BMRB Entry 27
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR27
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Title: Proton Nuclear Magnetic Resonance Study of Hirudin: Resonance Assignment and Secondary Structure
Deposition date: 1995-07-31 Original release date: 1995-07-31
Authors: Sukumaran, Dinesh; Clore, G.; Preuss, Axel; Zarbock, Jutta; Gronenborn, Angela
Citation: Sukumaran, Dinesh; Clore, G.; Preuss, Axel; Zarbock, Jutta; Gronenborn, Angela. "Proton Nuclear Magnetic Resonance Study of Hirudin: Resonance Assignment and Secondary Structure" Biochemistry 26, 333-338 (1987).
Assembly members:
hirudin, polymer, 65 residues, Formula weight is not available
Natural source: Common Name: leech Taxonomy ID: 6421 Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Hirudo medicinalis
Experimental source: Production method: not available
Entity Sequences (FASTA):
hirudin: VVYTDCTESGQNLCLCEGSN
VCGQGNKCILGSDGEKNQCV
TGEGTPKPQSHNDGDFEEIP
EEXLQ
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 403 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | hirudin | 1 |
Entities:
Entity 1, hirudin 65 residues - Formula weight is not available
| 1 | VAL | VAL | TYR | THR | ASP | CYS | THR | GLU | SER | GLY | ||||
| 2 | GLN | ASN | LEU | CYS | LEU | CYS | GLU | GLY | SER | ASN | ||||
| 3 | VAL | CYS | GLY | GLN | GLY | ASN | LYS | CYS | ILE | LEU | ||||
| 4 | GLY | SER | ASP | GLY | GLU | LYS | ASN | GLN | CYS | VAL | ||||
| 5 | THR | GLY | GLU | GLY | THR | PRO | LYS | PRO | GLN | SER | ||||
| 6 | HIS | ASN | ASP | GLY | ASP | PHE | GLU | GLU | ILE | PRO | ||||
| 7 | GLU | GLU | TYS | LEU | GLN |
Samples:
sample_one: hirudin 8 mM
sample_condition_set_one: pH: 3 na; temperature: 298 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| not available | sample_one | not available | sample_condition_set_one |
Software:
No software information available
NMR spectrometers:
- unknown unknown 0 MHz