# 1 "/opt/topspin/exp/stan/nmr/lists/pp/dept135" ;dept135 ;avance-version (02/05/31) ;dept polarization transfer ;with 135 degree read pulse to give XH, XH3 positive and XH2 negative ;with decoupling during acquisition ; ;$CLASS=HighRes ;$DIM=1D ;$TYPE= ;$SUBTYPE= ;$COMMENT= # 1 "/opt/topspin/exp/stan/nmr/lists/pp/Avance.incl" 1 ;Avance3.incl ; for AV III ; ;avance-version (07/12/14) ; ;$CLASS=HighRes Incl ;$COMMENT= ;$Id: Avance3.incl,v 1.6.2.2 2007/12/14 16:06:46 ber Exp $ # 14 "/opt/topspin/exp/stan/nmr/lists/pp/dept135" 2 # 1 "/opt/topspin/exp/stan/nmr/lists/pp/Delay.incl" 1 ;Delay.incl - include file for commonly used delays ; ;version 00/02/07 ; ;$CLASS=HighRes Incl ;$COMMENT= ;general delays define delay DELTA define delay DELTA1 define delay DELTA2 define delay DELTA3 define delay DELTA4 define delay DELTA5 define delay DELTA6 define delay DELTA7 define delay DELTA8 define delay TAU define delay TAU1 define delay TAU2 define delay TAU3 define delay TAU4 define delay TAU5 ;delays for centering pulses define delay CEN_HN1 define delay CEN_HN2 define delay CEN_HN3 define delay CEN_HC1 define delay CEN_HC2 define delay CEN_HC3 define delay CEN_HC4 define delay CEN_HP1 define delay CEN_HP2 define delay CEN_CN1 define delay CEN_CN2 define delay CEN_CN3 define delay CEN_CN4 define delay CEN_CP1 define delay CEN_CP2 ;loop counters define loopcounter COUNTER define loopcounter SCALEF define loopcounter FACTOR1 define loopcounter FACTOR2 define loopcounter FACTOR3 ;$Id: Delay.incl,v 1.12 2005/11/10 12:16:58 ber Exp $ # 15 "/opt/topspin/exp/stan/nmr/lists/pp/dept135" 2 "p2=p1*2" "p4=p3*2" "d2=1s/(cnst2*2)" "d12=20u" "DELTA=p1*4/3.1416" # 1 "mc_line 27 file /opt/topspin/exp/stan/nmr/lists/pp/dept135 expanding definition part of mc command before ze" define delay MCWRK define delay MCREST "MCWRK = 0.333333*30m" "MCREST = 30m - 30m" dccorr # 27 "/opt/topspin/exp/stan/nmr/lists/pp/dept135" 1 ze # 1 "mc_line 27 file /opt/topspin/exp/stan/nmr/lists/pp/dept135 expanding definition of mc command after ze" # 28 "/opt/topspin/exp/stan/nmr/lists/pp/dept135" # 1 "mc_line 28 file /opt/topspin/exp/stan/nmr/lists/pp/dept135 expanding start label for mc command" 2 MCWRK * 2 do:f2 LBLF0, MCWRK MCREST # 29 "/opt/topspin/exp/stan/nmr/lists/pp/dept135" d1 d12 pl2:f2 (p3 ph1):f2 d2 (p4 ph2):f2 (p1 ph4 d2):f1 (p3*1.5 ph3):f2 (p2 ph5 d2):f1 DELTA pl12:f2 go=2 ph31 cpd2:f2 # 1 "mc_line 37 file /opt/topspin/exp/stan/nmr/lists/pp/dept135 expanding mc command in line" MCWRK do:f2 wr #0 MCWRK zd lo to LBLF0 times td0 MCWRK # 38 "/opt/topspin/exp/stan/nmr/lists/pp/dept135" exit ph1=0 ph2=0 2 1 3 ph3=1 1 1 1 3 3 3 3 ph4=0 0 0 0 0 0 0 0 1 1 1 1 1 1 1 1 2 2 2 2 2 2 2 2 3 3 3 3 3 3 3 3 ph5=0 2 0 2 0 2 0 2 1 3 1 3 1 3 1 3 ph31=1 1 3 3 3 3 1 1 2 2 0 0 0 0 2 2 3 3 1 1 1 1 3 3 0 0 2 2 2 2 0 0 ;pl1 : f1 channel - power level for pulse (default) ;pl2 : f2 channel - power level for pulse (default) ;pl12: f2 channel - power level for CPD/BB decoupling ;p1 : f1 channel - 90 degree high power pulse ;p2 : f1 channel - 180 degree high power pulse ;p3 : f2 channel - 90 degree high power pulse ;p4 : f2 channel - 180 degree high power pulse ;d1 : relaxation delay; 1-5 * T1 ;d2 : 1/(2J(XH)) ;d12: delay for power switching [20 usec] ;cnst2: = J(XH) ;NS: 4 * n, total number of scans: NS * TD0 ;DS: 8 ;cpd2: decoupling according to sequence defined by cpdprg2 ;pcpd2: f2 channel - 90 degree pulse for decoupling sequence ;DELTA: delay to compensate for chemical shift evolution during ; RF pulse in order to give same phase correction as ; for reference 1D spectrum ;$Id: dept135,v 1.10 2005/11/10 12:16:59 ber Exp $