BMRB Entry 15033
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR15033
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Title: Dimeric solution structure of the cyclic octamer d(CCGTCCGT) PubMed: 17260988
Deposition date: 2006-11-16 Original release date: 2007-10-16
Authors: Escaja, N.; Gomez-Pinto, I.; Pedroso, E.; Gonzalez, C.
Citation: Escaja, N.; Gomez-Pinto, I.; Pedroso, E.; Gonzalez, C.. "Four stranded DNA structures can be stabilized by two different types of minor groove G:C:G:C tetrads" J. Am. Chem. Soc. 129, 2004-2014 (2007).
Assembly members:
5'-D(P*CP*CP*GP*TP*CP*CP*GP*T)-3', polymer, 8 residues, Formula weight is not available
Natural source: Common Name: not available Taxonomy ID: not available Superkingdom: not available Kingdom: not available Genus/species: not available not available
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
5'-D(P*CP*CP*GP*TP*CP*CP*GP*T)-3': CCGTCCGT
- assigned_chemical_shifts
| Data type | Count |
| 13C chemical shifts | 20 |
| 1H chemical shifts | 43 |
| 31P chemical shifts | 4 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | subunit 1 | 1 |
| 2 | subunit 2 | 1 |
Entities:
Entity 1, subunit 1 8 residues - Formula weight is not available
| 1 | DC | DC | DG | DT | DC | DC | DG | DT |
Samples:
sample: 5'-D(P*CP*CP*GP*TP*CP*CP*GP*T)-3' 5 mM; sodium chloride 100 mM; H2O 90%; D2O 10%
sample_conditions_1: ionic strength: 100 mM; pH: 7; pressure: 1 atm; temperature: 289 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D 1H-1H NOESY | sample | isotropic | sample_conditions_1 |
| 2D DQF-COSY | sample | isotropic | sample_conditions_1 |
Software:
MARDIGRAS v1.5, T.L. James - iterative matrix relaxation
AMBER v7.0, Kollman et al - refinement
NMR spectrometers:
- Bruker AVANCE 600 MHz
- Bruker AVANCE 800 MHz