label list: line no. pc label 283 0xffffffff 1 288 0xffffffff 2 289 0xffffffff LBLSTS2 290 0xffffffff LBLF2 291 0xffffffff LBLSTS1 292 0xffffffff LBLF1 294 0xffffffff 3 pulse program: /opt/topspin/data/gvts/nmr/CcR55_NC_crp/4/pulseprogram ============== dur0 == line 0 fixdel(1000.000000 usec) setNmr1: 0x10004 dur1 == line 0 fixdel(1000.000000 usec) 'noesyhsqcetgp3d_arom': line 1---> ;noesyhsqcetgp3d 'noesyhsqcetgp3d_arom': line 2---> ;avance-version (04/03/08) 'noesyhsqcetgp3d_arom': line 3---> ;NOESY-HSQC 'noesyhsqcetgp3d_arom': line 4---> ;3D sequence with 'noesyhsqcetgp3d_arom': line 5---> ; homonuclear correlation via dipolar coupling 'noesyhsqcetgp3d_arom': line 6---> ; dipolar coupling may be due to noe or chemical exchange. 'noesyhsqcetgp3d_arom': line 7---> ; H-1/X correlation via double inept transfer 'noesyhsqcetgp3d_arom': line 8---> ;phase sensitive (t1) 'noesyhsqcetgp3d_arom': line 9---> ;phase sensitive using Echo/Antiecho-TPPI gradient selection (t2) 'noesyhsqcetgp3d_arom': line 10---> ;using trim pulses in inept transfer 'noesyhsqcetgp3d_arom': line 11---> ;with decoupling during acquisition 'noesyhsqcetgp3d_arom': line 12---> ;using shaped pulses for inversion on f2 - channel 'noesyhsqcetgp3d_arom': line 13---> ;(use parameterset NOESYHSQCETGP3D) 'noesyhsqcetgp3d_arom': line 14---> ; 'noesyhsqcetgp3d_arom': line 15---> ;A.L. Davis, J. Keeler, E.D. Laue & D. Moskau, J. Magn. Reson. 98, 'noesyhsqcetgp3d_arom': line 16---> ; 207-216 (1992) 'noesyhsqcetgp3d_arom': line 17---> ;A.G. Palmer III, J. Cavanagh, P.E. Wright & M. Rance, J. Magn. 'noesyhsqcetgp3d_arom': line 18---> ; Reson. 93, 151-170 (1991) 'noesyhsqcetgp3d_arom': line 19---> ;L.E. Kay, P. Keifer & T. Saarinen, J. Am. Chem. Soc. 114, 'noesyhsqcetgp3d_arom': line 20---> ; 10663-5 (1992) 'noesyhsqcetgp3d_arom': line 21---> ;J. Schleucher et al., Angew. Chem. 114(10), 1518 (1993) 'Avance.incl': line 1---> ;Avance2.incl 'Avance.incl': line 2---> ; for 1 'Avance.incl': line 3---> ; 'Avance.incl': line 4---> ;avance-version (03/02/17) 'Avance.incl': line 122---> ;$Id: Avance2.incl,v 1.10 2003/02/25 14:46:08 ber Exp $ 'Grad.incl': line 1---> ;Grad2.incl - include file for Gradient Spectroscopy 'Grad.incl': line 2---> ; for 1 'Grad.incl': line 3---> ; 'Grad.incl': line 4---> ;avance-version (02/05/31) 'Grad.incl': line 24---> define list EA= 'Grad.incl': line 28---> ;$Id: Grad2.incl,v 1.7 2002/06/12 09:04:22 ber Exp $ 'Delay.incl': line 1---> ;Delay.incl - include file for commonly used delays 'Delay.incl': line 2---> ; 'Delay.incl': line 3---> ;version 00/02/07 'Delay.incl': line 6---> ;general delays 'Delay.incl': line 