BMRB Entry 19671
Chem Shift validation: AVS_full, LACS
BMRB Entry DOI: doi:10.13018/BMR19671
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Title: 3rC34Y, variant of Imunoglobulin light-chain of lambda 3 PubMed: 24816896
Deposition date: 2013-12-10 Original release date: 2015-04-15
Authors: Gil-Rodriguez, Paloma; Amero, Carlos
Citation: Gil-Rodriguez, Paloma; Amero, Carlos. "(1)H, (15)N and (13)C resonance assignments for 3rC and 3rCWP: amyloidogenic variants of imunoglobulin lambda 3 light-chain" Biomol NMR Assign. 9, 139-142 (2015).
Assembly members:
3rC34Y, polymer, 107 residues, Formula weight is not available
Natural source: Common Name: Human Taxonomy ID: 9606 Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Homo sapiens
Experimental source: Production method: recombinant technology Host organism: Escherichia coli
Entity Sequences (FASTA):
3rC34Y: SYELTQPPSVSVSPGQTASI
TCSGDKLGDKYAYWYQQKPG
QSPVLVIYQDSKRPSGIPER
FSGSNSGNTATLTISGTQAM
DEADYYCQAWDSSTAVVFGG
GTKLTVL
- assigned_chemical_shifts
Data type | Count |
13C chemical shifts | 273 |
15N chemical shifts | 91 |
1H chemical shifts | 458 |
Additional metadata:
Assembly:
Entity Assembly ID | Entity Name | Entity ID |
---|---|---|
1 | 3rC34Y | 1 |
Entities:
Entity 1, 3rC34Y 107 residues - Formula weight is not available
1 | SER | TYR | GLU | LEU | THR | GLN | PRO | PRO | SER | VAL | ||||
2 | SER | VAL | SER | PRO | GLY | GLN | THR | ALA | SER | ILE | ||||
3 | THR | CYS | SER | GLY | ASP | LYS | LEU | GLY | ASP | LYS | ||||
4 | TYR | ALA | TYR | TRP | TYR | GLN | GLN | LYS | PRO | GLY | ||||
5 | GLN | SER | PRO | VAL | LEU | VAL | ILE | TYR | GLN | ASP | ||||
6 | SER | LYS | ARG | PRO | SER | GLY | ILE | PRO | GLU | ARG | ||||
7 | PHE | SER | GLY | SER | ASN | SER | GLY | ASN | THR | ALA | ||||
8 | THR | LEU | THR | ILE | SER | GLY | THR | GLN | ALA | MET | ||||
9 | ASP | GLU | ALA | ASP | TYR | TYR | CYS | GLN | ALA | TRP | ||||
10 | ASP | SER | SER | THR | ALA | VAL | VAL | PHE | GLY | GLY | ||||
11 | GLY | THR | LYS | LEU | THR | VAL | LEU |
Samples:
sample_1: sodium phosphate 20 mM; sodium chloride 20 mM; 3rC34Y, [U-15N], 1 ± 0.3 mM; H2O 90%; D2O, [U-100% 2H], 10%
sample_2: sodium phosphate 20 mM; sodium chloride 20 mM; 3rC34Y, [U-13C; U-15N], 1 ± 0.3 mM; H2O 90%; D2O, [U-100% 2H], 10%
sample_3: TRIS 20 mM; 3rC34Y, [U-13C; U-15N], 1 ± 0.3 mM; sodium chloride 20 mM; H2O 90%; D2O, [U-100% 2H], 10%
sample_conditions_1: ionic strength: 0.02 M; pH: 6; pressure: 1 atm; temperature: 298 K
sample_conditions_2: ionic strength: 0.02 M; pH: 6; pressure: 1 atm; temperature: 303 K
sample_conditions_3: ionic strength: 0.02 M; pH: 8; pressure: 1 atm; temperature: 298 K
Experiments:
Name | Sample | Sample state | Sample conditions |
---|---|---|---|
2D 1H-15N HSQC | sample_1 | isotropic | sample_conditions_1 |
2D 1H-15N HSQC | sample_3 | isotropic | sample_conditions_3 |
2D 1H-15N HSQC | sample_1 | isotropic | sample_conditions_2 |
3D CBCA(CO)NH | sample_3 | isotropic | sample_conditions_3 |
3D HNCO | sample_3 | isotropic | sample_conditions_3 |
3D HNCA | sample_3 | isotropic | sample_conditions_3 |
3D HNCACB | sample_3 | isotropic | sample_conditions_3 |
3D HNCACB | sample_2 | isotropic | sample_conditions_1 |
3D HNCA | sample_2 | isotropic | sample_conditions_1 |
3D HCCH-TOCSY | sample_2 | isotropic | sample_conditions_1 |
3D 1H-15N NOESY | sample_2 | isotropic | sample_conditions_1 |
3D HBHA(CO)NH | sample_2 | isotropic | sample_conditions_2 |
3D HNCACB | sample_2 | isotropic | sample_conditions_2 |
3D HNCO | sample_2 | isotropic | sample_conditions_2 |
3D C(CO)NH | sample_2 | isotropic | sample_conditions_2 |
3D 1H-15N TOCSY | sample_2 | isotropic | sample_conditions_1 |
Software:
NMRPipe v7.9, Delaglio, Grzesiek, Vuister, Zhu, Pfeifer and Bax - processing
CARA v1.8.4, Keller and Wuthrich - data analysis
NMR spectrometers:
- Varian INOVA 700 MHz
Related Database Links:
PDB | |
BMRB | 19641 |
DBJ | BAA20022 BAC01665 BAC01796 |
EMBL | CAA12203 CAA80216 CAA85623 CAC10553 CAC10914 |
GB | AAA19492 AAB00975 AAC16875 AAD01813 AAD01814 |
PIR | S16440 S36065 |
PRF | 2001180C |
Download simulated HSQC data in one of the following formats:
CSV: Backbone
or all simulated shifts
SPARKY: Backbone
or all simulated shifts