BMRB

Biological Magnetic Resonance Data Bank


A Repository for Data from NMR Spectroscopy on Proteins, Peptides, Nucleic Acids, and other Biomolecules
Member of WWPDB

BMRB Entry 5427

Title: pKa determinations for P1-Ala OMTKY3   PubMed: 12627950

Authors: Song, Jikui; Laskowski, Michael; Qasim, Mohammad; Markley, John

Citation: Song, Jikui; Laskowski, Michael; Qasim, Mohammad; Markley, John. "NMR Determination of pKa Values for Asp, Glu, His, and Lys Mutants at Each Variable Contiguous Enzyme-inhibitor Contact Position of the Turkey Ovomucoid Third Domain"  Biochemistry 42, 2847-2856 (2003).

Assembly members:
P1-Ala Turkey Ovomucoid Third Domain, polymer, 51 residues, Formula weight is not available

Natural source:   Common Name: Turkey   Taxonomy ID: 9103   Superkingdom: Eukaryota   Kingdom: Metazoa   Genus/species: Meleagris gallopavo

Experimental source:   Production method: recombinant technology

Entity Sequences (FASTA):
P1-Ala Turkey Ovomucoid Third Domain: VDCSEYPKPACTAEYRPLCG SDNKTYGNKCNFCNAVVESN GTLTLSHFGKC

Data sets:
  • assigned_chemical_shifts
Data typeCount
pH NMR parameter values47
pKa values4

Additional metadata:

  • Assembly
  • Samples and Experiments
  • Software
  • Spectrometers
  • Hide all

Assembly:

Entity Assembly IDEntity NameEntity ID
1P1-Ala OMTKY31

Entities:

Entity 1, P1-Ala OMTKY3 51 residues - Formula weight is not available

1   VALASPCYSSERGLUTYRPROLYSPROALA
2   CYSTHRALAGLUTYRARGPROLEUCYSGLY
3   SERASPASNLYSTHRTYRGLYASNLYSCYS
4   ASNPHECYSASNALAVALVALGLUSERASN
5   GLYTHRLEUTHRLEUSERHISPHEGLYLYS
6   CYS

Samples:

sample_1: P1-Ala Turkey Ovomucoid Third Domain 2 mM; KCl 100 mM; DSS 0.4 mM

conditions_set_1: ionic strength: 100 mM; pH: .; temperature: 298 K

Experiments:

NameSampleSample stateSample conditions
TOCSYsample_1not availableconditions_set_1

Software:

No software information available

NMR spectrometers:

  • Bruker DMX 500 MHz

Related Database Links:

BMRB 1374 1375 4068 42 4864 4865 507 5411 5424 5425 5426 5428 5429 5448 5469 5518 5520
PDB
PIR A31445 B61588 C31438 E31437 E31442
SWISS-PROT P52245 P67944 P67945 P67946 P67947