8---> define delay DELTA 'Delay.incl': line 9---> define delay DELTA1 'Delay.incl': line 10---> define delay DELTA2 'Delay.incl': line 11---> define delay DELTA3 'Delay.incl': line 12---> define delay DELTA4 'Delay.incl': line 13---> define delay DELTA5 'Delay.incl': line 14---> define delay DELTA6 'Delay.incl': line 15---> define delay DELTA7 'Delay.incl': line 16---> define delay DELTA8 'Delay.incl': line 18---> define delay TAU 'Delay.incl': line 19---> define delay TAU1 'Delay.incl': line 20---> define delay TAU2 'Delay.incl': line 21---> define delay TAU3 'Delay.incl': line 22---> define delay TAU4 'Delay.incl': line 23---> define delay TAU5 'Delay.incl': line 26---> ;delays for centering pulses 'Delay.incl': line 28---> define delay CEN_HN1 'Delay.incl': line 29---> define delay CEN_HN2 'Delay.incl': line 30---> define delay CEN_HN3 'Delay.incl': line 31---> define delay CEN_HC1 'Delay.incl': line 32---> define delay CEN_HC2 'Delay.incl': line 33---> define delay CEN_HC3 'Delay.incl': line 34---> define delay CEN_HC4 'Delay.incl': line 35---> define delay CEN_HP1 'Delay.incl': line 36---> define delay CEN_HP2 'Delay.incl': line 37---> define delay CEN_CN1 'Delay.incl': line 38---> define delay CEN_CN2 'Delay.incl': line 39---> define delay CEN_CN3 'Delay.incl': line 40---> define delay CEN_CN4 'Delay.incl': line 41---> define delay CEN_CP1 'Delay.incl': line 42---> define delay CEN_CP2 'Delay.incl': line 45---> ;loop counters 'Delay.incl': line 47---> define loopcounter COUNTER 'Delay.incl': line 48---> define loopcounter SCALEF 'Delay.incl': line 49---> define loopcounter FACTOR1 'Delay.incl': line 50---> define loopcounter FACTOR2 'Delay.incl': line 51---> define loopcounter FACTOR3 'Delay.incl': line 55---> ;$Id: Delay.incl,v 1.11 2002/06/12 09:04:22 ber Exp $ 'noesyhsqcetgp3d_arom': line 30---> "p2=p1*2" 'noesyhsqcetgp3d_arom': line 32---> "p4=p3*2" 'noesyhsqcetgp3d_arom': line 34---> "d0=3u" 'noesyhsqcetgp3d_arom': line 36---> "d4=1s/(cnst2*4)" 'noesyhsqcetgp3d_arom': line 38---> "d10=3u" 'noesyhsqcetgp3d_arom': line 40---> "d11=30m" 'noesyhsqcetgp3d_arom': line 42---> "d12=20u" 'noesyhsqcetgp3d_arom': line 45---> "DELTA2=d4-larger(p2,p14)/2-p16-8u" 'noesyhsqcetgp3d_arom': line 46---> "DELTA3=d4-larger(p2,p14)/2" 'noesyhsqcetgp3d_arom': line 49---> "DELTA=larger(p14,p22)+d0*2" 'noesyhsqcetgp3d_arom': line 50---> "DELTA1=p16+d16+larger(p2,p22)+d10*2" 'noesyhsqcetgp3d_arom': line 57---> aqseq 321 'noesyhsqcetgp3d_arom': line 60, ex line 1---> ; dimension 3 aq-mode (F2) Echo-Antiecho (F1) States-TPPI F2->F1 'noesyhsqcetgp3d_arom': line 60, ex line 2---> define delay MCWRK 'noesyhsqcetgp3d_arom': line 