BMRB Entry 15460
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR15460
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Title: High resolution structure of AK12 in the presence of Lipopolysaccharide (LPS) PubMed: 18844294
Deposition date: 2007-09-05 Original release date: 2008-10-31
Authors: Bhunia, Anirban; Bhattacharjya, Surajit
Citation: Bhunia, Anirban; Mohanram, Harini; Bhattacharjya, Surajit. "Lipopolysaccharide bound structures of the active fragments of fowlicidin-1, a cathelicidin family of antimicrobial and antiendotoxic peptide from chicken, determined by transferred nuclear overhauser effect spectroscopy" Biopolymers 92, 9-22 (2009).
Assembly members:
AK12, polymer, 12 residues, 1428.736 Da.
Natural source: Common Name: not available Taxonomy ID: not available Superkingdom: not available Kingdom: not available Genus/species: not available not available
Experimental source: Production method: Standard F-moc solid phase peptide synthesised Host organism: Standard F-moc solid phase peptide synthesised
Entity Sequences (FASTA):
AK12: AGYNLYRAIKKK
- assigned_chemical_shifts
Data type | Count |
1H chemical shifts | 64 |
Additional metadata:
Assembly:
Entity Assembly ID | Entity Name | Entity ID |
---|---|---|
1 | AK12 | 1 |
Entities:
Entity 1, AK12 12 residues - 1428.736 Da.
1 | ALA | GLY | TYR | ASN | LEU | TYR | ARG | ALA | ILE | LYS | ||||
2 | LYS | LYS |
Samples:
sample_1: AK12 0.5 mM
sample_conditions_1: pH: 4.5; temperature: 288 K
Experiments:
Name | Sample | Sample state | Sample conditions |
---|---|---|---|
2D 1H-1H trNOESY | sample_1 | isotropic | sample_conditions_1 |
2D 1H-1H TOCSY | sample_1 | isotropic | sample_conditions_1 |
Software:
DYANA, Guntert, Braun and Wuthrich - refinement
NMR spectrometers:
- Bruker DRX 600 MHz