80 3.55 . . . . . . . 5996 9 85 . 1 1 137 137 LEU N N 15 88.62 3.66 . . . . . . . 5996 9 86 . 1 1 138 138 CYS N N 15 85.64 3.68 . . . . . . . 5996 9 87 . 1 1 140 140 LYS N N 15 88.37 3.91 . . . . . . . 5996 9 88 . 1 1 141 141 HIS N N 15 92.97 3.61 . . . . . . . 5996 9 89 . 1 1 142 142 GLY N N 15 97.66 4.55 . . . . . . . 5996 9 90 . 1 1 144 144 LEU N N 15 100.1 4.72 . . . . . . . 5996 9 91 . 1 1 145 145 ARG N N 15 94.78 3.48 . . . . . . . 5996 9 92 . 1 1 146 146 GLU N N 15 92.58 2.90 . . . . . . . 5996 9 93 . 1 1 148 148 ILE N N 15 94.64 3.38 . . . . . . . 5996 9 94 . 1 1 150 150 ASP N N 15 96.56 3.44 . . . . . . . 5996 9 95 . 1 1 151 151 LEU N N 15 86.08 6.82 . . . . . . . 5996 9 96 . 1 1 152 152 SER N N 15 71.91 2.18 . . . . . . . 5996 9 97 . 1 1 153 153 ASN N N 15 85.80 6.05 . . . . . . . 5996 9 98 . 1 1 155 155 ASN N N 15 84.48 0.93 . . . . . . . 5996 9 99 . 1 1 160 160 ALA N N 15 191.2 6.64 . . . . . . . 5996 9 100 . 1 1 162 162 GLU N N 15 336.3 10.8 . . . . . . . 5996 9 stop_ save_