60, ex line 3---> define delay MCREST 'noesyhsqcetgp3d_arom': line 60, ex line 4---> define loopcounter ST1CNT 'noesyhsqcetgp3d_arom': line 60, ex line 5---> "ST1CNT = td1 / (2)" 'noesyhsqcetgp3d_arom': line 60, ex line 6---> define loopcounter ST2CNT 'noesyhsqcetgp3d_arom': line 60, ex line 7---> "ST2CNT = td2 / (2)" 'noesyhsqcetgp3d_arom': line 60, ex line 8---> "MCWRK = 0.111111*d1" 'noesyhsqcetgp3d_arom': line 60, ex line 9---> "MCREST = d1 - d1" 'noesyhsqcetgp3d_arom': line 60---> 1 ze dur2 == line 283 fixdel(3000.000000 usec) EVENT-EOSZ ze1 'noesyhsqcetgp3d_arom': line 61---> d11 pl12:f2 dur3 == line 286 d11 channel 2: set power PL12 'noesyhsqcetgp3d_arom': line 62, ex line 1---> 2 MCWRK do:f2 dur4 == line 288 MCWRK channel 2: DO 'noesyhsqcetgp3d_arom': line 62, ex line 2---> LBLSTS2, MCWRK * 4 dur5 == line 289 MCWRK * 4 'noesyhsqcetgp3d_arom': line 62, ex line 3---> LBLF2, MCWRK * 3 dur6 == line 290 MCWRK * 3 'noesyhsqcetgp3d_arom': line 62, ex line 4---> LBLSTS1, MCWRK dur7 == line 291 MCWRK 'noesyhsqcetgp3d_arom': line 62, ex line 5---> LBLF1, MCREST dur8 == line 292 MCREST 'noesyhsqcetgp3d_arom': line 63---> 3 d12 pl0:f2 dur9 == line 294 d12 channel 2: set power PL0 'noesyhsqcetgp3d_arom': line 64---> (p1 ph7) Begin of PTList: lalign { dur10 == line 295 p1 SPF1 phase(7,0) } End of PTList 'noesyhsqcetgp3d_arom': line 65---> DELTA dur11 == line 296 DELTA 'noesyhsqcetgp3d_arom': line 66---> (p2 ph8) Begin of PTList: lalign { dur12 == line 297 p2 SPF1 phase(8,0) } End of PTList 'noesyhsqcetgp3d_arom': line 67---> d0 dur13 == line 298 d0 'noesyhsqcetgp3d_arom': line 70---> (center (p14:sp3 ph1):f2 (p22 ph1):f3 ) Begin of PTList: center { dur14 == line 301 p14 Shape SPF2 channel 2: shape pulse 3 via ptr -1 phase(1,0) } { dur15 == line 301 p22 SPF3 phase(1,0) } End of PTList 'noesyhsqcetgp3d_arom': line 75---> d0 dur16 == line 306 d0 'noesyhsqcetgp3d_arom': line 76---> (p1 ph1):f1 Begin of PTList: lalign { dur17 == line 307 p1 SPF1 phase(1,0) } End of PTList 'noesyhsqcetgp3d_arom': line 77---> d8 dur18 == line 308 d8 'noesyhsqcetgp3d_arom': line 78---> (p1 ph1):f1 Begin of PTList: lalign { dur19 == line 309 p1 SPF1 phase(1,0) } End of PTList 'noesyhsqcetgp3d_arom': line 79---> DELTA3 pl0:f2 dur20 == line 310 DELTA3 channel 2: set power PL0 'noesyhsqcetgp3d_arom': line 80---> 4u dur21 == line 311 fixdel(4.000000 usec) 'noesyhsqcetgp3d_arom': line 81---> (center (p2 ph1) (p13:sp6 ph6):f2 ) Begin of PTList: center { dur22 == line 312 p2 SPF1 phase(1,0) } { dur23 == line 312 p13 Shape SPF2 channel 2: shape pulse 6 via ptr -1 phase(6,0) } End of PTList 'noesyhsqcetgp3d_arom': line 82---> 4u dur24 == line 313 fixdel(4.000000 usec) 'noesyhsqcetgp3d_arom': line 83---> DELTA3 pl2:f2 setnmr3|0 setnmr0|34|32|33 dur25 == line 314 DELTA3 setRcp2: 0x7 setNmr1: 0x1 channel 2: set power PL2 'noesyhsqcetgp3d_arom': line 84---> p28 ph1 dur26 == line 315 p28 phase(1,0) 'noesyhsqcetgp3d_arom': line 85---> 4u dur27 == line 316 fixdel(4.000000 usec) 'noesyhsqcetgp3d_arom': line 86---> (p1 ph2) (p3 ph3):f2 Begin of PTList: lalign { dur28 == line 317 p1 SPF1 phase(2,0) } { dur29 == line 317 p3 SPF2 phase(3,0) } End of PTList 'noesyhsqcetgp3d_arom': line 87---> d10 dur30 == line 318 d10 'noesyhsqcetgp3d_arom': line 90---> (center (p2 ph5) (p22 ph1):f3 ) Begin of PTList: center { dur31 == line 321 p2 SPF1 phase(5,0) } { dur32 == line 321 p22 SPF3 phase(1,0) } End of PTList 'noesyhsqcetgp3d_arom': line 95---> d10 dur33 == line 326 d10 'noesyhsqcetgp3d_arom': line 96---> p16:gp1*EA dur34 == line 327 p16 NEXTGRAD 'noesyhsqcetgp3d_arom': line 97---> d16 dur35 == line 328 d16 'noesyhsqcetgp3d_arom': line 98---> (p4 ph4):f2 Begin of PTList: lalign { dur36 == line 329 p4 SPF2 phase(4,0) } End of PTList 'noesyhsqcetgp3d_arom': line 99---> DELTA1 dur37 == line 330 DELTA1 'noesyhsqcetgp3d_arom': line 100---> (ralign (p1 ph1) (p3 ph4):f2 ) Begin of PTList: ralign { dur38 == line 331 p1 SPF1 phase(1,0) } { dur39 == line 331 p3 SPF2 phase(4,0) } End of PTList 'noesyhsqcetgp3d_arom': line 101---> DELTA3 pl0:f2 dur40 == line 332 DELTA3 channel 2: set power PL0 'noesyhsqcetgp3d_arom': line 102---> (center (p2 ph1) (p13:sp6 ph1):f2 ) Begin of PTList: center { dur41 == line 333 p2 SPF1 phase(1,0) } { dur42 == line 333 p13 Shape SPF2 channel 2: shape pulse 6 via ptr -1 phase(1,0) } End of PTList 'noesyhsqcetgp3d_arom': line 103---> 4u dur43 == line 334 fixdel(4.000000 usec) 'noesyhsqcetgp3d_arom': line 104---> p16:gp2 dur44 == line 335 p16 NEXTGRAD 'noesyhsqcetgp3d_arom': line 105---> DELTA2 pl12:f2 dur45 == line 336 DELTA2 channel 2: set power PL12 'noesyhsqcetgp3d_arom': line 106---> 4u setnmr3^0 setnmr0^34^32^33 dur46 == line 337 fixdel(4.000000 usec) clrRcp2: 0x7 clrNmr1: 0x1 'noesyhsqcetgp3d_arom': line 107---> go=2 ph31 cpd2:f2 Begin of PTList: lalign { dur47 == line 338 de1 dur48 == line 338 fixdel(4.000000 usec) ADCGO RCU 1 channel 1: SY receive phase(31,8) receive + phase (0,8) } { dur49 == line 338 derx dur50 == line 338 fixdel(3.000000 usec) setNmr1: 0x200 } { dur51 == line 338 deadc dur52 == line 338 fixdel(2.000000 usec) setNmr1: 0x10100 phase(41,0) PHADDO PHREF } { dur53 == line 338 depa dur54 == line 338 fixdel(4.000000 usec) setNmr1: 0x400 dur55 == line 338 aq channel 1: CPDSNG prog 29 (CPDPRG30)via ptr 0 channel 2: CPD prog 1 (CPDPRG2)via ptr 0 dur56 == line 338 fixdel(2500.000000 usec) dur57 == line 338 fixdel(500.000000 usec) clrNmr1: 0x30700 channel 1: Dwell off channel 1: SY transmit EVENT-EOSZ eos1 loop to 'noesyhsqcetgp3d_arom': line 62, ex line 1 times ns (ns+ds) } End of PTList 'noesyhsqcetgp3d_arom': line 108, ex line 1---> MCWRK do:f2 wr #0 if #0 zd igrad EA 'noesyhsqcetgp3d_arom': line 108, ex line 2---> lo to LBLSTS2 times 2 dur58 == line 340 MCWRK channel 2: DO EVENT-EOSZ zd1 AQBUS-WR RCU 1 wrif 0 loop to 'noesyhsqcetgp3d_arom': line 62, ex line 2 times 2 'noesyhsqcetgp3d_arom': line 108, ex line 3---> MCWRK id10 MCWRK ip3*2 MCWRK ip6*2 MCWRK ip31*2 'noesyhsqcetgp3d_arom': line 108, ex line 4---> lo to LBLF2 times ST2CNT dur59 == line 342 MCWRK EVENT-ID 10 dur60 == line 342 MCWRK IRPTIPH 3 IRPTIFC3 dur61 == line 342 MCWRK IRPTIPH 6 IRPTIFC3 dur62 == line 342 MCWRK IRPTIPH 31 IRPTIFC3 loop to 'noesyhsqcetgp3d_arom': line 62, ex line 3 times l127 'noesyhsqcetgp3d_arom': line 108, ex line 5---> MCWRK rd10 MCWRK ip7 MCWRK ip8 'noesyhsqcetgp3d_arom': line 108, ex line 6---> lo to LBLSTS1 times 2 dur63 == line 344 MCWRK EVENT-RD 10 dur64 == line 344 MCWRK IRPTIPH 7 dur65 == line 344 MCWRK IRPTIPH 8 loop to 'noesyhsqcetgp3d_arom': line 62, ex line 4 times 2 'noesyhsqcetgp3d_arom': line 108, ex line 7---> MCWRK id0 'noesyhsqcetgp3d_arom': line 108, ex line 8---> lo to LBLF1 times ST1CNT dur66 == line 346 MCWRK EVENT-ID 0 loop to 'noesyhsqcetgp3d_arom': line 62, ex line 5 times l126 'noesyhsqcetgp3d_arom': line 111---> exit 'noesyhsqcetgp3d_arom': line 112---> dur67 == line 349 fixdel(50000.000000 usec) dur68 == line 349 fixdel(10000.000000 usec) EVENT-EOSZ esc0 dur69 == line 349 fixdel(10000.000000 usec) phase program no. 33: Fraction: 4.000000 Increment: 0x4000 = 90.00 degrees 0: 0 = 0.00 degrees 1: 0 = 0.00 degrees 2: 0x8000 = 180.00 degrees 3: 0x8000 = 180.00 degrees phase program no. 34: Fraction: 4.000000 Increment: 0x4000 = 90.00 degrees 0: 0 = 0.00 degrees 1: 0 = 0.00 degrees 2: 0x8000 = 180.00 degrees 3: 0x8000 = 180.00 degrees 4: 0x4000 = 90.00 degrees 5: 0x4000 = 90.00 degrees 6: 0xc000 = 270.00 degrees 7: 0xc000 = 270.00 degrees phase program no. 36: Fraction: 4.000000 Increment: 0x4000 = 90.00 degrees 0: 0 = 0.00 degrees phase program no. 37: Fraction: 4.000000 Increment: 0x4000 = 90.00 degrees 0: 0x4000 = 90.00 degrees phase program no. 38: Fraction: 4.000000 Increment: 0x4000 = 90.00 degrees 0: 0x8000 = 180.00 degrees phase program no. 39: Fraction: 4.000000 Increment: 0x4000 = 90.00 degrees 0: 0xc000 = 270.00 degrees phase program no. 41: Fraction: 4.000000 Increment: 0x4000 = 90.00 degrees 0: 0 = 0.00 degrees phase program no. 1: Fraction: 4.000000 Increment: 0x4000 = 90.00 degrees 0: 0 = 0.00 degrees phase program no. 2: Fraction: 4.000000 Increment: 0x4000 = 90.00 degrees 0: 0x4000 = 90.00 degrees phase program no. 3: Fraction: 4.000000 Increment: 0x4000 = 90.00 degrees 0: 0 = 0.00 degrees 1: 0x8000 = 180.00 degrees phase program no. 4: Fraction: 4.000000 Increment: 0x4000 = 90.00 degrees 0: 0 = 0.00 degrees 1: 0 = 0.00 degrees 2: 0 = 0.00 degrees 3: 0 = 0.00 degrees 4: 0 = 0.00 degrees 5: 0 = 0.00 degrees 6: 0 = 0.00 degrees 7: 0 = 0.00 degrees 8: 0x8000 = 180.00 degrees 9: 0x8000 = 180.00 degrees 10: 0x8000 = 180.00 degrees 11: 0x8000 = 180.00 degrees 12: 0x8000 = 180.00 degrees 13: 0x8000 = 180.00 degrees 14: 0x8000 = 180.00 degrees 15: 0x8000 = 180.00 degrees phase program no. 5: Fraction: 4.000000 Increment: 0x4000 = 90.00 degrees 0: 0 = 0.00 degrees 1: 0 = 0.00 degrees 2: 0x8000 = 180.00 degrees 3: 0x8000 = 180.00 degrees phase program no. 6: Fraction: 4.000000 Increment: 0x4000 = 90.00 degrees 0: 0 = 0.00 degrees phase program no. 7: Fraction: 4.000000 Increment: 0x4000 = 90.00 degrees 0: 0 = 0.00 degrees 1: 0 = 0.00 degrees 2: 0 = 0.00 degrees 3: 0 = 0.00 degrees 4: 0x8000 = 180.00 degrees 5: 0x8000 = 180.00 degrees 6: 0x8000 = 180.00 degrees 7: 0x8000 = 180.00 degrees phase program no. 8: Fraction: 4.000000 Increment: 0x4000 = 90.00 degrees 0: 0x4000 = 90.00 degrees 1: 0x4000 = 90.00 degrees 2: 0x4000 = 90.00 degrees 3: 0x4000 = 90.00 degrees 4: 0xc000 = 270.00 degrees 5: 0xc000 = 270.00 degrees 6: 0xc000 = 270.00 degrees 7: 0xc000 = 270.00 degrees phase program no. 31: Fraction: 4.000000 Increment: 0x4000 = 90.00 degrees 0: 0 = 0.00 degrees 1: 0x8000 = 180.00 degrees 2: 0 = 0.00 degrees 3: 0x8000 = 180.00 degrees 4: 0x8000 = 180.00 degrees 5: 0 = 0.00 degrees 6: 0x8000 = 180.00 degrees 7: 0 = 0.00 degrees 8: 0x8000 = 180.00 degrees 9: 0 = 0.00 degrees 10: 0x8000 = 180.00 degrees 11: 0 = 0.00 degrees 12: 0 = 0.00 degrees 13: 0x8000 = 180.00 degrees 14: 0 = 0.00 degrees 15: 0x8000 = 180.00 degrees file list: ================================================= filename actlineno offset ================================================= noesyhsqcetgp3d_arom 1 1 Avance.incl 25 25 noesyhsqcetgp3d_arom 148 125 Grad.incl 150 150 noesyhsqcetgp3d_arom 179 155 Delay.incl 181 181 noesyhsqcetgp3d_arom 237 212 noesyhsqcetgp3d_arom ex 272 212 noesyhsqcetgp3d_arom 282 223 noesyhsqcetgp3d_arom ex 284 223 noesyhsqcetgp3d_arom 285 225 noesyhsqcetgp3d_arom ex 287 225 noesyhsqcetgp3d_arom 293 231 noesyhsqcetgp3d_arom ex 339 231 noesyhsqcetgp3d_arom 348 238